- 专利标题: Continuous process for making polybutylene terephthalate using purified terephthalic acid and 1,4-butane diol
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申请号: US16298235申请日: 2019-03-11
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公开(公告)号: US10899875B2公开(公告)日: 2021-01-26
- 发明人: Husnu Alp Alidedeoglu , Prashant Kumar , Brian Bougher , Cornelis Adrianus Maria van Gool , Sasi Sethumadhavan Kannamkumarath , Bing Zhou
- 申请人: SABIC Global Technologies B.V.
- 申请人地址: NL Bergen op Zoom
- 专利权人: SABIC Global Technologies B.V.
- 当前专利权人: SABIC Global Technologies B.V.
- 当前专利权人地址: NL Bergen op Zoom
- 代理机构: Cantor Colburn LLP
- 主分类号: C08G63/183
- IPC分类号: C08G63/183 ; C08G63/78
摘要:
A device for making polybutylene terephthalate includes (1) a slurry paste vessel; (2) a tower reactor to which a mixture of 1,4-butane diol and terephthalic acid from vessel (1) is supplied, the tower reactor having a plurality of reactor zones wherein the lower third of the tower reactor is in the form of a hydrocyclone with attached heat exchanger, and the hydrocyclone has a supply line from vessel (1), the hydrocyclone being connected to the top side of the tower reactor; (3) a first continuously stirred tank reactor to which the product from tower reactor (2) is supplied; (4) an optional second continuously stirred tank reactor to which the product from (3) is supplied; (5) a dual shaft ring reactor to which the product from stirred tank reactor (3) or (4), is supplied; and (6) a pelletizer where the product from dual shaft ring reactor (5) is continuously fed and pelletized.
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