Invention Grant
US09073826B2 Process for preparing and purifying salts of acrylamido-2-methylpropanesulfonic acid
有权
制备和纯化丙烯酰胺-2-甲基丙磺酸盐的方法
- Patent Title: Process for preparing and purifying salts of acrylamido-2-methylpropanesulfonic acid
- Patent Title (中): 制备和纯化丙烯酰胺-2-甲基丙磺酸盐的方法
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Application No.: US13687156Application Date: 2012-11-28
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Publication No.: US09073826B2Publication Date: 2015-07-07
- Inventor: Klaus Ebel , Tobias Voitl , Andreas Keller , Stefan Rüdenauer , Karsten Bartling , Bjorn Langlotz , Jochen Steiner
- Applicant: BASF SE
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Drinker Biddle & Reath LLP
- Main IPC: C07C303/22
- IPC: C07C303/22 ; C07C309/15 ; C07C303/32 ; C07C303/44

Abstract:
A process for preparing salts of acrylamido-2-methylpropanesulfonic acid (A) using the steps of: preparing a solution of a contaminated salt of acrylamido-2-methyl-propanesulfonic acid (A) in an anhydrous organic solvent (L) using at least one basic component (B) selected from the group of alkali metal oxides, alkaline earth metal oxides, alkali metal hydroxides, alkaline earth metal hydroxides and amines of the formula (I) NRaRbRc (I) where the Ra, Rb and Rc radicals are each independently: hydrogen, C1-C4-alkyl, hydroxy-C1-C4-alkyl or C1-C4-alkoxy, where the molar ratio of compound (A) to the basic component (B) is 1:1 to 1:3, recovering the dissolved salt of compound (A) by crystallization or by precipitation, by altering the temperature and/or the pressure and/or the concentration of the salt in the solution. This leads to salts which are low in by-products and are particularly suitable for polymerization.
Public/Granted literature
- US20130137893A1 PROCESS FOR PREPARING AND PURIFYING SALTS OF ACRYLAMIDO-2-METHYLPROPANESULFONIC ACID Public/Granted day:2013-05-30
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