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    OMEGA 3 CONCENTRATE
    3.
    发明公开
    OMEGA 3 CONCENTRATE 审中-公开
    OMEGA-3-KONZENTRAT

    公开(公告)号：EP2659780A2

    公开(公告)日：2013-11-06

    申请号：EP11817504.1

    申请日：2011-12-25

    申请人： Golden Omega S.A.

    发明人： SEPÚLVEDA REYES, Juvenal Antonio ,  BERRIOS CORNEJO, Miriam Rosa ,  FUENZALIDA DÍAZ, Miguel Ángel ,  MARKOVITS ROJAS, Alejandro ,  HARTING GLADE, Thomas Francis

    IPC分类号： A23D9/00 ,  C11B1/10 ,  C11B3/00

    CPC分类号： C11B3/001 ,  A23D9/00 ,  C11B1/10 ,  C11C1/08 ,  C11C1/10 ,  C11C3/003

    摘要： An efficient and simple process to obtain a concentrate that comprising over 80% in weight of ethyl esters of ω-3 fatty acids based on a composition of matter that contains esters of ω-3 fatty acids or free ω-3 fatty acids that comprises the steps of:
    a) contacting the composition of matter with ethanol of at least 96% in weight and a hydroxide of an alkali metal at a temperature between 60 and 200 °C to form a liquid mixture comprising alkaline salts of fatty acids;
    b) cooling the liquid mixture to a temperature between soft and -20 °C to form a solid phase and a liquid phase and separate the liquid phase from the solid phase;
    c) contacting the separated liquid phase of step b) with an acid to form an acidified mixture with a water content under 10%, where the mixture consists of a solid phase that includes the alkali metal salt of the acid and a liquid phase comprising ω-3 fatty acids;
    d) heating the mixture of step c) between 50 to 150 °C in the presence of an esterification catalyst to form a mixture comprising ethyl esters of ω-3 fatty acids;
    e) contacting the mixture of stage d) with an alkali to form a neutralized mixture;
    f) distilling the neutralized mixture to obtain a distillate that includes over 80% in weight of ethyl esters of ω-3 fatty acids.

    摘要翻译： 基于含有É-3脂肪酸酯或游离É-3脂肪酸的物质的组成，获得含有超过80重量％的É-3脂肪酸乙酯的浓缩物的有效和简单的方法，其包含 步骤：a）将物质组合物与至少96％重量的乙醇和碱金属氢氧化物在60至200℃之间的温度下接触以形成包含脂肪酸碱盐的液体混合物; b）将液体混合物冷却至软和-20℃之间的温度以形成固相和液相，并将液相与固相分离; c）使步骤b）的分离的液相与酸接触以形成水含量低于10％的酸化混合物，其中混合物由包含酸的碱金属盐的固相和包含É -3脂肪酸; d）在酯化催化剂存在下将步骤c）的混合物加热至50-150℃以形成包含É-3脂肪酸乙酯的混合物; e）使阶段d）的混合物与碱反应以形成中和的混合物; f）蒸馏中和的混合物以获得包含超过80重量％的É-3脂肪酸乙酯的馏出物。