发明授权
US06914032B2 Method of producing tungsten-copper based composite powder and sintered alloys for heat-sink using said composite powder 失效
使用所述复合粉末制造用于散热器的钨铜基复合粉末和烧结合金的方法

Method of producing tungsten-copper based composite powder and sintered alloys for heat-sink using said composite powder
摘要:
The present invention relates to a method of producing W—Cu based composite powder, which is used in heat-sink materials for high-power integrated circuits, electric contact materials, etc, and to a method of producing a W—Cu based sintered alloy by using the composite powder. The method of producing tungsten-copper based composite powder includes first preparing composite oxide powder by dissolving ammonium metatungstate, [(NH4)6(H2W12O40).4H2O], as water-soluble tungsten salt, and copper nitrate or copper acetate in water to the desirable composition, followed by spray-drying and calcining; then preparing a tungsten oxide powder by separately calcining a tungsten-containing salt, such as ammonium paratungstate, (NH4)10(H10W12O46); forming ultra-fine tungsten-copper based composite oxide powder by mixing 20˜75 wt % of the composite oxide powder and 80˜25 wt % of the tungsten oxide powder to the desirable composition, followed by ball-milling; and reducing the ultra-fine tungsten-copper based composite oxide powder at temperature of 650˜1,050° C. If the composite powder is molded into a certain size and sintered thereafter in temperature of 1,110˜1,450° C., a W—Cu based sintered alloy of superior thermal and electric conductivities can be obtained thereby.
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