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1.发明申请公开(公告)号：US20130259797A1
公开(公告)日：2013-10-03
申请号：US13601560
申请日：2012-08-31
申请人： Zhiguang JIANG , Dong HUA , Xiangyu LIU
发明人： Zhiguang JIANG , Dong HUA , Xiangyu LIU
IPC分类号： C01F11/28
CPC分类号： C01F11/28 , C01F11/32 , C01P2006/80
摘要： High-purity barium chloride (99.60% or more) is produced having low strontium (lower than 10 ppm) by using barium carbonate or a clear barium chloride filtration and hydrochloric acid mixed under agitation at a maintained temperature and pH. The barium chloride is obtained as liquid phase and then crystallized through further processes.
摘要翻译： 通过使用碳酸钡或透明氯化钡过滤和在搅拌下在保持的温度和pH下混合的盐酸生产低锶（低于10ppm）的高纯度氯化钡（99.60％以上）。 获得氯化钡作为液相，然后通过进一步的方法结晶。
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公开(公告)号：US20050226980A1
公开(公告)日：2005-10-13
申请号：US10820395
申请日：2004-04-08
申请人： Manoj Bhinde
发明人： Manoj Bhinde
CPC分类号： C01F11/32 , Y10S210/915
摘要： Significant amounts of soluble fluoride, known to create problems in processes requiring high quality grade calcium chloride, are removed from calcium chloride solution using hydroxyapatite as a removal mechanism. Under acidic conditions, calcium chloride solution is purified to about less than 10 ppm fluoride, significantly, to less than 1 ppm fluoride. At least 0.1 weight percent hydroxyapatite and concentrated hydrochloric acid are added to calcium chloride solution and slurried to remove fluoride and create a highly purified calcium chloride solution, substantially free of fluoride.
摘要翻译： 使用羟基磷灰石作为去除机理，从氯化钙溶液中除去大量可溶性氟化物，已知在需要高品质级氯化钙的方法中产生问题。 在酸性条件下，将氯化钙溶液纯化至大约低于10ppm的氟化物，显着地提纯至小于1ppm的氟化物。 将至少0.1重量％的羟基磷灰石和浓盐酸加入到氯化钙溶液中并浆化以除去氟化物，并产生基本上不含氟化物的高度纯化的氯化钙溶液。
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公开(公告)号：US3682602A
公开(公告)日：1972-08-08
申请号：US3682602D
申请日：1970-11-17
申请人： EDUARD MIKHAILOVICH MITKEVICH , VLADIMIR NIKOLAEVICH KOROBANOV , VERA JURIEVNA BABKINA , ALEXANDRA FILIPPOVNA SHAKHOVA , VLADIMIR NIKOLAEVICH MEFODIEV , NIKOLAI IVANOVICH GAIDASH
发明人： MITKEVICH EDUARD MIKHAILOVICH , KOROBANOV VLADIMIR NIKOLAEVICH , BABKINA VERA JURIEVNA , SHAKHOVA ALEXANDRA FILIPPOVNA , MEFODIEV VLADIMIR NIKOLAEVICH , GAIDASH NIKOLAI IVANOVICH
CPC分类号： C01D3/00 , C01D7/18 , C01F11/32 , Y10S159/25
摘要： CALCIUM AND SODIUM CHLORIDES ARE PRODUCED BY EVAPORATING THE DISTILLATION LIQUID RESULTING FROM THE AMMONIA SODA ASH PRODUCTION PROCESS. THIS LIQUID IS CLARIFIED AND INTRODUCED INTO THE EVAPORATORS TO MIX WITH A CONCENTRATED CALIUM CHLORIDE SOLUTION CONTAINED THEREIN, THE CONCENTRATION OF CALCIUM CHLORIDE IN SUCH A MIXED SOLUTION BEING MAINTAINED AT 28-45 WT. PERCENT. IN THE PROCESS ACCORDING TO THE METHOD DISCLOSED HEREIN, STEAM IS PASSED CONSECUTIVELY THROUGH ALL THE EVAPORATORS OF THE PLANT.
