Invention Grant
- Patent Title: Method for preparing precursor of lithium composite transition metal oxide using a reactor
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Application No.: US15040348Application Date: 2016-02-10
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Publication No.: US09899675B2Publication Date: 2018-02-20
- Inventor: Byungchun Park , Seong Hoon Kang , HoSuk Shin , SangMin Park , Hong Kyu Park
- Applicant: LG Chem, Ltd.
- Applicant Address: KR
- Assignee: LG Chem, Ltd.
- Current Assignee: LG Chem, Ltd.
- Current Assignee Address: KR
- Agency: Lerner, David, Littenberg, Krumholz & Mentlik, LLP
- Priority: KR10-2012-0010134 20120201
- Main IPC: H01M4/00
- IPC: H01M4/00 ; H01M4/505 ; B01J19/18 ; B01J19/28 ; C01G45/12 ; C01G51/00 ; C01G53/00 ; C01G53/04 ; H01M4/525 ; H01M10/052

Abstract:
Disclosed is a method for preparing a precursor of lithium composite transition metal oxide for lithium secondary batteries, using a reactor having a closed structure including an outer stationary cylinder; an inner rotary cylinder on the same axis; and a rotation reaction area disposed between them, wherein ring-shaped vortex pairs that are uniformly arranged in a rotation axis direction and rotate in opposite directions are formed in the rotation reaction area. According to the method of the invention, raw materials comprising an aqueous solution of two or more transition metal salts, an aqueous solution of a complex forming additive, and a basic aqueous solution for maintaining pH are fed through an inlet into the rotation reaction area where a coprecipitation reaction is performed under a non-nitrogen atmosphere to form lithium composite transition metal oxide particles which are then discharged through a reactor outlet.
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