发明授权
- 专利标题: Process for preparing molecular sieves via continuous addition of nutrients
- 专利标题(中): 通过连续添加营养素制备分子筛的方法
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申请号: US11199044申请日: 2005-08-08
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公开(公告)号: US07112316B1公开(公告)日: 2006-09-26
- 发明人: Brian S. Konrad , Julio C. Marte , Beckay J. Mezza , Stephen T. Wilson , Lance L. Jacobsen , David A. Lesch
- 申请人: Brian S. Konrad , Julio C. Marte , Beckay J. Mezza , Stephen T. Wilson , Lance L. Jacobsen , David A. Lesch
- 申请人地址: US IL Des Plaines
- 专利权人: UOP LLC
- 当前专利权人: UOP LLC
- 当前专利权人地址: US IL Des Plaines
- 代理商 John G. Tolomei; Frank S. Molinaro
- 主分类号: C01B39/02
- IPC分类号: C01B39/02 ; C01B37/08
摘要:
A process for synthesizing a variety of molecular sieves has been developed. The process involves forming a reaction mixture comprising reactive sources of the framework elements plus at least one templating agent, reacting the mixture to at least partially crystallize the molecular sieve and provide a slurry of seed crystals and adding to it nutrients (sources) of the framework elements, e.g. aluminum and silicon in order to grow the seed crystals. The rate of addition of the nutrients is controlled such that it is substantially the same as the crystal growth rate and such that there is substantially no nucleation of new crystals. The seed crystals may be the same or different than the nutrients being added, thus allowing for a layered molecular sieve. When the crystals have reached a desired size, they are isolated by conventional techniques.
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