Invention Grant
- Patent Title: Method for synthesizing mesoporous nano-sized zeolite beta
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Application No.: US18059712Application Date: 2022-11-29
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Publication No.: US12017207B2Publication Date: 2024-06-25
- Inventor: Lianhui Ding , Khalid Otaibi , Faisal Alotaibi
- Applicant: Saudi Arabian Oil Company
- Applicant Address: SA Dhahran
- Assignee: Saudi Arabian Oil Company
- Current Assignee: Saudi Arabian Oil Company
- Current Assignee Address: SA Dhahran
- Agency: DINSMORE & SHOHL LLP
- Main IPC: B01J29/70
- IPC: B01J29/70 ; B01J35/23 ; B01J35/61 ; B01J35/63 ; B01J35/64 ; B01J37/00 ; B01J37/02 ; B01J37/03 ; B01J37/04 ; B01J37/06 ; C01B39/48

Abstract:
Methods for synthesizing a mesoporous nano-sized zeolite beta are described. The method may include mixing an aqueous base solution with hexadecyltrimethylammonium bromide (CTAB) to form a first solution; adding nano-sized zeolite particles having a particle size of less than or equal to 100 nm to the first solution to form a second solution. The nano-sized zeolite particles include a microporous framework with a plurality of micropores having diameters of less than or equal to 2 nm and a BEA framework type. The method may further include transferring the second solution to an autoclave operated at 25° C. to 200° C. for 3 to 24 hours to form a colloid; drying the colloid at 100° C. to 200° C. for 8 to 36 hours without washing the colloid to form a zeolite precursor; and calcining the zeolite precursor at 250° C. to 600° C. for 1 to 8 hours to form the mesoporous nano-sized zeolite beta.
Public/Granted literature
- US20240173706A1 METHOD FOR SYNTHESIZING MESOPOROUS NANO-SIZED ZEOLITE BETA Public/Granted day:2024-05-30
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