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    PROCESS FOR THE MANUFACTURE OF ACETIC ACID
    3.
    发明公开
    PROCESS FOR THE MANUFACTURE OF ACETIC ACID 有权
    VERFAHREN ZUR HERSTELLUNG VONESSIGSÄURE

    公开(公告)号：EP2794542A4

    公开(公告)日：2015-05-27

    申请号：EP12860700

    申请日：2012-12-14

    申请人： LYONDELLBASELL ACETYLS LLC

    发明人： HALLINAN NOEL C ,  HEARN JOHN D ,  PATEL MIRAJ S ,  FITZPATRICK MICHAEL E

    IPC分类号： C07C51/42 ,  C07C51/12 ,  C07C51/48 ,  C07C51/50 ,  C07C53/08

    CPC分类号： C07C51/44 ,  C07C51/12 ,  C07C51/48 ,  C07C51/50 ,  C07C53/08

    摘要： The phase separation in the decanter of a process for producing acetic acid by carbonylating methanol in the presence of a catalyst under low water-high acid conditions is improved by forming a liquid mixture (D) which has a water content of at most 20% by weight, based on the weight of the liquid mixture, and a weight ratio of acetic acid to water of at least 1:1, and partitioning the liquid mixture by providing for an alkane(s) content of D of from 0.1 to 15% by weight, based on the weight of D, to obtain a light, aqueous phase and a heavy, organic phase.

    摘要翻译： 通过在低水 - 高酸条件下在催化剂存在下羰基化甲醇制备乙酸的方法中的滗析器中的相分离通过形成水含量至多为20％的液体混合物（D）而得到改善， 重量，基于液体混合物的重量，以及乙酸与水的重量比至少为1:1，并通过提供0.1至15％的烷烃含量为0.1至15％来分配液体混合物，通过 重量，基于D的重量，以获得轻的，水相和重的有机相。

    ACETIC ACID PRODUCTION PROCESS
    9.
    发明公开
    ACETIC ACID PRODUCTION PROCESS 审中-公开
    VERFAHREN ZUR HERSTELLUNG VONESSIGSÄURE

    公开(公告)号：EP3110785A1

    公开(公告)日：2017-01-04

    申请号：EP15755596.2

    申请日：2015-02-24

    申请人： LyondellBasell Acetyls, LLC

    发明人： HALLINAN, Noel ,  SALISBURY, Brian A. ,  WHITE, Daniel F. ,  RAMAGE, David L.

    IPC分类号： C07C51/15 ,  C07C53/08 ,  C07C51/573

    摘要： Processes for producing acetic acid and determining corrosion therein are described herein. The processes generally include contacting methanol and carbon monoxide in the presence of a liquid reaction medium under carbonylation conditions sufficient to form acetic acid, wherein the liquid reaction medium includes: a carbonylation catalyst selected from rhodium catalysts, iridium catalysts and palladium catalysts; from 1 wt. % to 14 wt. % water; and one or more, in-situ generated derivatives of the one or more additives and combinations thereof; wherein the one or more additives are independently selected from non-benzoyl containing pentavalent phosphine oxides, compound mixtures of at least four phosphine oxides and pentavalent aryl or alkaryl phosphine oxides including one or more benzoyl groups; and recovering acetic acid from the process.

    摘要翻译： 本文描述了生产乙酸和确定腐蚀的方法。 该方法通常包括在足以形成乙酸的羰基化条件下在液体反应介质存在下使甲醇和一氧化碳接触，其中液体反应介质包括：选自铑催化剂，铱催化剂和钯催化剂的羰基化催化剂; 从1重量％ ％至14重量％ ％ 水; 和一种或多种原位产生的一种或多种添加剂及其组合的衍生物; 其中所述一种或多种添加剂独立地选自非苯甲酰基的五价氧化膦，至少四种氧化膦的化合物混合物和包括一个或多个苯甲酰基的五价芳基或烷芳基氧化膦; 并从该方法回收乙酸。

    PROCESS FOR THE MANUFACTURE OF ACETIC ACID
    10.
    发明公开
    PROCESS FOR THE MANUFACTURE OF ACETIC ACID 有权
    制造醋酸的方法

    公开(公告)号：EP2794541A1

    公开(公告)日：2014-10-29

    申请号：EP12859483.5

    申请日：2012-12-19

    申请人： Lyondellbasell Acetyls, LLC

    发明人： HALLINAN, Noel, C ,  HEARN, John, D. ,  FITZPATRICK, Michael, E. ,  PATEL, Miraj, S.

    IPC分类号： C07C51/235 ,  C07C51/50 ,  C07C53/08

    CPC分类号： C07C51/12 ,  C07C51/44 ,  C07C53/08

    摘要： The phase separation in the decanter of a process for producing acetic acid by carbonylating methanol in the presence of a catalyst under low water-high acid conditions is facilitated and expedited by forming a liquid mixture (D) which has a water content of at most 10% by weight, based on the weight of the liquid mixture, an acetic acid content of at least 10% by weight, based on the weight of the liquid mixture, and a weight ratio of methyl iodide to methyl acetate of at least 1.5: 1, and partitioning the liquid mixture at a temperature of from 0 to 35°C.

    摘要翻译： 通过在低水 - 高酸条件下在催化剂存在下使甲醇羰基化来制备乙酸的方法的滗析器中的相分离通过形成具有至多10的水含量的液体混合物（D） 以液体混合物的重量为基准计，以液体混合物的重量为基准计，乙酸含量至少为10重量％，甲基碘与乙酸甲酯的重量比为至少1.5:1 并在0至35℃的温度下分配液体混合物。