Invention Grant
- Patent Title: Method for producing 3,3-dichloro-1,1,1-triflouroacetone
- Patent Title (中): 3,3-二氯-1,1,1-三氟丙酮的制备方法
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Application No.: US60180Application Date: 1998-04-15
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Publication No.: US5905174APublication Date: 1999-05-18
- Inventor: Masatomi Kanai , Takashi Sakaya , Mineo Watanabe , Yoshihiko Goto , Ryo Nadano
- Applicant: Masatomi Kanai , Takashi Sakaya , Mineo Watanabe , Yoshihiko Goto , Ryo Nadano
- Applicant Address: JPX Yamaguchi
- Assignee: Central Glass Company, Limited
- Current Assignee: Central Glass Company, Limited
- Current Assignee Address: JPX Yamaguchi
- Priority: JPX9-097623 19970415; JPX9-097624 19970415; JPX9-137376 19970528
- Main IPC: B01J27/08
- IPC: B01J27/08 ; B01J27/125 ; C07C45/63 ; C07C45/82 ; C07C45/83 ; C07C45/00
Abstract:
The invention relates to a method for producing 3,3-dichloro-1,1,1-trifluoroacetone. This method includes a step of fluorinating pentachloroacetone by hydrogen fluoride in the presence of a fluorination catalyst. This fluorination may be conducted in a liquid phase in the presence of an antimony compound as the fluorination catalyst. Alternatively, the fluorination may be conducted in a gas phase in the presence of a fluorination catalyst which may be a fluorinated alumina or at least one compound of at least one metal selected from Al, Cr, Mn, Ni, and Co. The method is suited to an industrial scale production of 3,3-dichloro-1,1,1-trifluoroacetone. The invention further relates to another method for producing 3,3-dichloro-1,1,1-trifluoroacetone. This method includes a step of purifying a crude 3,3-dichloro-1,1,1-trifluoroacetone by a distillation in the presence of water, thereby to produce 3,3-dichloro-1,1,1-trifluoroacetone which is substantially free of organic matters other than 3,3-dichloro-1,1,1-trifluoroacetone. This crude 3,3-dichloro-1,1,1-trifluoroacetone may be the reaction products of the fluorination of pentachloroacetone in a gas phase. Due to the provision of the another method, 3,3-dichloro-1,1,1-trifluoroacetone can be produced with high yield.
Public/Granted literature
- USD388569S Cleaning tool Public/Granted day:1997-12-30
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