公开(公告)号：WO99060356A1

公开(公告)日：1999-11-25

申请号：PCT/EP1999/003485

申请日：1999-05-20

IPC: G01K17/00 ,  G01K17/04 ,  G01N25/48

CPC classification number: G01N25/4866 ,  G01K17/00 ,  G01K17/04

Abstract: A method and an apparatus of heat flux control for calorimetry, adiabatic shielding, precise temperature setting and the like, on an object (2). The steps are provided of arranging a shield (1) about the object (2); heating uniformly (5) the shield (1) and monitoring (3) the heating step to maintain the shield (1) at a chosen temperature; arranging about the shield a thermal bath (7) at a known temperature in any case lower than the temperature of the shield (1); measuring the temperature of the object (2); and controlling (8) the heat flux (5) between the object (2) and the shield (1) by checking the temperature (4) of the object (2) and the temperature (3) of the shield (1). The application in the field of the calorimetry allows advantages and the use of a same calorimeter both in the classic adiabatic way, and in the temperature scanning adiabatic way as well as in the modulated way.

Abstract translation: 在物体（2）上的用于量热法，绝热屏蔽，精确温度设定等的热通量控制的方法和装置。 提供了围绕物体（2）布置屏蔽件（1）的步骤; 加热均匀（5）屏蔽（1）和监测（3）加热步骤以将屏蔽（1）保持在选定的温度; 在任何情况下，低于屏蔽（1）的温度，在已知温度下围绕屏蔽罩布置热浴（7）; 测量物体（2）的温度; 以及通过检查物体（2）的温度（4）和屏蔽件（1）的温度（3）来控制（8）物体（2）和屏蔽件（1）之间的热通量（5）。 在量热学领域的应用允许在经典绝热方式和温度扫描绝热方式以及调制方式中使用相同的量热计的优点和使用。

公开(公告)号：WO9928735A8

公开(公告)日：1999-07-29

申请号：PCT/US9825637

申请日：1998-12-02

Applicant: SMITH ALLAN L ,  WADSO INGEMAR

Inventor： SMITH ALLAN L ,  WADSO INGEMAR

IPC: G01G3/16 ,  G01G3/13 ,  G01K17/06 ,  G01K17/20 ,  G01N5/02 ,  G01N25/18 ,  G01N25/48 ,  G01N27/00 ,  G01N11/00

CPC classification number: G01G3/13 ,  G01K17/20 ,  G01N5/02 ,  G01N25/4813 ,  G01N25/4866

Abstract: Provided is a mass and heat flow measurement apparatus comprising sample and reference microresonators (70, 80), such as sample and reference quartz crystal microbalances; sample and reference heat flow sensors (75, 85), such as sample and reference isothermal heat conduction calorimeters; and sample and reference heat sinks coupled thermally to the heat flow sensors. The apparatus may be used to measure changes in mass due to sample (8) on a surface of the sample microresonator and also to measure heat flows from the sample (8) on the surface of the sample microresonator by utilizing the heat flow sensors, which are coupled thermally to the corresponding sample or reference microresonators. Also provided is a method for measuring the mass of a sample (8) and the flow of heat from the sample (8) to the heat sink by utilizing such apparatus.

Abstract translation: 提供了包括样品和参考微共振器（70,80），例如样品和参考石英晶体微量平衡的质量和热流测量装置; 样品和参考热流传感器（75,85），如样品和参考等温热传导量热仪; 以及与热流传感器热耦合的样品和参考散热器。 该装置可以用于测量样品微共振器表面上的样品（8）的质量变化，并且还通过利用热流传感器来测量样品微谐振器表面上的样品（8）的热流，其中 被热耦合到相应的样品或参考微谐振器。 还提供了一种通过利用这种装置来测量样品（8）的质量和从样品（8）到散热器的热量的方法。

公开(公告)号：WO99028735A1

公开(公告)日：1999-06-10

申请号：PCT/US1998/025637

申请日：1998-12-02

IPC: G01G3/16 ,  G01G3/13 ,  G01K17/06 ,  G01K17/20 ,  G01N5/02 ,  G01N25/18 ,  G01N25/48 ,  G01N27/00 ,  G01N11/00

CPC classification number: G01G3/13 ,  G01K17/20 ,  G01N5/02 ,  G01N25/4813 ,  G01N25/4866

