公开(公告)号：US20030077835A1

公开(公告)日：2003-04-24

申请号：US10302306

申请日：2002-11-22

申请人： Eurovector S.p.a.

发明人： Stefano Boursier Niutta ,  Leonardo Sisti

IPC分类号： G01N031/12

CPC分类号： G01N31/12 ,  G01N30/12 ,  G01N2030/125 ,  Y10T436/12

摘要： A method and device are provided for dynamic flash combustion reaction connected with gas chromatography for the elemental analysis of C H N S O in an automatic elemental analyzer. A combustion reactor is provided with a sampling device and an oxygen feed line. Controlled volumes of oxygen are admitted with the oxygen feed line into the combustion reactor depending on the sample for the complete combustion thereof. A pneumatic circuit is provided, in which the oxygen feed line converges and the pneumatic circuit creates a continuous flow of a carrier gas that is able to carry the oxygen to the reactor and the gases of the combustion through the reactor, then through a gas chromatographic analyzer, and after their separation, into a thermal conductivity detector. An electronic apparatus with a data processor is provided for controlling the process systems. The difference in the pressure of the gas upstream and downstream of a restrictor or restriction is determined. The electronic pressure regulator or flow regulator of the reference carrier gas and at least one carrier gas outlet valve, which is also used as purging, is inserted on this carrier gas reference line.

摘要翻译： 提供了一种与气相色谱相连的动态闪燃反应方法和装置，用于在自动元素分析仪中对C H N S O进行元素分析。 燃烧反应器设置有取样装置和氧气供给管线。 根据用于其完全燃烧的样品，氧气的受控体积被氧气进入管线进入燃烧反应器。 提供了一种气动回路，其中氧气供给管线汇合，气动回路产生能够将氧气输送到反应器的氧气和通过反应器的燃烧气体的载气的连续流，然后通过气相色谱 分析仪，并在分离后进入热导检测器。 提供具有数据处理器的电子设备用于控制处理系统。 确定限流器或限制器上游和下游气体的压力差。 参考载体气体的电子压力调节器或流量调节器以及还用作清洗的至少一个载气出口阀被插入到该载气参考线上。

公开(公告)号：US08616073B2

公开(公告)日：2013-12-31

申请号：US12849660

申请日：2010-08-03

申请人： Leonardo Sisti

发明人： Leonardo Sisti

IPC分类号： G01N1/22

CPC分类号： G01N30/24 ,  G01N1/34 ,  G01N1/44 ,  G01N30/66 ,  G01N31/12 ,  G01N35/1097 ,  G01N2001/2267 ,  G01N2030/025 ,  G01N2030/125 ,  G01N2030/8859

摘要： A sampler for an elemental analyzer comprises a sample housing suitable to accommodate one or more samples, sealed in tin or silver capsules, to be analyzed, a closure mechanism suitable to reversibly seal the sample housing, a sample passage having a connection opening for the passage by gravity of the one or more samples from the sampler into the analyzer through the connection opening. The sampler further comprises a heater for heating the sample housing and a vacuum system or other means for pumping out environmental gases and vapors from the sample housing.

摘要翻译： 用于元素分析器的采样器包括适于容纳要分析的一个或多个密封在锡或银胶囊中的一个或多个样品的样品壳体，适于可逆地密封样品壳体的闭合机构，具有用于通道的连接开口的样品通道 通过重力将一个或多个样品从采样器通过连接口进入分析器。 采样器还包括用于加热样品壳体的加热器和用于从样品壳体泵出环境气体和蒸汽的真空系统或其它装置。

公开(公告)号：US07255834B2

公开(公告)日：2007-08-14

申请号：US10302306

申请日：2002-11-22

申请人： Stefano Boursier Niutta ,  Leonardo Sisti

发明人： Stefano Boursier Niutta ,  Leonardo Sisti

IPC分类号： B32B5/02

CPC分类号： G01N31/12 ,  G01N30/12 ,  G01N2030/125 ,  Y10T436/12

摘要： A method and device are provided for dynamic flash combustion reaction connected with gas chromatography for the elemental analysis of C H N S O in an automatic elemental analyzer. A combustion reactor is provided with a sampling device and an oxygen feed line. Controlled volumes of oxygen are admitted with the oxygen feed line into the combustion reactor depending on the sample for the complete combustion thereof. A pneumatic circuit is provided, in which the oxygen feed line converges and the pneumatic circuit creates a continuous flow of a carrier gas that is able to carry the oxygen to the reactor and the gases of the combustion through the reactor, then through a gas chromatographic analyzer, and after their separation, into a thermal conductivity detector. An electronic apparatus with a data processor is provided for controlling the process systems. The difference in the pressure of the gas upstream and downstream of a restrictor or restriction is determined. The electronic pressure regulator or flow regulator of the reference carrier gas and at least one carrier gas outlet valve, which is also used as purging, is inserted on this carrier gas reference line.

摘要翻译： 提供了一种与气相色谱相连的动态闪燃反应方法和装置，用于在自动元素分析仪中对C H N S O进行元素分析。 燃烧反应器设置有取样装置和氧气供给管线。 根据用于其完全燃烧的样品，氧气的受控体积被氧气进入管线进入燃烧反应器。 提供了一种气动回路，其中氧气供给管线汇合，气动回路产生能够将氧气输送到反应器的氧气和通过反应器的燃烧气体的载气的连续流，然后通过气相色谱 分析仪，并在分离后进入热导检测器。 提供具有数据处理器的电子设备用于控制处理系统。 确定限流器或限制器上游和下游气体的压力差。 参考载体气体的电子压力调节器或流量调节器以及还用作清洗的至少一个载气出口阀被插入到该载气参考线上。