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16 条记录 (耗时 0.008 秒)

    Method of making polyamide-imide foams
    1.
    发明公开
    Method of making polyamide-imide foams 失效
    制备聚酰胺酰亚胺的方法

    公开(公告)号：EP0205702A3

    公开(公告)日：1988-04-27

    申请号：EP85307262

    申请日：1985-10-10

    申请人： Gagliani, John ,  Long, John V.

    发明人： Gagliani, John

    IPC分类号： C08G73/14 ,  C08J09/08

    CPC分类号： C08J9/02 ,  C08J2379/08

    摘要： ® A method of making a flexible, flame-resistant polyamide-imide foam comprises reacting an aromatic N-substituted imidocarboxylic acid monoanhydride or an aromatic N,N'-disubstituted bisimidodicarboxylic acid (component A) with an organic diisocyanate (component B) in the presence of a tertiary amine catalyst (C) and water to form a polyamide-imide foam.

    Method of making imide precursor compositions for polyimide coatings and adhesives
    2.
    发明公开
    Method of making imide precursor compositions for polyimide coatings and adhesives 失效
    一种用于制备酰亚胺前体组合物为聚酰亚胺涂层和粘合剂的过程。

    公开(公告)号：EP0191213A2

    公开(公告)日：1986-08-20

    申请号：EP85303097.1

    申请日：1985-05-01

    申请人： Gagliani, John ,  Long, John V.

    发明人： Gagliani, John ,  Long, John V.

    IPC分类号： C08G73/14 ,  C09D3/70 ,  C09J3/16 ,  C07D207/404 ,  C07D209/48

    CPC分类号： C08G73/1007 ,  C08G73/1028 ,  C08G73/1032

    摘要： A method of making an imide resin composition comprises:

    (a) mixing at least one lactam and/or amino acid (component A) with at least one aromatic dianhydride (component B) in a mole ratio of A:B of up to 10:1,
    (b) mixing a solvent with the mixture from step (a) and heating the resulting mixture, and
    (c) mixing at least one diamine (component C) with the product of step (b) to give a solution of the imide precursor which forms a polyimide upon heating.

    摘要翻译： 使得在酰亚胺树脂组合物的方法包括：（a）将至少一种内酰胺和/或氨基酸（组分A）与A的摩尔比至少一种芳族四羧酸二酐（组分B）：高达10的B： 1，（b）将溶剂与来自步骤将混合物（a）和加热得到的混合物，和（c）与步骤的产物混合至少一种二胺（组分C）（b）中得到的酰亚胺的溶液 其前体形成在加热时的聚酰亚胺。

    Method of making imide precursor compositions for polimide adhesives and matric materials
    5.
    发明公开
    Method of making imide precursor compositions for polimide adhesives and matric materials 失效
    Verfahren zur Herstellung vonImidvorläufer-ZusammensetzungenfürPolyimidklebstoffe und Matrixmaterialien。

    公开(公告)号：EP0198973A2

    公开(公告)日：1986-10-29

    申请号：EP85304777.7

    申请日：1985-07-04

    申请人： Long, John V. ,  Gagliani, John

    发明人： Long, John V. ,  Gagliani, John

    IPC分类号： C08G73/10 ,  C08J5/24 ,  C09J3/16

    CPC分类号： C08G73/1032 ,  C08G73/1007 ,  C08G73/1028 ,  C09J179/08 ,  Y10T428/31721

    摘要： A method of making an imide precursor composition comprises:

    (a) mixing a lactam (component A) with a tetracarboxylic acid dianhydride component (component B) comprising at least 50 mole % of 1, 2, 3, 4-butanetetra-carboxylic acid dianhydride in a mole ratio of A:B of from 0.1:1 to 10:1 to form an N, N-disubstituted bisimide dicarboxylic acid,
    (b) dissolving the product of step (a) in an inert solvent, and
    (c) mixing at least one aromatic diamine (component C) with the solution from step (b) to give a solution of an imide precursor which forms a polyimide on heating.

    摘要翻译： 制备酰亚胺前体组合物的方法包括：（a）将内酰胺（组分A）与四羧酸二酐组分（组分B）混合，所述四羧酸二酐组分包含至少50摩尔％的1,2,3,4-丁四
    胺 二酸酐的摩尔比为A：B为0.1:1至10:1，以形成N，N-二取代双酰亚胺二羧酸，（b）将步骤（a）的产物溶解在惰性溶剂中，和（ c）将至少一种芳族二胺（组分C）与步骤（b）的溶液混合，得到加热时形成聚酰亚胺的酰亚胺前体溶液。

    Method of making polyimide foam and precursor therefor
    6.
    发明公开
    Method of making polyimide foam and precursor therefor 失效
    制备聚酰胺泡沫及其前体的方法

    公开(公告)号：EP0141481A3

    公开(公告)日：1986-02-12

    申请号：EP84302921

    申请日：1984-05-01

    申请人： Gagliani, John ,  Long, John V.

