- 专利标题: Method of preparing copper-based composite conductive powder
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申请号: US14825146申请日: 2015-08-12
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公开(公告)号: US09761346B2公开(公告)日: 2017-09-12
- 发明人: Jianhong Liu , Qianling Zhang , Chuanxin He , Jian Xu , Xiangning Ren , Xiaoming Li , Chuhong Liao
- 申请人: Jianhong Liu
- 申请人地址: CN Shenzhen
- 专利权人: SHENZHEN EIGEN-EQUATION GRAPHENE TECHNOLOGY CO., LTD.
- 当前专利权人: SHENZHEN EIGEN-EQUATION GRAPHENE TECHNOLOGY CO., LTD.
- 当前专利权人地址: CN Shenzhen
- 代理机构: Matthias Scholl P.C.
- 主分类号: H01B1/08
- IPC分类号: H01B1/08 ; B22F9/24 ; C09J9/02 ; C09D133/20 ; C08L79/00 ; C08F220/44
摘要:
A method of preparing a copper-based composite conductive powder. The method includes: (1) preparing a liquid polyacrylonitrile (LPAN) solution, stirring the LPAN solution to yield a cyclized polyacrylonitrile solution; (2) heating the cyclized LPAN solution at between 200 and 300° C. for between 1 and 10 hrs to yield a thermally-oxidized polyacrylonitrile having a ladder structure; (3) adding the thermally-oxidized polyacrylonitrile and a copper compound to a solvent, and uniformly mixing, to yield a polyacrylonitrile coated copper compound; (4) drying the polyacrylonitrile coated copper compound to yield a carbonized precursor coated copper compound; and (5) calcining the carbonized precursor coated copper compound in the presence of an inert gas flow of between 10 and 500 mL/min for between 6 and 24 hrs at the temperature of between 300 and 1800° C.