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    Preparation of hydrolyzable group-containing organohydrogenpolysiloxane and organopolysiloxane derived therefrom
    71.
    发明公开
    Preparation of hydrolyzable group-containing organohydrogenpolysiloxane and organopolysiloxane derived therefrom 有权
    Herstellung von hydrolysierbarem gruppenhaltigen Organowasserstoffpolysiloxan und daraus abgeleitetes Organpolysiloxan

    公开(公告)号：EP2147949A1

    公开(公告)日：2010-01-27

    申请号：EP09251831.5

    申请日：2009-07-20

    申请人： Shin-Etsu Chemical Co., Ltd.

    发明人： Amemiya, Masahiro ,  Uehara, Hitoshi ,  Kudo, Muneo ,  Asai, Mitsuo

    IPC分类号： C08G77/08 ,  C08G77/12

    CPC分类号： C08G77/12 ,  C08G77/08 ,  C08G77/34 ,  C08G77/38

    摘要： A hydrolyzable group-containing organohydrogenpolysiloxane is prepared by (A) reacting (a) an organosiloxane with (b) an organosilane or organosiloxane containing a hydrolyzable group, at least one of components (a) and (b) containing hydrosilyl, in the presence of a superstrong acid catalyst, (B) adding an inorganic basic neutralizing agent and/or an adsorbent to the resulting reaction solution, and (C) removing the neutralized and/or adsorbed form of the superstrong acid catalyst. The process proceeds in an essentially non-aqueous system, and the organohydrogenpolysiloxane free of residual acidic catalyst is obtainable at low cost.

    摘要翻译： 通过（A）使（a）有机硅氧烷与（b）含有可水解基团的有机硅烷或有机硅氧烷，含有氢化甲硅烷基的组分（a）和（b））中的至少一种在（A）存在下反应，制备可水解基团的有机氢聚硅氧烷， 超强酸催化剂，（B）向所得反应溶液中添加无机碱性中和剂和/或吸附剂，（C）除去超强酸催化剂的中和和/或吸附形式。 该方法在基本上非水系统中进行，并且以低成本获得不含残留酸性催化剂的有机氢聚硅氧烷。

    Method for making alkoxy-modified silsesquioxanes
    74.
    发明公开
    Method for making alkoxy-modified silsesquioxanes 有权
    Verfahren zur Herstellung von alkylmodifizierten Silsequioxanen

    公开(公告)号：EP1995267A2

    公开(公告)日：2008-11-26

    申请号：EP08009287.7

    申请日：2008-05-20

    申请人： Bridgestone Corporation

    发明人： Hergenrother, William L. ,  Pawlow, James H. ,  Hogan, Terrence E. ,  Hilton, Ashley S.

    IPC分类号： C08G77/18 ,  C08G77/04 ,  C08G77/28 ,  C08G77/08

    CPC分类号： C08G77/08 ,  B60C1/00 ,  C08G77/18 ,  C08G77/28 ,  C08K3/013 ,  C08L9/00 ,  C08L21/00 ,  C08L83/06 ,  C08L83/08 ,  Y02P20/584 ,  C08L83/00

    摘要： A method is presented for making alkoxy-modified silsesquioxanes (AMS) or coalkoxy-modified silsesquioxanes (co-AMS,) comprising the steps of (a) combining as a reaction mixture (i) water, (ii) an acid-stable solvent for the water, (iii) a solid strong cationic hydrolysis and condensation catalyst, and (iv) a trialkoxysilane compound, (b) allowing the reaction mixture to react for about 0.5 hours to about 200 hours to form the alkoxy-modified silsesquioxanes; and (c) recovering the alkoxy-modified silsesquioxanes from the reaction mixture. The use of solid strong cationic catalysts in this reaction system is advantageous because they remain as solids throughout the reaction, allowing simplified separation of the solid catalyst from the soluble AMS or co-AMS products, resulting in total or near total recovery of the AMS or co-AMS products, the products being free of, or substantially free of residual acid catalyst, as well as virtual total recovery of the catalyst for recycling. The improved AMS and co-AMS compounds, vulcanizable rubber compounds containing them, and a pneumatic tire having a component made from the vulcanized rubber compounds are also presented.

