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    METHOD AND APPARATUS FOR PRODUCING VAPOR GROWN CARBON FIBER
    71.
    发明公开
    METHOD AND APPARATUS FOR PRODUCING VAPOR GROWN CARBON FIBER 有权
    用于生产碳纤维直接存入从气体（VGCF）

    公开(公告)号：EP1407064A1

    公开(公告)日：2004-04-14

    申请号：EP02743727.6

    申请日：2002-06-26

    申请人： SHOWA DENKO K.K.

    发明人： MURAMAKI, Kazuo,c/o Showa Denko K.K. ,  SAKAMOTO, Y.,c/o Showa Denko K.K. ,  YAMAMOTO, Ryuji,c/o Showa Denko K.K. ,  MORITA, Toshio,c/o Showa Denko K.K.

    IPC分类号： D01F9/127 ,  D01F9/133

    CPC分类号： B82Y30/00 ,  D01F9/127 ,  D01F9/133

    摘要： (1) A method for producing vapor grown carbon, comprising mixing a raw material gas containing an organic compound and an organo-transition metallic compound preliminarily heated preferably to a temperature 100 to 145 °C with a carrier gas heated preferably to a temperature 700 to 1,600 °C, and introducing the resultant gas mixture into a carbon fiber production zone, wherein preferably a mixture of an aromatic compound and acetylene, ethylene, or butadiene is used as an organic compound; (2) a method in which a transition metallic compound is dissolved in a solvent, the resultant solution is atomized into fine droplets, the solvent in the droplets is evaporated to thereby obtain fine particles of the transition metal compound, the drifting particles are introduced with an organic compound gas into the carbon fiber production zone; (3) an apparatus used in the production methods; and (4) vapor grown carbon fiber thereby produced.

    FINE CARBON FIBER AND PROCESS FOR PRODUCING THE SAME, AND CONDUCTIVE MATERIAL COMPRISING THE SAME
    77.
    发明公开
    FINE CARBON FIBER AND PROCESS FOR PRODUCING THE SAME, AND CONDUCTIVE MATERIAL COMPRISING THE SAME 审中-公开
    FEINE KOHLENSTOFFFASERN，HERSTELLUNGSVERFAHREN UND DARAUS HERGESTELLTESLEITFÄHIGESMATERIAL

    公开(公告)号：EP1275759A1

    公开(公告)日：2003-01-15

    申请号：EP01919852.2

    申请日：2001-04-10

    申请人： SHOWA DENKO K.K.

    发明人： MORITA, Toshio ,  INOUE, Hitoshi ,  NISHIMURA, Kunio ,  SUHARA, Yutaka c/o SHOWA ALUMINUM POWDER K.K. ,  OHSHIMA, Satoshi, c/o NATIONAL INST. ,  YUMURA, Motoo, c/o NATIONAL INST.

    IPC分类号： D01F9/127

    CPC分类号： B82Y30/00 ,  D01F9/127

    摘要： A fine carbon fiber having an outer diameter of 1 to 80 nm and an aspect ratio of 10 to 30,000, comprising a hollow center portion and a multi-layer sheath structure of a plurality of carbon layers, the layers forming annular rings, wherein the sheath-forming carbon layers form an incomplete sheath, i.e., the carbon layers are partially broken or disrupted in a longitudinal direction, and the outer diameter of the carbon fiber and/or the diameter of the hollow center portion are not uniform in a longitudinal direction. The carbon fiber is obtained by instantaneously reacting a carrier gas at a high temperature and an organic compound gas kept at a temperature below the decomposition temperature of the transition metal compound and has a conductivity equivalent to that of a conventional vapor phase method and is useful as a filler material in resins, rubbers, paints and the like.

    摘要翻译： 一种外径为1〜80nm，纵横比为10〜30,000的细碳纤维，其包括中空中心部分和多层碳层的多层护套结构，所述层形成环状环，其中所述护套 形成碳层形成不完整的护套，即碳层在纵向上部分断裂或破裂，碳纤维的外径和/或中空中心部分的直径在纵向方向上不均匀。 碳纤维通过使高温下的载气和保持在低于过渡金属化合物的分解温度的温度的有机化合物气体瞬时反应而获得，并且具有与常规气相法相当的导电性，可用作 树脂，橡胶，油漆等中的填充材料。

    Expanded carbon fiber product and composite using the same
    78.
    发明公开
    Expanded carbon fiber product and composite using the same 有权
    Expandierte Kohlenstofffasern und Verbundwerkstoffe unter Verwendung derselben