Abstract: Provided is a mass and heat flow measurement apparatus comprising sample and reference microresonators, such as sample and reference quartz crystal microbalances (70, 80), sample and reference heat flow sensors (75, 85), such as sample and reference isothermal heat conduction calorimeters; and sample and reference heat sinks coupled thermally to the heat flow sensors. The apparatus may be used to measure changes in mass due to sample (8) on a surface of the microresonator and also to measure heat flows from the sample (8) on the surface of the sample microresonator by utilizing the heat flow sensors, which are coupled thermally to the corresponding sample or reference microresonators. Also provided is a method for measuring the mass of a sample (8) and the flow of heat from the sample (8) to the heat sink by utilizing such apparatus.

Abstract translation: 提供了一种质量和热流测量装置，其包括样品和参考微共振器，例如样品和参考石英晶体微量平衡（70,80），样品和参考热流传感器（75,85），例如样品和参考等温热传导量热计 ; 以及与热流传感器热耦合的样品和参考散热器。 该装置可以用于测量由于在微谐振器表面上的样品（8）的质量变化，并且还通过利用热流传感器来测量来自样品微谐振器表面上的样品（8）的热流 与相应的样品或参考微共振器热耦合。 还提供了一种通过利用这种装置来测量样品（8）的质量和从样品（8）到散热器的热量的方法。

公开(公告)号：WO99028734A1

公开(公告)日：1999-06-10

申请号：PCT/US1998/025636

申请日：1998-12-02

IPC: G01G3/16 ,  G01G3/13 ,  G01K17/06 ,  G01K17/20 ,  G01N5/02 ,  G01N25/18 ,  G01N25/48 ,  G01N27/00 ,  G01N11/00

CPC classification number: G01G3/13 ,  G01K17/20 ,  G01N5/02 ,  G01N25/4813 ,  G01N25/4866

Abstract: Provided are mass and heat flow measurement sensors comprising a microresonator, such as a quartz crystal microbalance; a heat flow sensor (c), such as an isothermal heat conduction calorimeter; and a heat sink (d) coupled thermally to the heat flow sensor. The sensors may be used to measure changes in mass due to a sample (8) on a surface of the microresonator and also to measure heat flow from the sample (8) on the surface of the microresonator by utilizing the heat flow sensor, which is coupled thermally to the microresonator. Also provided are methods for measuring the mass of a sample (8) and the flow of heat from the sample (8) to the heat sink (d) by utilizing such mass and heat flow measurement sensors.

Abstract translation: 提供了包括微谐振器（例如石英晶体微量天平）的质量和热流测量传感器; 诸如等温热传导量热计的热流传感器（c）; 和与热流传感器热耦合的散热器（d）。 传感器可用于测量由于在微谐振器表面上的样品（8）的质量变化，并且还通过利用热流传感器来测量来自微谐振器表面上的样品（8）的热流 与微谐振器热耦合。 还提供了通过利用这种质量和热流测量传感器来测量样品（8）的质量和从样品（8）到散热器（d）的热量的方法。

公开(公告)号：WO1998020314A2

公开(公告)日：1998-05-14

申请号：PCT/US1997020523

申请日：1997-10-31

Applicant: TA INSTRUMENTS, INC.

Inventor： TA INSTRUMENTS, INC. ,  DANLEY, Robert, L. ,  READER, John, R., Jr. ,  SCHAEFER, John, W.

IPC: G01K00/00

CPC classification number: G01N25/482 ,  G01K17/00 ,  G01N25/4833 ,  G01N25/4866

Abstract: A Differential Scanning Calorimeter (DSC) which has constant calorimetric sensitivity over its entire range of operating temperatures from -200 DEG C to 540 DEG C. The DSC sensor consists of a pair of thin-film Resistance Temperature Detectors (RTDs) which are used to sense the temperature of a sample and the temperature difference between the sample and an inert reference. The RTDs are supplied with an excitation current which varies according to the temperature of the reference to achieve constant calorimetric sensitivity, independent of the operating temperature.

