- 专利标题: Method for synthesizing mesoporous nano-sized zeolite beta
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申请号: US18059712申请日: 2022-11-29
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公开(公告)号: US12017207B2公开(公告)日: 2024-06-25
- 发明人: Lianhui Ding , Khalid Otaibi , Faisal Alotaibi
- 申请人: Saudi Arabian Oil Company
- 申请人地址: SA Dhahran
- 专利权人: Saudi Arabian Oil Company
- 当前专利权人: Saudi Arabian Oil Company
- 当前专利权人地址: SA Dhahran
- 代理机构: DINSMORE & SHOHL LLP
- 主分类号: B01J29/70
- IPC分类号: B01J29/70 ; B01J35/23 ; B01J35/61 ; B01J35/63 ; B01J35/64 ; B01J37/00 ; B01J37/02 ; B01J37/03 ; B01J37/04 ; B01J37/06 ; C01B39/48
摘要:
Methods for synthesizing a mesoporous nano-sized zeolite beta are described. The method may include mixing an aqueous base solution with hexadecyltrimethylammonium bromide (CTAB) to form a first solution; adding nano-sized zeolite particles having a particle size of less than or equal to 100 nm to the first solution to form a second solution. The nano-sized zeolite particles include a microporous framework with a plurality of micropores having diameters of less than or equal to 2 nm and a BEA framework type. The method may further include transferring the second solution to an autoclave operated at 25° C. to 200° C. for 3 to 24 hours to form a colloid; drying the colloid at 100° C. to 200° C. for 8 to 36 hours without washing the colloid to form a zeolite precursor; and calcining the zeolite precursor at 250° C. to 600° C. for 1 to 8 hours to form the mesoporous nano-sized zeolite beta.
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