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    PROCESS FOR PREPARING A TERTIARY ALKYL ORGANIC PEROXIDE
    83.
    发明公开
    PROCESS FOR PREPARING A TERTIARY ALKYL ORGANIC PEROXIDE 审中-公开

    公开(公告)号：EP4385975A1

    公开(公告)日：2024-06-19

    申请号：EP22213902.4

    申请日：2022-12-15

    申请人： Nouryon Chemicals International B.V.

    发明人： VAN DEN BERG, Michel ,  KROSENDIJK, Edgard Everick ,  STEENSMA, Maria

    IPC分类号： C07C407/00 ,  C07C409/16

    CPC分类号： C07C407/00

    摘要： The present disclosure relates to a process for preparing a tertiary alkyl organic peroxides comprising:
    a) in a first condensation stage, reacting a component containing at least one tertiary alcohol group with a compound containing at least one tertiary hydroperoxide function, in the presence of a catalyst and optional co-catalyst, to form a mixture comprising an organic phase comprising the tertiary alkyl organic peroxide and an aqueous phase,
    b) in a dewatering stage, separating the aqueous phase from the organic phase, and
    c) in a second condensation stage, continuing reacting the component containing at least one tertiary alcohol group with the compound containing at least one tertiary hydroperoxide group, in the presence of a catalyst and optional co-catalyst,

    wherein, in the first condensation stage, the mole ratio between the compound containing at least one tertiary hydroperoxide function and the component containing at least one tertiary alcohol group is at least 3:1, and
    wherein no dewatering takes place during the first condensation stage.