发明授权
- 专利标题: Process for the production of highly concentrated pastes of .alpha.-sulfofatty acid alkyl ester alkali metal salts
- 专利标题(中): 生产高浓度糊精α-磺基脂肪酸烷基酯碱金属盐的方法
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申请号: US949511申请日: 1992-11-24
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公开(公告)号: US5382677A公开(公告)日: 1995-01-17
- 发明人: Dietmar Colignon , Erich Dorra , Guenter Panthel , Wolfgang Schmidt , Norbert Wrede
- 申请人: Dietmar Colignon , Erich Dorra , Guenter Panthel , Wolfgang Schmidt , Norbert Wrede
- 申请人地址: DEX Duesseldorf
- 专利权人: Henkel Kommanditgesellschaft auf Aktien
- 当前专利权人: Henkel Kommanditgesellschaft auf Aktien
- 当前专利权人地址: DEX Duesseldorf
- 优先权: DEX4017468 19900530
- 主分类号: B01F17/08
- IPC分类号: B01F17/08 ; C07C303/06 ; C07C303/32 ; C07C303/44 ; C07C309/17 ; C11D1/28
摘要:
In the production of highly concentrated pastes of .alpha.-sulfofatty acid alkyl ester alkali metal salts by reaction of fatty acid alkyl esters with gaseous SO.sub.3, subsequent after-reaction in liquid phase and neutralization with aqueous alkali hydroxide solutions, the sulfonation product and aqueous alkali metal hydroxide solution are introduced during neutralization into an aqueous phase initially containing at least 55% by weight washing-active substance at a pH value in the range from 2 to 8 and washing-active substance contents of 60 to 70% by weight are established.
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