- 专利标题: Method for producing ceramic sintered body, ceramic sintered body, and light emitting device
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申请号: US17643883申请日: 2021-12-13
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公开(公告)号: US11976228B2公开(公告)日: 2024-05-07
- 发明人: Hirofumi Ooguri , Shoji Hosokawa
- 申请人: NICHIA CORPORATION
- 申请人地址: JP Anan
- 专利权人: NICHIA CORPORATION
- 当前专利权人: NICHIA CORPORATION
- 当前专利权人地址: JP Anan
- 代理机构: Hunton Andrews Kurth LLP
- 优先权: JP 18225511 2018.11.30
- 分案原申请号: US16695702 2019.11.26
- 主分类号: C09K11/77
- IPC分类号: C09K11/77 ; C09K11/08 ; H01L33/50
摘要:
Provided are a method for producing a ceramic sintered body having improved light emission intensity, a ceramic sintered body, and a light emitting device. The method for producing a ceramic sintered body comprises preparing a molded body that contains a nitride fluorescent material having a composition containing: at least one alkaline earth metal element M1 selected from the group consisting of Ba, Sr, Ca, and Mg; at least one metal element M2 selected from the group consisting of Eu, Ce, Tb, and Mn; Si; and N, wherein a total molar ratio of the alkaline earth metal element M1 and the metal element M2 in 1 mol of the composition is 2, a molar ratio of the metal element M2 is a product of 2 and a parameter y and wherein y is in a range of 0.001 or more and less than 0.5, a molar ratio of Si is 5, and a molar ratio of N is 8, and wherein the nitride fluorescent material has a crystallite size, as calculated by X-ray diffraction measurement using the Halder-Wagner method, of 550 Å or less, and calcining the molded body at a temperature in a range of 1,600° C. or more and 2,200° C. or less to obtain a sintered body.
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