    摘要翻译： 提出了制备烷氧基改性倍半硅氧烷（AMS）或共烷氧基改性倍半硅氧烷（co-AMS）的方法，其包括以下步骤：（a）将反应混合物（i）水，（ii）酸稳定溶剂 水，（iii）固体强阳离子水解和缩合催化剂，和（iv）三烷氧基硅烷化合物，（b）使反应混合物反应约0.5小时至约200小时以形成烷氧基改性倍半硅氧烷; 和（c）从反应混合物中回收烷氧基改性的倍半硅氧烷。 在该反应体系中使用固体强阳离子催化剂是有利的，因为它们在整个反应中保留为固体，允许固体催化剂与可溶性AMS或共-AMS产物的简单分离，导致AMS或 共同AMS产品，产品没有或基本上没有残留的酸催化剂，以及用于再循环的催化剂的虚拟总回收。 还提出了改进的AMS和共AMS化合物，含有它们的可硫化橡胶化合物和具有由硫化橡胶化合物制成的组分的充气轮胎。

    Hydrophilic Polysiloxane Elastomers
    75.
    发明公开
    Hydrophilic Polysiloxane Elastomers 审中-公开
    亲水聚硅氧烷弹性体

    公开(公告)号：EP1970397A1

    公开(公告)日：2008-09-17

    申请号：EP07103950.7

    申请日：2007-03-12

    申请人： Schering Oy

    发明人： Tiitinen, Emilia ,  Jukarainen, Harri

    IPC分类号： C08G77/06 ,  C08G77/46 ,  C08G77/08

    CPC分类号： C08G77/46 ,  C08G77/06 ,  C08G77/08

    摘要： The present invention relates to a method for manufacturing hydrophilic polysiloxanes, wherein a hydrido-containing cyclic siloxane is reacted with a hydrophilic molecule comprising a carbon-carbon double bond, having the general formula (l) H 2 C=CH-(CHR) n -O-(CHR 1 CR 2 R 3 ) m R 4 or (II) H 2 C=CH-(CHR) n -R 5 , wherein n is an integer from 0 to 4, m is an integer from 0 to 5, R, R 1 , R 2 , R 3 and R 4 are each independently hydrogen or a C 1 to C 6 alkyl, R 5 is a saturated cyclic hydrocarbon containing carbonyl group, in the presence of a first catalyst to obtain a monomer, and polymerising said monomer in the presence of a second catalyst. The present invention also relates to hydrophilic polysiloxanes and to elastomers based on these polysiloxanes.

    摘要翻译： 本发明涉及一种亲水性聚硅氧烷的制造方法，其中含氢环状硅氧烷与包含碳 - 碳双键的亲水性分子反应，具有通式（I）H 2 C = CH-（CHR）n -O-（CHR 1 CR 2 R 3）m R 4或（II）H 2 C = CH-（CHR）n -R 5，其中n为0至4的整数，m为0至5的整数 R 1，R 2，R 3和R 4各自独立地为氢或C 1〜C 6烷基，R 5为饱和的含有羰基的烃基，在第一催化剂存在下，得到单体， 并在第二催化剂存在下使所述单体聚合。 本发明还涉及亲水性聚硅氧烷和基于这些聚硅氧烷的弹性体。

    SILICON COMPOUND CONTAINING EPOXY GROUP AND THERMOSETTING RESIN COMPOSITION
    79.
    发明公开
    SILICON COMPOUND CONTAINING EPOXY GROUP AND THERMOSETTING RESIN COMPOSITION 审中-公开
    环氧化物SILICON连接及热固性树脂组合物

    公开(公告)号：EP1593703A4

    公开(公告)日：2007-06-06

    申请号：EP04709709

    申请日：2004-02-10

    申请人： NIPPON KAYAKU KK

    发明人： NAKAYAMA KOJI

    IPC分类号： C08G77/14 ,  C08L63/00 ,  C08L83/06 ,  C08G59/02

    CPC分类号： C08G77/14 ,  C08G77/08 ,  C08L63/00 ,  C08L83/06 ,  C08L2666/14

    摘要： A silicon compound containing an epoxy group which is obtainable by subjecting at least one alkoxy silicon compound containing an epoxy group represented by a general formula (1a): R1aSi(OR2)3, wherein R1a represents a substituent having an epoxy group and R2 represents an alkyl group having four or less carbon atoms, by itself, or said compound and at least one substituted alkoxy silicon compound represented by a general formula (1b): R1bSi(OR3)3, wherein R1b represents an alkyl group having ten or less carbon atoms, an aryl group or an unsaturated aliphatic residue, and R3 represents an alkyl group having four or less carbon atoms, to a condensation reaction in the presence of a basic catalyst.