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公开(公告)号:WO2022103908A1
公开(公告)日:2022-05-19
申请号:PCT/US2021/058886
申请日:2021-11-11
Applicant: DOW SILICONES CORPORATION
Inventor: FROESCHLE, Kalyn , NATTERODT, Jens , FREUDENBERGER, Rainer , PEITZ, Thomas , ROMAIN, Roger , SIEBMANN, Ruediger
IPC: C08J3/20 , C08J3/205 , B29B7/74 , B29B7/88 , B29B7/84 , B29C48/40 , B29B7/007 , B29B7/325 , B29B7/48 , B29B7/7461 , B29B7/7495 , B29B7/826 , B29B7/845 , B29B7/86 , B29B7/90 , C08J2383/07 , C08J3/201 , C08J3/203
Abstract: A process for the continuous preparation of silicone rubber base compositions using an in situ silica treatment and twin-screw extruder technology comprising (a) introducing a hydrophobing treating agent (C), a diorganopolysiloxane containing at least two alkenyl and/or alkynyl groups, and optionally water into a first static mixer and then introducing it in a first twin-screw extruder; (b) adding reinforcing silica filler at a temperature of 20-80°C and providing at least one vent to the atmosphere up and/or downstream of the reinforcing silica filler (B) entry port to allow gases present to escape; (c) mixing in the extruder; (d) further mixing in a residence zone; (e) vacuum stripping at a temperature of at least 100°C; and (f) introducing component (C) either into the twin-screw extruder between steps (c) and (d) and/or during step (d) to dilute and further hydrophobically treat silica. Also resulting compositions produced therefrom.
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公开(公告)号:WO2019024432A1
公开(公告)日:2019-02-07
申请号:PCT/CN2018/000279
申请日:2018-07-31
Applicant: DOW SILICONES CORPORATION , GAO, Jianjun , FREUDENBERGER, Rainer , HEIDENFELDER, Franz , SIEBMANN, Ruediger , FROESCHLE, Kalyn , CLEMENTS, Travis L.
Inventor: GAO, Jianjun , FREUDENBERGER, Rainer , HEIDENFELDER, Franz , SIEBMANN, Ruediger , FROESCHLE, Kalyn , CLEMENTS, Travis L.
Abstract: Provided are an assembly and process for the continuous or semi-continuous preparation of addition-crosslinking liquid silicone rubbers and to liquid silicone rubber compositions made therefrom. Also disclosed are articles made from the liquid silicone rubber compositions.
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公开(公告)号:WO2019023841A1
公开(公告)日:2019-02-07
申请号:PCT/CN2017/095152
申请日:2017-07-31
Applicant: DOW SILICONES CORPORATION , GAO, Jianjun , FREUDENBERGER, Rainer , HEIDENFELDER, Franz , SIEBMANN, Ruediger , FROESCHLE, Kalyn , CLEMENTS, Travis L.
Inventor: GAO, Jianjun , FREUDENBERGER, Rainer , HEIDENFELDER, Franz , SIEBMANN, Ruediger , FROESCHLE, Kalyn , CLEMENTS, Travis L.
Abstract: Provided are an assembly and a process for the continuous preparation of addition-crosslinking liquid silicone rubbers and liquid silicone rubber compositions made therefrom. Also disclosed are articles made from the liquid silicone rubber compositions.
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