公开(公告)号：US08293950B2

公开(公告)日：2012-10-23

申请号：US11993843

申请日：2006-03-31

申请人： Yuanhua Jiang ,  Xiaoqin Yang ,  Pingguan Bian ,  Jiaxin Feng ,  Jinjun Dong ,  Huazhong He ,  Yuanhai Li ,  Yexiang Zhang ,  Leguan Huang

发明人： Yuanhua Jiang ,  Xiaoqin Yang ,  Pingguan Bian ,  Jiaxin Feng ,  Jinjun Dong ,  Huazhong He ,  Yuanhai Li ,  Yexiang Zhang ,  Leguan Huang

IPC分类号： C07C29/38 ,  C07C31/18 ,  C07C31/24

CPC分类号： C07C29/38 ,  C07C29/78 ,  C07C31/245

摘要： A method of preparing monopentaerythritol, dipentaerthritol, and sodium formate through high temperature condensation and cascade recrystallization is disclosed. The method lowers the energy consumption dramatically and improves the cost-effectiveness by carrying out the reaction in a non-low-temperature zone, and thereby avoiding the requirement for refrigeration. The method alleviates the difficulty of separation and improves the product quality by means of cascade separation process, and thereby avoiding the low purity from a single separation. In addition, the mother liquor obtained after each separation step is recycled to the previous step as the recycling liquor, which avoids discharging waste, increases the product yield and lowers raw materials consumption.

摘要翻译： 公开了通过高温冷凝和级联重结晶制备单季戊四醇，二季戊四醇和甲酸钠的方法。 该方法显着降低了能量消耗，通过在非低温区域进行反应提高了成本效益，从而避免了制冷的需要。 该方法减轻了分离的难度，通过级联分离方法提高了产品质量，从而避免了单一分离的低纯度。 此外，在每个分离步骤之后获得的母液被再循环至前一步骤，作为避免排放废物的再循环液体，增加了产品产率并降低了原料消耗。

公开(公告)号：US20100152500A1

公开(公告)日：2010-06-17

申请号：US11993843

申请日：2006-03-31

申请人： Yuanhua Jiang ,  Xiaoquin Yang ,  Pingguan Bian ,  Jiaxin Feng ,  Jinjun Dong ,  Huazhong He ,  Yuanhai Li ,  Yexiang Zhang ,  Leguan Huang

发明人： Yuanhua Jiang ,  Xiaoquin Yang ,  Pingguan Bian ,  Jiaxin Feng ,  Jinjun Dong ,  Huazhong He ,  Yuanhai Li ,  Yexiang Zhang ,  Leguan Huang

IPC分类号： C07C31/24

CPC分类号： C07C29/38 ,  C07C29/78 ,  C07C31/245

摘要： A method of preparing monopentaerythritol, dipentaerthritol, and sodium formate through high temperature condensation and cascade recrystallization is disclosed. The method lowers the energy consumption dramatically and improves the cost-effectiveness by carrying out the reaction in a non-low-temperature zone, and thereby avoiding the requirement for refrigeration. The method alleviates the difficulty of separation and improves the product quality by means of cascade separation process, and thereby avoiding the low purity from a single separation. In addition, the mother liquor obtained after each separation step is recycled to the previous step as the recycling liquor, which avoids discharging waste, increases the product yield and lowers raw materials consumption.

摘要翻译： 公开了通过高温冷凝和级联重结晶制备单季戊四醇，二季戊四醇和甲酸钠的方法。 该方法显着降低了能量消耗，通过在非低温区域进行反应提高了成本效益，从而避免了制冷的需要。 该方法减轻了分离的难度，通过级联分离方法提高了产品质量，从而避免了单一分离的低纯度。 此外，在每个分离步骤之后获得的母液被再循环至前一步骤，作为避免排放废物的再循环液体，增加了产品产率并降低了原料消耗。