发明授权
US07255834B2 Method and devices for improving the dynamic flash combustion reaction connected with gas chromatography for the elemental analysis of C H N S O 有权
用于改进与气相色谱相连的动态闪燃反应的方法和装置,用于C H N S O的元素分析

  • 专利标题: Method and devices for improving the dynamic flash combustion reaction connected with gas chromatography for the elemental analysis of C H N S O
  • 专利标题(中): 用于改进与气相色谱相连的动态闪燃反应的方法和装置,用于C H N S O的元素分析
  • 申请号: US10302306
    申请日: 2002-11-22
  • 公开(公告)号: US07255834B2
    公开(公告)日: 2007-08-14
  • 发明人: Stefano Boursier NiuttaLeonardo Sisti
  • 申请人: Stefano Boursier NiuttaLeonardo Sisti
  • 申请人地址: IT Milan
  • 专利权人: Eurovector S.p.A.
  • 当前专利权人: Eurovector S.p.A.
  • 当前专利权人地址: IT Milan
  • 代理机构: Shoemaker and Mattare
  • 优先权: ITBS98A000068 19980923
  • 主分类号: B32B5/02
  • IPC分类号: B32B5/02
Method and devices for improving the dynamic flash combustion reaction connected with gas chromatography for the elemental analysis of C H N S O
摘要:
A method and device are provided for dynamic flash combustion reaction connected with gas chromatography for the elemental analysis of C H N S O in an automatic elemental analyzer. A combustion reactor is provided with a sampling device and an oxygen feed line. Controlled volumes of oxygen are admitted with the oxygen feed line into the combustion reactor depending on the sample for the complete combustion thereof. A pneumatic circuit is provided, in which the oxygen feed line converges and the pneumatic circuit creates a continuous flow of a carrier gas that is able to carry the oxygen to the reactor and the gases of the combustion through the reactor, then through a gas chromatographic analyzer, and after their separation, into a thermal conductivity detector. An electronic apparatus with a data processor is provided for controlling the process systems. The difference in the pressure of the gas upstream and downstream of a restrictor or restriction is determined. The electronic pressure regulator or flow regulator of the reference carrier gas and at least one carrier gas outlet valve, which is also used as purging, is inserted on this carrier gas reference line.
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