THE APPLICATION OF THE PROPOSED METHOD PRACTICALLY PRECLUDES THE FORMATION OF GYPSUM DEPOSITS ON THE HEATING SURFACES OF THE EVAPORATORS.-
公开(公告)号：US2032702A
公开(公告)日：1936-03-03
申请号：US72838534
申请日：1934-05-31
申请人： SOLVAY PROCESS CO
发明人： KEENE PAUL A , JULIEN ARLIE P
IPC分类号： C01F11/32
CPC分类号： C01F11/32
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公开(公告)号：US20240010516A1
公开(公告)日：2024-01-11
申请号：US18025278
申请日：2021-09-10
申请人： LIXIVIA, INC.
发明人： Michael D Wyrsta
CPC分类号： C01G49/02 , C01F11/28 , C01F11/32 , B01J20/06 , B01J20/3085 , B01D53/48 , B01D53/81 , B01D2257/30 , B01D2257/60 , B01D2256/245 , B01D2258/05 , B01D2253/1124
摘要： Methods for utilizing waste products of the steel industry are provided that utilize spent pickle liquor to recover valuable alkaline earth metals from low value wastes with significant calcium content in the form of insoluble oxide, hydroxides, and/or salts are provided, as well as methods for generating a ferric oxide hydroxide composite from steel slag. Suitable raw materials include slag from steel manufacturing and ash from various operations. Ferric oxide hydroxide composite materials described herein can be used for removal of sulfur and metals from contaminated materials. Accordingly, compositions and methods of the inventive concept introduce considerable value to low value waste materials that would otherwise be discarded. In addition, compositions and methods of the inventive concept serve to reduce waste streams from industrial processes.
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公开(公告)号：US07037480B2
公开(公告)日：2006-05-02
申请号：US10820395
申请日：2004-04-08
申请人： Manoj V. Bhinde
发明人： Manoj V. Bhinde
CPC分类号： C01F11/32 , Y10S210/915
摘要： Significant amounts of soluble fluoride, known to create problems in processes requiring high quality grade calcium chloride, are removed from calcium chloride solution using hydroxyapatite as a removal mechanism. Under acidic conditions, calcium chloride solution is purified to about less than 10 ppm fluoride, significantly, to less than 1 ppm fluoride. At least 0.1 weight percent hydroxyapatite and concentrated hydrochloric acid are added to calcium chloride solution and slurried to remove fluoride and create a highly purified calcium chloride solution, substantially free of fluoride.
摘要翻译： 使用羟基磷灰石作为去除机理，从氯化钙溶液中除去大量可溶性氟化物，已知在需要高品质级氯化钙的方法中产生问题。 在酸性条件下，将氯化钙溶液纯化至大约低于10ppm的氟化物，显着地提纯至小于1ppm的氟化物。 将至少0.1重量％的羟基磷灰石和浓盐酸加入到氯化钙溶液中并浆化以除去氟化物，并产生基本上不含氟化物的高度纯化的氯化钙溶液。
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7.发明申请Method of purifying metal salt, method of deacidifying titanium material and method of producing the same 审中-公开纯化金属盐的方法，钛材料脱酸方法及其制备方法公开(公告)号：US20050139483A1
公开(公告)日：2005-06-30
申请号：US10509250
申请日：2003-04-21
申请人： Shinji Shimosaki
发明人： Shinji Shimosaki
CPC分类号： C01D3/20 , C01F11/32 , C22B34/1295
摘要： A purification method of a metal salt which comprises bringing a metal salt formed by melting an alkali metal salt, an alkaline earth metal salt or a mixture thereof into contact with titanium or the like, thereby adsorbing impurities in the metal salt, a deoxidization method by melting metallic calcium into a molten product of the metal salt purified by the purification method and bringing the same into contact with a titanium material, and a production method of the titanium material which comprises conducting molten salt electrolysis by using the molten product of the purified metal salt for an electrolytic bath. Using the purification or production method the molten metal salt can be purified simply and conveniently at good efficiency. Then, use of the purified metal salt can minimize contamination caused by the metal impurities in the molten salt and the titanium material of high quality can be produced.