    发明人： Gagliani, John

    IPC分类号： C08G73/10 ,  C08G73/14 ,  C08J09/12 ,  C08J09/02

    CPC分类号： C08J9/34 ,  C08G73/1028 ,  C08J9/02 ,  C08J2379/08 ,  C08L79/08

    摘要： Methods of making low density modified polyimide! polyimide-amide foams and the resulting compositions. An N-substituted aliphatic imide is prepared by reacting a suitable aromatic dianhydride with a suitable oxime. A polyimide forming material is prepared by dissolving the N-substituted aliphatic imide in an esterifying solvent, then adding a suitable aromatic diamine. This material is dried to a powder. A suitable hydrated compound which is stable up to at least about 100°C. is mixed with the powder. A foam is then produced by heating the material to reaction temperature for a period sufficient to produce a stable foam. The material melts, then spontaneously expands into a foam which becomes self supporting and cures to a resilient flexible foam. The addition of the hydrated compound is found to result in an exceptionally low density foam. Depending upon heating conditions, a polyimide, polyimide- amide or mixture thereof may be produced, resulting in foams having selectively variable physical properties.

    Production of macro balloon structures
    8.
    发明公开
    Production of macro balloon structures 失效
    Herstellung von Strukturen ausMakrobläschen。

    公开(公告)号：EP0116759A1

    公开(公告)日：1984-08-29

    申请号：EP83307241.6

    申请日：1983-11-28

    申请人： Gagliani, John ,  Long, John V.

    发明人： Gagliani, John ,  Long, John V.

    IPC分类号： C08J9/22 ,  C08G73/14 ,  C08G73/10 ,  C08L79/08

    CPC分类号： C08J9/32 ,  B32B5/18 ,  C08G73/1028 ,  C08J9/02 ,  C08J9/16 ,  C08J9/236 ,  C08J2379/08 ,  Y10S264/06 ,  Y10S521/915

    摘要： A method of making light weight flame resistant structures from bonded polyimide macroballoons. An aromatic tetracarboxylic acid dianhydride is reacted with a lactam to produce an N-substituted imide, which is then esterfied with a reactive solvent. At least one diamine is added. The resulting liquid is dried and the dry residue is reduced to an uniform powder having particles with diameters generally in the 0.5 to 10mm. range. The powder expands when heated to a temperature in the range of about 90 to 150°C for a suitable period. Closed cell "macroballoons" having average diameters between about 0.4 and 15mm. result. The macroballoons are bonded together with a very small amount of a suitable resin.

    摘要翻译： 一种从粘合的聚酰亚胺宏观球体制造轻质阻燃结构的方法。 使芳族四羧酸二酐与内酰胺反应，生成N-取代的酰亚胺，然后用活性溶剂进行酯化。 加入至少一种二胺。 将所得液体干燥并将干燥残余物还原成具有通常为0.5至10mm直径的颗粒的均匀粉末。 范围。 当加热到约90至150℃的温度一段合适的时间时，粉末膨胀。 具有约0.4和15mm之间的平均直径的闭孔“宏观气球”。 结果。 宏观气球用非常少量的合适的树脂粘合在一起。

    Closed cell polyimide foams and methods of making same
    9.
    发明公开
    Closed cell polyimide foams and methods of making same 失效
    闭孔聚酰亚胺泡沫材料及其制备方法。

    公开(公告)号：EP0107262A1

    公开(公告)日：1984-05-02

    申请号：EP83301628.0

    申请日：1983-03-23

    申请人： Gagliani, John ,  Long, John V.

    发明人： Gagliani, John ,  Long, John V.

    IPC分类号： C08G73/10 ,  C08J9/02 ,  C08J9/32 ,  C08L79/08 ,  B29C67/22

    CPC分类号： B32B5/20 ,  B32B3/12 ,  B32B5/18 ,  B32B2266/08 ,  B32B2305/024 ,  B32B2305/30 ,  B32B2307/3065 ,  C08G73/1028 ,  C08J9/02 ,  C08J9/16 ,  C08J9/236 ,  C08J2379/08 ,  Y10T428/1234

    摘要： @ A high temperature and flame resistant closed cell polyimide foam material and methods of making the foam. An aromatic tetracarboxylic acid dianhydride is reacted with an oxomine to produce an N-substituted imide, which is then esterified with a suitable alcohol. The resulting liquid is dried and the dry residue is reduced to a uniform powder having particles with diameters generally in the 0.5 to 10 mm range. The powder is preferably further dried, either before or after final size reduction, in a moderate vaccum at moderate temperature to remove any excess residual alcohol. The powder spontaneously expands to form a closed cell foam when heated to a temperature in the range of about 90 to 150°C for a suitable period. When the powder is expanded in a closed mold, a well consolidated, uniform, closed cell foam product results. When expanded in an unrestricted manner, closed cell "macroballoons" having average diameters between about 0.4 and 15 mm result. The closed cell foam produced has excellent flexibility and resistance to heat and flame, and does not shrink appreciably when exposed to flame.