Invention Grant
- Patent Title: Process for the preparation of 2,3,3,3-tetrafluoropropene
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Application No.: US15095911Application Date: 2016-04-11
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Publication No.: US10053404B2Publication Date: 2018-08-21
- Inventor: Dominique Deur-Bert , Bertrand Collier , Laurent Wendlinger
- Applicant: Arkema France
- Applicant Address: FR Colombes
- Assignee: Arkema France
- Current Assignee: Arkema France
- Current Assignee Address: FR Colombes
- Agency: NK Patent Law, PLLC
- Main IPC: C07C17/25
- IPC: C07C17/25 ; C07C17/20 ; C07C21/18 ; C07C17/383 ; C01B7/19 ; B01J37/12 ; B01J37/24 ; B01J37/26 ; B01J23/26 ; B01J23/86 ; B01J27/132 ; C07C17/38

Abstract:
The present invention provides a process for preparing 2,3,3,3-tetrafluoropropene from 1,1,1,2,3-pentachloropropane and/or 1,1,2,2,3-pentachloropropane, comprising the following steps: (a) catalytic reaction of 1,1,1,2,3-pentachloropropane and/or 1,1,2,2,3-pentachloropropane with HF into a reaction mixture comprising HCl, 2-chloro-3,3,3-trifluoropropene, 2,3,3,3-tetrafluoropropene, unreacted HF, and optionally 1,1,1,2,2-pentafluoropropane; (b) separating the reaction mixture into a first stream comprising HCl and 2,3,3,3-tetrafluoropropene and a second stream comprising HF, 2-chloro-3,3,3-trifluoropropene and optionally 1,1,1,2,2-pentafluoropropane; (c) catalytic reaction of the second stream into a reaction mixture comprising 2,3,3,3-tetrafluoropropene, HCl, unreacted 2-chloro-3,3,3-trifluoropropene, unreacted HF and optionally 1,1,1,2,2-pentafluoropropane and (d) feeding the reaction mixture of step (c) directly without separation to step (a).
Public/Granted literature
- US20160221901A1 PROCESS FOR THE PREPARATION OF 2,3,3,3-TETRAFLUOROPROPENE Public/Granted day:2016-08-04
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