- 专利标题: Method for preparing nickel-cobalt-manganese hydroxide
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申请号: US14775397申请日: 2013-04-28
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公开(公告)号: US09815709B2公开(公告)日: 2017-11-14
- 发明人: Yannan Ou , Changdong Li , Haijun Yu
- 申请人: GUANGDONG BRUNP RECYCLING TECHNOLOGY CO., LTD , HUNAN BRUNP RECYCLING TECHNOLOGY CO., LTD
- 申请人地址: CN Guangdung CN Hunan
- 专利权人: Guangdong Brunp Recycling Technology Co., Ltd,Hunan Brunp Recycling Technology Co. Ltd.
- 当前专利权人: Guangdong Brunp Recycling Technology Co., Ltd,Hunan Brunp Recycling Technology Co. Ltd.
- 当前专利权人地址: CN Guangdung CN Hunan
- 代理机构: Hahn Loeser & Parks, LLP—San Diego
- 优先权: CN201310076317 20130311
- 国际申请: PCT/CN2013/074976 WO 20130428
- 国际公布: WO2014/139200 WO 20140918
- 主分类号: C01G53/00
- IPC分类号: C01G53/00 ; H01M4/04 ; H01M4/485 ; H01M4/505 ; H01M4/525 ; H01M10/052
摘要:
A method for preparing nickel-cobalt-manganese hydroxide. The method comprises the following steps: (1) dissolving microcrystalline cellulose into water to obtain a suspension; and adding a nickel source, a cobalt source, and a manganese source into the suspension to obtain a solution containing nickel, cobalt, and manganese; (2) adding hexamethylenetetramine into the solution containing nickel, cobalt, and manganese, heating the reaction solution to 80-90° C., and reacting for 5-10 min, then heating with a microwave hydrothermal synthesis instrument at a frequency of 2450 MHz for 10-60 min; and (3) filtering the reaction solution obtained in step (2), and taking the filter residue, washing the filter residue with pure water and ethanol respectively, then drying, crushing, and screening the filter residue to obtain nickel-cobalt-manganese hydroxide. Nickel-cobalt-manganese hydroxide prepared from the abovementioned method has a uniform particle size and consistent morphology and structure; thus solving the problems of the uncontrollable appearance and structure and the inconsistent performances of the product caused by the vigorous reaction in the existing method for preparing nickel-cobalt-manganese hydroxide.
公开/授权文献
- US20160016815A1 METHOD FOR PREPARING NICKEL-COBALT-MANGANESE HYDROXIDE 公开/授权日:2016-01-21
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