利索-全球专利检索

  1. 登录
  2. 注册

搜索结果

348 条记录 (耗时 0.011 秒)

    PROCESS FOR THE PRODUCTION OF HCFC-1233ZD
    1.
    发明公开
    PROCESS FOR THE PRODUCTION OF HCFC-1233ZD 审中-公开

    公开(公告)号：EP4461716A2

    公开(公告)日：2024-11-13

    申请号：EP24201575.8

    申请日：2013-02-11

    申请人： Honeywell International Inc.

    发明人： COTTRELL, Stephen ,  TUNG, Hsueh Sung ,  POKROVSKI, Konstantin A. ,  WANG, Haiyou ,  MERKEL, Daniel

    IPC分类号： C07B61/00

    摘要： A process for the manufacture of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) at commercial scale from the reaction of HCC-240 and HF is disclosed. In one embodiment, HCC-240fa and HF are fed to a reactor operating at high pressure. Several different reactor designs useful in this process include; a stirred-tank reactor (batch and/or continuous flow); a plug flow reactor, a static mixer used as a reactor, at least one of the above reactors operating at high pressure; optionally combined with a distillation column running at a lower pressure; and combinations of the above; and/or with a distillation column. The resulting product stream consisting of 1233zd, HCl, HF, and other byproducts is partially condensed to recover HF by phase separation. The recovered HF phase is recycled to the reactor. The HCl is scrubbed from the vapor stream and recovered as an aqueous solution. The remaining organic components including the desired HCFC-1233zd are scrubbed, dried and distilled to meet commercial product specifications.