Invention Grant
- Patent Title: Method for producing tetrafluoroborate
- Patent Title (中): 生产四氟硼酸盐的方法
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Application No.: US13377795Application Date: 2009-06-19
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Publication No.: US09376323B2Publication Date: 2016-06-28
- Inventor: Masahide Waki , Kazuhiro Miyamoto , Kazutaka Hirano
- Applicant: Masahide Waki , Kazuhiro Miyamoto , Kazutaka Hirano
- Applicant Address: JP Osaka-Shi
- Assignee: STELLA CHEMIFA CORPORATION
- Current Assignee: STELLA CHEMIFA CORPORATION
- Current Assignee Address: JP Osaka-Shi
- Agency: Law Office of Katsuhiro Arai
- International Application: PCT/JP2009/061216 WO 20090619
- International Announcement: WO2010/146710 WO 20101223
- Main IPC: C01B35/06
- IPC: C01B35/06 ; H01M10/0525 ; H01M10/0568

Abstract:
An object of the invention is to provide a tetrafluoroborate producing method that allows high-yield, high-efficiency production of a tetrafluoroborate by a continuous process, a tetrafluoroborate-containing electrolyte, and an electrical storage device including such an electrolyte. The invention provides a method for producing a tetrafluoroborate, which includes: a first step including dissolving boron trifluoride gas in an organic solvent; a second step including adding, to the organic solvent, a fluoride (MFn, wherein M represents a metal or NH4, and 1≦n≦3) in an amount stoichiometrically equivalent to or less than the amount of the boron trifluoride so that a tetrafluoroborate solution is produced; and a third step including circulating the tetrafluoroborate solution through the first step so that the boron trifluoride gas is dissolved in the tetrafluoroborate solution instead of the organic solvent.
Public/Granted literature
- US20120082608A1 METHOD FOR PRODUCING TETRAFLUOROBORATE Public/Granted day:2012-04-05
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