发明授权
US5847178A Method for purifying 3-methacryloxypropyldimethylhalosilanes and 3-methacryloxypropylmethyldihalosilanes 失效
3-甲基丙烯酰氧基丙基二甲基硅烷和3-甲基丙烯酰氧基丙基甲基二卤代硅烷的纯化方法

  • 专利标题: Method for purifying 3-methacryloxypropyldimethylhalosilanes and 3-methacryloxypropylmethyldihalosilanes
  • 专利标题(中): 3-甲基丙烯酰氧基丙基二甲基硅烷和3-甲基丙烯酰氧基丙基甲基二卤代硅烷的纯化方法
  • 申请号: US982768
    申请日: 1997-12-02
  • 公开(公告)号: US5847178A
    公开(公告)日: 1998-12-08
  • 发明人: Tadashi Okawa
  • 申请人: Tadashi Okawa
  • 申请人地址: JPX Tokyo
  • 专利权人: Dow Corning Toray Silicone Co., Ltd.
  • 当前专利权人: Dow Corning Toray Silicone Co., Ltd.
  • 当前专利权人地址: JPX Tokyo
  • 优先权: JPX8-336332 19961202
  • 主分类号: C07F7/12
  • IPC分类号: C07F7/12 C07F7/20 C07F7/08
Method for purifying 3-methacryloxypropyldimethylhalosilanes and
3-methacryloxypropylmethyldihalosilanes
摘要:
A method for purifying 3-methacryloxypropyldimethylhalosilanes or 3-methacryloxypropyl methyldihalosilanes which is characterized by the fact that 1-methyl-2-methacryloxyethyldimethyl halosilanes or 1-methyl-2-methacryloxyethylmethyldihalosilanes contained in products or fractions consisting of 3-methacryloxypropyldimethylhalosilanes or 3-methacryloxypropylmethyl dihalosilanes produced by a hydrosilation reaction of allyl methacrylate with dimethylhalosilanes or methyldihalosilanes are decomposed by means of at least one copper compound selected from the group consisting of copper hydroxides, copper salts other than copper halides, and copper oxides, after which these compounds are subjected to fractional distillation.
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