摘要翻译： 一种金属盐的净化方法，其特征在于，将通过使碱金属盐，碱土金属盐或其混合物熔融而形成的金属盐与钛等接触，从而吸附金属盐中的杂质，脱氧法由 将金属钙熔融成通过纯化方法纯化的金属盐的熔融产物，并使其与钛材料接触，以及钛材料的制造方法，其包括通过使用纯化金属的熔融产物进行熔融盐电解 盐为电解浴。 使用纯化或生产方法，可以以良好的效率简单方便地纯化熔融金属盐。 然后，使用纯化的金属盐可以最小化由熔融盐中的金属杂质引起的污染，并且可以生产高质量的钛材料。
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公开(公告)号：US5578218A
公开(公告)日：1996-11-26
申请号：US514624
申请日：1995-08-14
申请人： Terumi Matsuoka , Masahiro Ohara , Izumi Kawamura
发明人： Terumi Matsuoka , Masahiro Ohara , Izumi Kawamura
摘要： In a brine treatment method of removing sulfate ions from sulfate-ion contained brine, sulfate-ion contained brine is brought into dispersive contact with granular ion exchange resin carrying zirconium hydrous oxide thereon in a fluid state under an acidic condition to thereby cause the sulfate ions to be adsorbed by the ion exchange resin and removed from the brine, then the granular ion exchange resin is washed with aqueous solution whose pH value is equal to or lower than a pH value in the adsorbing step, thereby removing chloride ions from the granular ion exchange resin, then in a fluid state, the granular ion exchange resin adsorbing the sulfate ions is brought into dispersive contact with aqueous solution of pH value higher than the pH value in the adsorbing step, thereby desorbing the adsorbed sulfate ions from the granular ion exchange resin, and then the granular ion exchange resin is washed with water.
摘要翻译： 在从含有硫酸根离子的盐水中除去硫酸根离子的盐水处理方法中，在酸性条件下，将含有硫酸根离子的盐水与流动状态的载有氧化锆水的粒状离子交换树脂分散接触，从而使硫酸根离子 被离子交换树脂吸附并从盐水中除去，然后用吸附步骤中pH值等于或低于pH值的水溶液洗涤粒状离子交换树脂，从而从颗粒离子中除去氯离子 在流体状态下，吸附硫酸根离子的粒状离子交换树脂与吸附工序中pH值以上的pH值分散接触，从而从粒状离子交换器吸附硫酸根离子 树脂，然后用水洗涤颗粒状离子交换树脂。
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公开(公告)号：US5290531A
公开(公告)日：1994-03-01
申请号：US853392
申请日：1992-03-18
摘要： A method of converting sodium bromide brine to ammonium bromide brine and optionally to calcium bromide is disclosed. The method involves introducing ammonia and carbon dioxide into the reactant brine, removing a resulting bicarbonate precipitate, driving off any excess ammonium carbonate, and optionally contacting with lime.
摘要翻译： 公开了将溴化钠盐水转化为溴化铵盐水和任选地加入溴化钙的方法。 该方法包括将氨和二氧化碳引入反应物盐水中，除去所得的碳酸氢盐沉淀物，排除任何过量的碳酸铵，以及任选地与石灰接触。
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公开(公告)号：US2032727A
公开(公告)日：1936-03-03
申请号：US72838634
申请日：1934-05-31
申请人： SOLVAY PROCESS CO
发明人： CARL SUNDSTROM , HAYES JOHN W
IPC分类号： C01F11/32
CPC分类号： C01F11/32
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