- 专利标题: Methods for manufacturing silicon carbide single crystal ingot and silicon carbide single crystal wafer
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申请号: US18362117申请日: 2023-07-31
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公开(公告)号: US12071709B2公开(公告)日: 2024-08-27
- 发明人: Isaho Kamata , Hidekazu Tsuchida , Norihiro Hoshino , Yuichiro Tokuda , Takeshi Okamoto
- 申请人: DENSO CORPORATION
- 申请人地址: JP Kariya
- 专利权人: DENSO CORPORATION
- 当前专利权人: DENSO CORPORATION
- 当前专利权人地址: JP Kariya
- 代理机构: Posz Law Group, PLC
- 优先权: JP 19173463 2019.09.24
- 分案原申请号: US17027840 2020.09.22
- 主分类号: C30B25/00
- IPC分类号: C30B25/00 ; C30B25/02 ; C30B25/10 ; C30B29/36 ; C30B33/00
摘要:
A raw material gas is supplied to a space in which a silicon carbide seed crystal is placed. A silicon carbide single crystal is grown on the seed crystal by keeping a monosilane partial pressure at 4 kPa or more and heating the space to a temperature of 2400° C. to 2700° C. The temperature of the space and supply of the raw material gas are controlled such that a temperature gradient of a growth crystal surface of the silicon carbide single crystal in a radial direction is 0.1° C./mm or less, and a radius of curvature of the growth crystal surface is 4.5 m or more, thereby producing a silicon carbide single crystal ingot having a growth length of 3 mm or more and an internal stress of 10 MPa or less. The ingot is then cut into a silicon carbide single crystal wafer.
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