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779 条记录 (耗时 0.023 秒)

    Lead-free low-melting glass
    92.
    发明公开
    Lead-free low-melting glass 有权
    Bleifreies niedrigschmelzendes Glas

    公开(公告)号：EP1361199A1

    公开(公告)日：2003-11-12

    申请号：EP03009192.0

    申请日：2003-04-22

    申请人： Central Glass Company, Limited

    发明人： Hayakawa, Naoya, Central Glass Company, Limited ,  Shimooka, Taishin, Central Glass Company, Limited

    IPC分类号： C03C3/066 ,  C03C8/24

    CPC分类号： C03C8/24 ,  C03C3/066 ,  Y10T428/24802

    摘要： The invention relates to a lead-free, low-melting glass for covering a substrate. This glass contains 0.1-25 wt% of SiO 2 , 1-50 wt% of B 2 O 3 , 1-45 wt% of ZnO, 20-90 wt% of Bi 2 O 3 , 0.1-40 wt% of V 2 O 5 , 0-5 wt% of Nb 2 O 5 , 0-20 wt% of R 2 O where R is Li, Na or K, and 0-20 wt% of RO where R is Mg, Ca, Sr or Ba. This glass has a thermal expansion coefficient of from 65 × 10 -7 /°C to 100 × 10 -7 /°C within a range of 30-300°C; and has a softening point of not higher than 630°C.

    摘要翻译： 本发明涉及一种用于覆盖基板的无铅低熔点玻璃。 该玻璃含有0.1-25重量％的SiO 2，1-50重量％的B 2 O 3，1-45重量％的ZnO，20-90重量％的Bi 2 O 3，0.1-40重量％的V 2 O 5，0-5重量％的Nb 2 O 5 ，0-20重量％的R 2 O，其中R是Li，Na或K，和0-20重量％的RO，其中R是Mg，Ca，Sr或Ba。 该玻璃在30〜300℃的范围内的热膨胀系数为65×10 -7 /℃至100×10 -7 /℃; 且软化点不高于630℃。

    Process for synthesizing ionic metal complex
    94.
    发明公开
    Process for synthesizing ionic metal complex 有权
    一种用于离子金属配合物的制备方法

    公开(公告)号：EP1308449A3

    公开(公告)日：2003-09-24

    申请号：EP02024608.8

    申请日：2002-11-04

    申请人： Central Glass Company, Limited

    发明人： Tsujioka, Shoichi ,  Takase, Hironari ,  Takahashi, Mikihiro ,  Isono, Yoshimi

    IPC分类号： C07F5/02 ,  C07F9/6571

    CPC分类号： C07F5/022 ,  C07F9/6571

    摘要： The invention relates to a process for synthesizing an ionic metal complex represented by the general formula (1) or (5). This process includes reacting in an organic solvent a compound (corresponding to ligand of the complex) represented by the general formula (2) or (6) with a halogen-containing compound represented by the general formula (3) or (4), in the presence of a reaction aid containing an element selected from the group consisting of elements of groups 1-4 and 11-14 of the periodic table. It is possible by this process to easily and efficiently synthesize the ionic metal complex, which can be used as a supporting electrolyte for electrochemical devices, a polymerization catalyst of polyolefins and so forth, or a catalyst for organic synthesis.

    Process for synthesizing ionic metal complex
    99.
    发明公开
    Process for synthesizing ionic metal complex 有权
    Verfahren zur Herstellung ionischer Metallkomplexe

    公开(公告)号：EP1308449A2

    公开(公告)日：2003-05-07

    申请号：EP02024608.8

    申请日：2002-11-04

    申请人： Central Glass Company, Limited

    发明人： Tsujioka, Shoichi ,  Takase, Hironari ,  Takahashi, Mikihiro ,  Isono, Yoshimi

    IPC分类号： C07F5/02 ,  C07F9/6571

    CPC分类号： C07F5/022 ,  C07F9/6571

    摘要： The invention relates to a process for synthesizing an ionic metal complex represented by the general formula (1) or (5). This process includes reacting in an organic solvent a compound (corresponding to ligand of the complex) represented by the general formula (2) or (6) with a halogen-containing compound represented by the general formula (3) or (4), in the presence of a reaction aid containing an element selected from the group consisting of elements of groups 1-4 and 11-14 of the periodic table. It is possible by this process to easily and efficiently synthesize the ionic metal complex, which can be used as a supporting electrolyte for electrochemical devices, a polymerization catalyst of polyolefins and so forth, or a catalyst for organic synthesis.