Abstract translation: 差示扫描量热计（DSC），其在-200℃至540℃的整个操作温度范围内具有恒定的量热灵敏度。DSC传感器由一对薄膜电阻温度检测器（RTD）组成，用于 感测样品的温度和样品与惰性参比之间的温度差。 RTD提供的激励电流根据参考温度而变化，以实现恒定的量热灵敏度，与工作温度无关。

公开(公告)号：WO1998016818A1

公开(公告)日：1998-04-23

申请号：PCT/US1997015839

申请日：1997-10-07

Applicant: MICROCAL INCORPORATED

Inventor： MICROCAL INCORPORATED ,  PLOTNIKOV, Valerian, V. ,  BRANDTS, John, F. ,  BRANDTS, Michael, J.

IPC: G01N25/20

CPC classification number: G01N25/4866

Abstract: A differential calorimeter includes a reference cell (1), a sample cell (2), a thermal shield (9) surrounding the reference cell (1) and the sample cell (2), a heating device (3, 4) thermally coupled to the thermal shield (9), a temperature sensor (14) for monitoring a temperature of the thermal shield (9), a temperature sensor (12) for monitoring a temperature differential between the thermal shield (9) and the cells (1, 2), and a control system (6). The control system (6) has an output line connected to the heating device (3, 4), input lines to receive signals from the temperature sensors (12, 13), and is configured to generate on its output line an output signal which is a function of both the input signals received on its input lines.

Abstract translation: 差示热量计包括参考单元（1），样品池（2），围绕参考单元（1）和样品池（2）的热屏蔽（9），加热装置（3,4），热耦合到 热屏蔽（9），用于监测热屏蔽（9）的温度的温度传感器（14），用于监测热屏蔽（9）和电池（1,2）之间的温度差的温度传感器（12） ）和控制系统（6）。 控制系统（6）具有连接到加热装置（3,4）的输出线，用于接收来自温度传感器（12,13）的信号的输入线，并且被配置为在其输出线上产生输出信号 在其输入线上接收的输入信号的功能。

公开(公告)号：WO1995033200A1

公开(公告)日：1995-12-07

申请号：PCT/US1995006465

申请日：1995-05-22

Applicant: PERKIN-ELMER CORPORATION

Inventor： PERKIN-ELMER CORPORATION ,  SCHAWE, Juergen ,  MARGULIES, Marcel

IPC: G01N25/00

CPC classification number: G01K17/00 ,  G01N25/4833 ,  G01N25/4866

Abstract: The invention is directed to a differential analysis method and apparatus (10) wherein a sample (58) and a reference (56) are subjected to an externally applied disturbance, such as a temperature change, in accord with a prescribed function comprising the sum of a linearly changing part and a periodically changing part, and the measured differential signal is processed into real and imaginary components relating, respectively, to the energy storage and energy loss portions of the signal.

Abstract translation: 本发明涉及一种差分分析方法和装置（10），其中样品（58）和参考物（56）根据规定的功能进行外部施加的干扰，例如温度变化，该规定的功能包括 线性变化部分和周期性变化部分，并且所测量的差分信号被分别与信号的能量存储和能量损失部分相关联的实分量和虚分量进行处理。

公开(公告)号：WO2017003762A1

公开(公告)日：2017-01-05

申请号：PCT/US2016/038517

申请日：2016-06-21

Applicant: DOW GLOBAL TECHNOLOGIES LLC

Inventor： WU, Xiaosong ,  WEEKS, Ron ,  WICKHAM, Rennisha

IPC: C08K3/36

CPC classification number: C08K3/013 ,  C08K3/36 ,  C08L23/14 ,  C08L23/16 ,  C09D123/14 ,  E04F15/105 ,  G01N25/4866 ,  C08L23/10

Abstract: Embodiments of this invention relate to a composition composed of at least (A) a propylene-based polymer, and (B) a filler dispersed within the propylene-based polymer, which can be used as a wear layer on a resilient flooring or other substrate, among other uses.

