Invention Grant
- Patent Title: Production method for hexafluoro-1,3-butadiene
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Application No.: US16611879Application Date: 2018-04-25
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Publication No.: US11192838B2Publication Date: 2021-12-07
- Inventor: Yohsuke Fukuchi , Atsushi Nakamura , Nozomi Inoue , Mitsuhiro Hino , Tomoki Sekiguchi
- Applicant: SHOWA DENKO K.K.
- Applicant Address: JP Tokyo
- Assignee: SHOWA DENKO K.K.
- Current Assignee: SHOWA DENKO K.K.
- Current Assignee Address: JP Tokyo
- Agency: Sughrue Mion, PLLC
- Priority: JPJP2017-101063 20170522
- International Application: PCT/JP2018/016881 WO 20180425
- International Announcement: WO2018/216426 WO 20181129
- Main IPC: C07C17/23
- IPC: C07C17/23 ; C07C17/383 ; C07C21/18 ; C07C21/20 ; B01J23/06

Abstract:
Provided is a method that is for producing hexafluoro-1,3-butadiene, discharges small amounts of industrial wastes, and is industrially applicable. The method for producing hexafluoro-1,3-butadiene includes a reaction step of reacting a halogenated butane represented by chemical formula, CF2X1-CFX2-CFX3-CF2X4 (X1, X2, X3, and X4 are each independently a halogen atom other than a fluorine atom) in an organic solvent in the presence of zinc to eliminate the halogen atoms, X1, X2, X3, and X4, other than the fluorine atoms to generate hexafluoro-1,3-butadiene, giving a reaction product containing the hexafluoro-1,3-butadiene, and an aftertreatment step of separating the hexafluoro-1,3-butadiene from the reaction product produced in the reaction step, then adding water to a reaction product residue after the separating, and removing the organic solvent, giving an aqueous solution of zinc halide.
Public/Granted literature
- US20210163382A1 PRODUCTION METHOD FOR HEXAFLUORO-1,3-BUTADIENE Public/Granted day:2021-06-03
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