发明授权
- 专利标题: Process for preparing 2,2-dichloroacetoacetyl chloride
- 专利标题(中): 制备2,2-二氯乙酰乙酰氯的方法
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申请号: US383935申请日: 1982-06-01
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公开(公告)号: US4404149A公开(公告)日: 1983-09-13
- 发明人: Jean-Claude Perlberger
- 申请人: Jean-Claude Perlberger
- 申请人地址: CHX Gampel
- 专利权人: Lonza Ltd.
- 当前专利权人: Lonza Ltd.
- 当前专利权人地址: CHX Gampel
- 优先权: CHX8549/80 19801119
- 主分类号: C07C59/347
- IPC分类号: C07C59/347 ; B01J27/00 ; C07B61/00 ; C07C51/00 ; C07C51/62 ; C07C53/16 ; C07C67/00
摘要:
2,2-Dichloroacetoacetyl chloride having the formula: ##STR1## Process for producing 2,2-dichloroacetoacetyl chloride wherein acetyl chloride is reacted by means of a Lewis acid as a catalyst with chlorine at a temperature of 30.degree. to 60.degree. C. The mole ratio of acetyl chloride to the catalyst is from 1:0.005 to 1:0.5 and the mole ratio of acetyl chloride to the chlorine is from 1:0.1 to 1:1.5. The most preferred catalysts are aluminum chloride and aluminum bromide.
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