    摘要翻译： 本发明涉及一种合成由通式（1）或（5）表示的离子金属络合物的方法。 该方法包括在有机溶剂中使由通式（2）或（6）表示的化合物（相当于络合物的配位体）与通式（3）或（4）表示的含卤素化合物在 含有选自元素周期表第1-4和11-14族元素的元素的反应助剂的存在。 该方法可以容易且有效地合成可用作电化学装置的支持电解质，聚烯烃等的聚合催化剂或有机合成催化剂的离子金属络合物。

    Process for producing 4-sustituted benzopyran derivatives
    100.
    发明公开
    Process for producing 4-sustituted benzopyran derivatives 审中-公开
    生产4-取代苯并吡喃衍生物的方法

    公开(公告)号：EP1298129A2

    公开(公告)日：2003-04-02

    申请号：EP02021753.5

    申请日：2002-09-25

    申请人： Central Glass Company, Limited

    发明人： Komata, Takeo, Chemical Research Center ,  Fujiwara, Masaki, Chemical Research Center ,  Tarui, Takanao, Chemical Research Center ,  Saito, Yusuke, Chemical Research Center ,  Minesaki, Hiroshi, Chemical Research Center

    IPC分类号： C07D311/58 ,  C07C49/84 ,  C07C45/68

    CPC分类号： C07D311/58 ,  C07C45/46 ,  C07C45/673 ,  C07C49/84 ,  C07C49/825

    摘要： The present invention relates to a first process for producing a 2,2-bis(fluoromethyl)-6-(perfluoroalkyl)-2H-1-benzopyran-4-carboxylic acid. The first process includes the steps of (a) reacting a 2,2-bis(fluoromethyl)-6-(perfluoroalkyl)-2H-1-benzopyran-4-one with a perfluoroalkanesulfonic acid anhydride in the presence of a base, thereby obtaining a perfluoroalkanesulfonic 2,2-bis(fluoromethyl)-6-(perfluoroalkyl)-2H-1-benzopyran-4-yl ester; and (b) reacting the benzopyranyl ester with carbon monoxide in the presence of a palladium complex compound and a base, thereby obtaining the carboxylic acid. The present invention further relates to a second process for producing a 2-hydroxy-5-(perfluoroalkyl) acetophenone, which can be a raw material for producing the carboxylic acid. The second process includes the steps of (c) reacting a 4-(perfluoroalkyl)alkoxybenzene with acetic anhydride or an acyl halide in the presence of a Lewis acid, thereby obtaining a 2-alkoxy-5- (perfluoroalkyl)acetophenone; and (d) dealkylating the 2-alkoxy-5-(perfluoroalkyl) acetophenone by a dealkylating agent.

    摘要翻译： 本发明涉及生产2,2-双（氟甲基）-6-（全氟烷基）-2H-1-苯并吡喃-4-羧酸的第一种方法。 第一种方法包括以下步骤：（a）在碱存在下使2,2-双（氟甲基）-6-（全氟烷基）-2H-1-苯并吡喃-4-酮与全氟链烷磺酸酐反应，从而得到 全氟烷基磺酸2,2-双（氟甲基）-6-（全氟烷基）-2H-1-苯并吡喃-4-基酯; （b）使该苯并吡喃基酯与一氧化碳在钯络合物和碱的存在下反应，由此得到羧酸。 本发明还涉及生产2-羟基-5-（全氟烷基）苯乙酮的第二种方法，其可以是用于生产羧酸的原料。 第二种方法包括以下步骤：（c）使4-（全氟烷基）烷氧基苯与乙酸酐或酰基卤在路易斯酸存在下反应，由此得到2-烷氧基-5-（全氟烷基）苯乙酮; 和（d）用脱烷基剂将2-烷氧基-5-（全氟烷基）苯乙酮脱烷基化。