    公开(公告)号：EP1243676A2

    公开(公告)日：2002-09-25

    申请号：EP02006390.5

    申请日：2002-03-21

    申请人： GSI Creos Corporation ,  Endo, Morinobu

    发明人： Yanagisawa, Takashi, GSI Creos Corporation ,  Endo, Morinobu

    IPC分类号： D01F9/127 ,  C08K7/06

    CPC分类号： B82Y30/00 ,  C08K7/24 ,  D01F9/127 ,  Y10S977/742 ,  Y10T428/249927 ,  Y10T428/24994 ,  Y10T428/2918

    摘要： In an expanded carbon fiber product according to the present invention, a number of hexagonal carbon layers in the shape of a cup having no bottom are stacked. At least part of edges of the hexagonal carbon layers is exposed at an outer surface or inner surface of the expanded carbon fiber product. At least part of gaps between the hexagonal carbon layers is larger than the gaps between the hexagonal carbon layers at the time of vapor growth.

    摘要翻译： 在根据本发明的膨胀碳纤维产品中，堆叠了多个没有底部的杯形状的六角形碳层。 六角形碳层的边缘的至少一部分在膨胀碳纤维制品的外表面或内表面露出。 六方碳层之间的间隙的至少一部分大于气相生长时六方碳层间的间隙。

    Graphite nanofibers and their use
    79.
    发明公开
    Graphite nanofibers and their use 有权
    Graphitnanofaser und deren Verwendung

    公开(公告)号：EP1122344A2

    公开(公告)日：2001-08-08

    申请号：EP01102417.1

    申请日：2001-02-02

    申请人： Nihon Shinku Gijutsu Kabushiki Kaisha

    发明人： Murakami, Hirohiko, Nihon Shinku Gijutsu K. K. ,  Hirakawa, Masaaki, Nihon Shinku Gijutsu K. K. ,  Tanaka, Chiaki, Nihon Shinku Gijutsu K. K.

    IPC分类号： D01F9/127 ,  H01J31/12 ,  H01M4/58

    CPC分类号： H01M4/587 ,  B82Y10/00 ,  B82Y30/00 ,  D01F9/127 ,  H01J1/3048 ,  H01J2201/30469 ,  H01M4/133 ,  H01M4/1393 ,  H01M10/0525 ,  H01M2004/022 ,  Y10S977/939

    摘要： A graphite nanofiber material herein provided has a cylindrical structure in which graphene sheets each having an ice-cream cone-like shape whose tip is cut off are put in layers through catalytic metal particles; or a structure in which small pieces of graphene sheets having a shape adapted for the facial shape of a catalytic metal particle are put on top of each other through the catalytic metal particles. The catalytic metal comprises Fe, Co or an alloy including at least one of these metals. The material can be used for producing an electron-emitting source, a display element, which is designed in such a manner that only a desired portion of a luminous body emits light, a negative electrode carbonaceous material for batteries and a lithium ion secondary battery.

    摘要翻译： 本文提供的石墨纳米纤维材料具有圆柱形结构，其中每个具有切割尖端的冰淇淋锥形状的石墨烯片通过催化金属颗粒层叠; 或其中具有适于催化金属颗粒的面形状的小块石墨烯片的结构通过催化金属颗粒彼此放置在顶部上。 催化金属包括Fe，Co或包含这些金属中的至少一种的合金。 该材料可以用于制造电子发射源，显示元件，其设计成只有发光体的所需部分发光，用于电池的负极碳质材料和锂离子二次电池。

    Process for producing carbon fibrils and reaction apparatus
    80.
    发明公开
    Process for producing carbon fibrils and reaction apparatus 失效
    一种用于生产碳纤维和装置的过程为此

    公开(公告)号：EP0969127A3

    公开(公告)日：2000-02-23

    申请号：EP99114233.2

    申请日：1989-12-18

    申请人： HYPERION CATALYSIS INTERNATIONAL, INC.

    发明人： Mandeville, W. Harry ,  Truesdale, Larry K. ,  Tennent, Howard G.

    IPC分类号： D01F9/127 ,  D01F9/133

    CPC分类号： B82Y30/00 ,  D01F9/1272 ,  D01F9/1275 ,  D01F9/1276 ,  D01F9/1278

    摘要： The present invention relates to a a continuous process for producing carbon fibrils by decomposing a source of carbon at elevated temperatures in contact with a multivalent metal and recovering the fibrils formed thereby comprising the steps of introducing catalyst particles having a size of up to 400 µm (microns) and comprising at least one multivalent transition metal on a particulate substrate into a reactor heated to a temperature of 500°C to 1500°C, and recovering the fibrils formed thereby wherein said metal is present on said substrate as a multiplicity of discontinuous catalytic sites which, at least during fibril formation, have a size of 3,5 to 70 nm (35 to 700 Å) which size is measured by measuring the size of the transition metal particles recovered along with produced fibrils. This invention also relates to a reaction apparatus to be used for carrying out said process.