Invention Grant
- Patent Title: Method for producing transition alumina catalyst monoliths
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Application No.: US15733841Application Date: 2019-05-28
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Publication No.: US11547981B2Publication Date: 2023-01-10
- Inventor: Matthias Georg Schwab , Esther Groeneveld , Peter Berben , Harry Bouwman , Willem Dijkstra , Bart Michielsen , Jasper Lefevere
- Applicant: BASF SE
- Applicant Address: DE Ludwigshafen am Rhein
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen am Rhein
- Agency: Faegre Drinker Biddle & Reath LLP
- Priority: EP18174925 20180529
- International Application: PCT/EP2019/063815 WO 20190528
- International Announcement: WO2019/229061 WO 20191205
- Main IPC: B01J21/04
- IPC: B01J21/04 ; B33Y10/00 ; B29C64/106 ; B01J35/00 ; B01J35/04 ; B01J35/06 ; B01J35/10 ; B01J37/00 ; B01J37/04 ; B01J37/08 ; B28B1/00 ; B28B11/24 ; C07C1/24 ; C07C5/27 ; B33Y70/00 ; B33Y80/00 ; B29K509/02

Abstract:
A method for producing a three-dimensional porous transition alumina catalyst monolith of stacked catalyst fibers, comprising:
a) Preparing a paste in a liquid diluent of hydroxide precursor particles and/or oxyhydroxide precursor particles of transition alumina particles, all particles in the suspension having a number average particle size in the range of from 0.05 to 700 μm,
b) extruding the paste nozzle(s) to form fibers, and depositing the extruded fibers to form a three-dimensional porous catalyst monolith precursor,
c) drying the precursor to remove the liquid diluent,
d) performing a temperature treatment of the dried porous catalyst monolith precursor to form the transition alumina catalyst monolith,
wherein no temperature treatment of the porous catalyst monolith precursor or porous catalyst monolith at temperatures above 1000° C. is performed and wherein no further catalytically active metals, metal oxides or metal compounds are applied to the surface.
a) Preparing a paste in a liquid diluent of hydroxide precursor particles and/or oxyhydroxide precursor particles of transition alumina particles, all particles in the suspension having a number average particle size in the range of from 0.05 to 700 μm,
b) extruding the paste nozzle(s) to form fibers, and depositing the extruded fibers to form a three-dimensional porous catalyst monolith precursor,
c) drying the precursor to remove the liquid diluent,
d) performing a temperature treatment of the dried porous catalyst monolith precursor to form the transition alumina catalyst monolith,
wherein no temperature treatment of the porous catalyst monolith precursor or porous catalyst monolith at temperatures above 1000° C. is performed and wherein no further catalytically active metals, metal oxides or metal compounds are applied to the surface.
Public/Granted literature
- US20210213423A1 METHOD FOR PRODUCING TRANSITION ALUMINA CATALYST MONOLITHS Public/Granted day:2021-07-15
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