Abstract translation: 本发明的实施方案涉及由至少（A）丙烯类聚合物和（B）分散在丙烯类聚合物内的填料组成的组合物，其可以用作弹性地板或其它基材上的耐磨层 ，其他用途。

公开(公告)号：WO2016203410A1

公开(公告)日：2016-12-22

申请号：PCT/IB2016/053556

申请日：2016-06-16

Applicant: BIOCON LIMITED

Inventor： PALLE, Venkata, Raghavendracharyulu ,  BHAT, Ramakrishna, Parameshwar ,  KALIAPPAN, Mariappan ,  BABU, Jithendra, R. ,  SHANMUGHASAMY, Rajmahendra

IPC: C07C253/14 ,  C07C255/23

CPC classification number: C07C255/23 ,  C07C253/00 ,  C07C253/14 ,  C07D261/08 ,  G01N23/20075 ,  G01N25/4866 ,  G01R33/46

Abstract: The present invention provides a process for the preparation of Teriflunomide (Formula-I). The present invention describes the synthesis of Teriflunomide without isolating the intermediate Leflunomide. Teriflunomide is prepared from 5-Methyl isoxazole-4-carboxylic acid by converting to its acid chloride and coupling with 4-trifluoromethyl aniline to obtain Leflunomide (which is not isolated) followed by ring opening reaction using aq. Sodium Hydroxide to form Teriflunomide. In other words, the process is telescoped from 5- methylisoxazole-4-carbonyl chloride.

Abstract translation: 本发明提供了制备特菲立姆（通式I）的方法。 本发明描述了不分离中间性来氟米特的特菲立姆的合成。 通过转化为其酰氯并与4-三氟甲基苯胺偶联，从5-甲基异恶唑-4-羧酸制备特里伦铵，得到来氟米特（其未分离），然后使用水杨酸开环反应。 氢氧化钠形成特立氟铵。 换句话说，该方法由5-甲基异恶唑-4-碳酰氯进行伸缩。

公开(公告)号：WO2016163371A1

公开(公告)日：2016-10-13

申请号：PCT/JP2016/061174

申请日：2016-04-05

Applicant: 日本ゼオン株式会社

Inventor： 藤井　健作 ,  寳川　卓士 ,  小松原　拓也 ,  清水　康寛

IPC: C08F232/00 ,  C08G61/08

CPC classification number: C08G61/08 ,  C07C13/64 ,  C08F8/04 ,  C08F232/00 ,  C08F232/04 ,  G01N25/4866 ,  G01R33/46

Abstract: 　本発明は、１又は２種以上の環状オレフィン単量体と、１又は２種以上の鎖状オレフィン単量体とを共重合して得られる共重合体、又は、２種以上の環状オレフィン単量体を共重合して得られる共重合体であって、ガラス転移温度（Ｔｇ）が１００℃以上、屈折率が１．５４５以上、かつ、アッベ数が５０以上であることを特徴とする共重合体、及び、下記式（Ｉ）で示される単量体を単独で開環重合して得られる単独開環重合体、前記式（Ｉ）で示される単量体と、前記式（Ｉ）で示される単量体と開環共重合可能な単量体とを開環共重合して得られる開環共重合体、及びこれらの重合体の水素化物から選ばれる重合体（Ｂ）、前記共重合体（Ａ）又は重合体（Ｂ）を含有する成形材料、及びこの成形材料を成形して得られる樹脂成形体である。

Abstract translation: 本发明提供：通过使一种或多种环烯烃单体和一种或多种链烯烃单体共聚合或通过共聚两种或更多种环状烯烃单体而获得的共聚物，其特征在于具有玻璃化转变 温度（Tg）为100℃以上，折射率为1.545以上，阿贝数为50以上。 选自通过由式（I）表示的单体开环聚合而得到的开环均聚物本身的聚合物（B），通过式（I）表示的单体的开环共聚获得的开环共聚物 （I）和与式（I）表示的单体开环共聚的单体和这些聚合物的氢化产物; 含有共聚物（A）或聚合物（B）的成型材料; 以及通过模制该成型材料而获得的树脂成形体。