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    IRON-COMPRISING HETEROGENEOUS CATALYST AND PROCESS FOR PREPARING OLEFINS BY REACTION OF CARBON MONOXIDE WITH HYDROGEN
    3.
    发明申请
    IRON-COMPRISING HETEROGENEOUS CATALYST AND PROCESS FOR PREPARING OLEFINS BY REACTION OF CARBON MONOXIDE WITH HYDROGEN 有权
    含有异构催化剂的铁和通过氢氧化碳反应制备烯烃的方法

    公开(公告)号：US20130245138A1

    公开(公告)日：2013-09-19

    申请号：US13782353

    申请日：2013-03-01

    Applicant: BASF SE

    Inventor： Jochen Steiner ,  Kerem Bay ,  Ekkehard Schwab ,  Ralf Böhling

    IPC: B01J27/20

    CPC classification number: B01J27/20 ,  B01J23/745 ,  B01J23/78 ,  B01J35/023 ,  B01J37/0201 ,  B01J37/086 ,  B01J37/18 ,  C10G2/332 ,  C10G2400/20

    Abstract: A process for preparing olefins by reaction of carbon monoxide with hydrogen in the presence of a an iron-comprising heterogeneous catalyst produced by the following steps: thermal decomposition of gaseous iron pentacarbonyl to give carbonyl iron powder having spherical primary particles; treatment of carbonyl iron powder with hydrogen, resulting in the metallic spherical primary particles at least partially forming agglomerates; contacting the agglomerates with iron pentacarbonyl; and thermal decomposition of the iron pentacarbonyl to give at least predominantly pore-free and void-free secondary particles.

    Abstract translation: 一种通过一氧化碳与氢反应在含铁非均相催化剂存在下通过以下步骤制备的烯烃的方法：热分解气态铁五羰基，得到具有球形初级颗粒的羰基铁粉; 用氢气处理羰基铁粉末，导致金属球形初级颗粒至少部分形成附聚物; 使附聚物与五羰基铁接触; 并且五羰基铁的热分解至少主要是无孔隙和无空隙的二次颗粒。

    Process for preparing and purifying salts of acrylamido-2-methylpropanesulfonic acid
    5.
    发明授权
    Process for preparing and purifying salts of acrylamido-2-methylpropanesulfonic acid 有权
    制备和纯化丙烯酰胺-2-甲基丙磺酸盐的方法

    公开(公告)号：US09073826B2

    公开(公告)日：2015-07-07

    申请号：US13687156

    申请日：2012-11-28

    Applicant: BASF SE

    Inventor： Klaus Ebel ,  Tobias Voitl ,  Andreas Keller ,  Stefan Rüdenauer ,  Karsten Bartling ,  Bjorn Langlotz ,  Jochen Steiner

    IPC: C07C303/22 ,  C07C309/15 ,  C07C303/32 ,  C07C303/44

    CPC classification number: C07C303/22 ,  C07C303/32 ,  C07C303/44 ,  C07C309/15

    Abstract: A process for preparing salts of acrylamido-2-methylpropanesulfonic acid (A) using the steps of: preparing a solution of a contaminated salt of acrylamido-2-methyl-propanesulfonic acid (A) in an anhydrous organic solvent (L) using at least one basic component (B) selected from the group of alkali metal oxides, alkaline earth metal oxides, alkali metal hydroxides, alkaline earth metal hydroxides and amines of the formula (I) NRaRbRc  (I) where the Ra, Rb and Rc radicals are each independently: hydrogen, C1-C4-alkyl, hydroxy-C1-C4-alkyl or C1-C4-alkoxy, where the molar ratio of compound (A) to the basic component (B) is 1:1 to 1:3, recovering the dissolved salt of compound (A) by crystallization or by precipitation, by altering the temperature and/or the pressure and/or the concentration of the salt in the solution. This leads to salts which are low in by-products and are particularly suitable for polymerization.

    Abstract translation: 一种使用以下步骤制备丙烯酰氨基-2-甲基丙磺酸（A）的盐的方法：使用至少在无水有机溶剂（L）中制备丙烯酰胺基-2-甲基 - 丙磺酸（A）的污染盐的溶液 选自碱金属氧化物，碱土金属氧化物，碱金属氢氧化物，碱土金属氢氧化物和式（I）NRaRbRc（I）的胺的一种碱性组分（B），其中R a，R b和R c基团各自为 独立地：氢，C1-C4-烷基，羟基-C1-C4-烷基或C1-C4-烷氧基，其中化合物（A）与碱性组分（B）的摩尔比为1:1至1:3，回收 化合物（A）的溶解盐通过结晶或沉淀，改变溶液中盐的温度和/或压力和/或浓度。 这导致副产物低的盐，特别适用于聚合。

    PROCESS FOR PREPARING AND PURIFYING SALTS OF ACRYLAMIDO-2-METHYLPROPANESULFONIC ACID
    6.
    发明申请
    PROCESS FOR PREPARING AND PURIFYING SALTS OF ACRYLAMIDO-2-METHYLPROPANESULFONIC ACID 有权
    丙烯酰胺-2-甲基丙烯酸的制备和纯化工艺

    公开(公告)号：US20130137893A1

    公开(公告)日：2013-05-30

    申请号：US13687156

    申请日：2012-11-28

    Applicant: BASF SE

    Inventor： Klaus Ebel ,  Tobias Voitl ,  Andreas Keller ,  Stefan Rüdenauer ,  Karsten Bartling ,  Bjorn Langlotz ,  Jochen Steiner

    IPC: C07C303/22 ,  C07C309/15

    CPC classification number: C07C303/22 ,  C07C303/32 ,  C07C303/44 ,  C07C309/15

    Abstract: A process for preparing salts of acrylamido-2-methylpropanesulfonic acid (A) using the steps of: preparing a solution of a contaminated salt of acrylamido-2-methyl-propanesulfonic acid (A) in an anhydrous organic solvent (L) using at least one basic component (B) selected from the group of alkali metal oxides, alkaline earth metal oxides, alkali metal hydroxides, alkaline earth metal hydroxides and amines of the formula (I) NRaRbRc  (I) where the Ra, Rb and Rc radicals are each independently: hydrogen, C1-C4-alkyl, hydroxy-C1-C4-alkyl or C1-C4-alkoxy, where the molar ratio of compound (A) to the basic component (B) is 1:1 to 1:3, recovering the dissolved salt of compound (A) by crystallization or by precipitation, by altering the temperature and/or the pressure and/or the concentration of the salt in the solution. This leads to salts which are low in by-products and are particularly suitable for polymerization.

    Abstract translation: 一种使用以下步骤制备丙烯酰氨基-2-甲基丙磺酸（A）的盐的方法：使用至少在无水有机溶剂（L）中制备丙烯酰氨基-2-甲基 - 丙磺酸（A）的污染盐的溶液 选自碱金属氧化物，碱土金属氧化物，碱金属氢氧化物，碱土金属氢氧化物和式（I）NRaRbRc（I）的胺的一种碱性组分（B），其中R a，R b和R c基团各自为 独立地：氢，C1-C4-烷基，羟基-C1-C4-烷基或C1-C4-烷氧基，其中化合物（A）与碱性组分（B）的摩尔比为1:1至1:3，回收 化合物（A）的溶解盐通过结晶或沉淀，改变溶液中盐的温度和/或压力和/或浓度。 这导致副产物低的盐，特别适用于聚合。

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