Invention Grant
- Patent Title: Process of making polyimide micronized particles, particles formed therefrom, and articles prepared therefrom
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Application No.: US15737649Application Date: 2016-06-29
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Publication No.: US10377863B2Publication Date: 2019-08-13
- Inventor: Viswanathan Kalyanaraman , Hareesh Shamrao Deshpande , Ekrem Mehmet Morali
- Applicant: SABIC Global Technologies B.V.
- Applicant Address: NL Bergen op Zoom
- Assignee: SABIC GLOBAL TECHNOLOGIES B.V.
- Current Assignee: SABIC GLOBAL TECHNOLOGIES B.V.
- Current Assignee Address: NL Bergen op Zoom
- Agency: Cantor Colburn LLP
- Priority: IN1949/DEL/2015 20150630
- International Application: PCT/US2016/039994 WO 20160629
- International Announcement: WO2017/004140 WO 20170105
- Main IPC: C08J3/14
- IPC: C08J3/14 ; C08J3/07 ; C09D179/08 ; B01D21/26 ; B01D33/64 ; C08G73/10 ; C09J179/08

Abstract:
A method of manufacturing polyimide particles includes combining a polyimide solution including a polyimide and an organic solvent with an aqueous solution including water in the presence of an emulsifying surfactant at a shear rate from 1,000 to 3,000 revolutions per minute to form an emulsion. The method further includes removing the organic solvent to form an aqueous polymer dispersion including polyimide particles, and recovering the polyimide particles. The polyimide particles have a spherical morphology and a volume based D10 diameter from 3 to 50 micrometers, a volume based D90 diameter from 3 to 80 micrometers, and a volume based D100 diameter from 3 to 100 micrometers.
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