- 专利标题: METHOD FOR PRODUCING ACETIC ACID
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申请号: US15540177申请日: 2017-05-25
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公开(公告)号: US20180118649A1公开(公告)日: 2018-05-03
- 发明人: Masahiko SHIMIZU
- 申请人: DAICEL CORPORATION
- 申请人地址: JP Osaka-shi, Osaka
- 专利权人: DAICEL CORPORATION
- 当前专利权人: DAICEL CORPORATION
- 当前专利权人地址: JP Osaka-shi, Osaka
- 优先权: JP2016-211922 20161028; JP2017-039388 20170302
- 国际申请: PCT/JP2017/019572 WO 20170525
- 主分类号: C07C51/12
- IPC分类号: C07C51/12 ; C07C51/44 ; B01D1/30 ; B01D53/14 ; B01D3/14
摘要:
Provided is a method for producing acetic acid, which suppresses catalyst precipitation and accumulation in an evaporator, can efficiently recycle catalysts to a reaction vessel, and can contribute to maintenance and improvement in acetic acid productivity and securing of safety operation. In the method, the evaporator has a catalyst precipitation and accumulation prevention structure: (a) structure where inclination angle θ of inside wall surface of an inverted truncated conical cylindrical connection portion is 5° to 85°; and/or (b) structure where a vortex breaker comprising a plate-like vortex breaker main body and a leg is disposed such that the vortex breaker main body covers right above the connection portion of an evaporator bottom part to a residual liquid stream recycle line, and linear velocity r of the residual liquid stream passing through a gap between the vortex breaker main body and the evaporator bottom part is larger than 10 m/h.
公开/授权文献
- US10266473B2 Method for producing acetic acid 公开/授权日:2019-04-23
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