公开(公告)号：EP0848286A1

公开(公告)日：1998-06-17

申请号：EP97203834.3

申请日：1997-12-06

申请人： AGFA-GEVAERT N.V.

发明人： Emmers, Sabine ,  Horsten, Bartholomeus ,  Geuens, Ingrid ,  Gilliams, Yvan ,  Bellens, André ,  Bollen, Dirk ,  Hoogmartens, Ivan

IPC分类号： G03C1/498 ,  C07C51/41 ,  B41M5/32

CPC分类号： G03C1/49809 ,  C07C51/412 ,  G03C1/498 ,  G03C1/4989 ,  G03C2001/0157 ,  G03C2001/7635 ,  G03C2200/43 ,  C07C53/126

摘要： A recording material comprising a support and a thermosensitive element comprising silver behenate, an organic reducing agent therefor in thermal working relationship therewith and a binder, characterized in that the silver behenate is not associated with mercury and/or lead ions and when the recording material is irradiated with a copper Kα 1 X-ray source the ratio, normalized to a quantity of silver in the recording material of 1g per m 2 thereof, of the sum of the peak heights of the X-ray diffraction lines attributable to silver behenate at Bragg angles, 2Θ, of 6.01°, 7.56°, 9.12°, 10.66°, 12.12° and 13.62° to the sum of the peak heights of the X-ray diffraction lines at Bragg angles, 2Θ, of 25.60°, 35.16° and 43.40° of NIST standard 1976, rhombohedral Al 2 O 3 , determined with the same X-ray diffractometer in the same state of adjustment, is greater than 0.85; production processes for particles of substantially light-insensitive organic silver salt comprising silver behenate with these X-ray characteristics in the presence and substantial absence of organic solvent.

摘要翻译： 在与热的工作关系存在和粘合剂，其包括载体和热敏元件，包括山嵛酸银，有机还原剂的用于其的记录材料，其特征做了山嵛酸银不与汞和/或铅离子，并当记录材料是相关联 用铜Kα阿尔法1的X射线源的比率，归一化到银的每米1g的记录材料的量照射<2>体，在X射线衍射线的峰高度之和的属性能够银 山嵛酸在布喇格角，6点01°，7时56°，12.09°，10.66°，12.12°，13.62°〜X射线在布拉格衍射角线，2 THETA的峰值高度之和的2 THETA，25.60° ，35.16°和43.40°NIST标准1976，菱面体晶氧化铝，确定性与调整的相同的状态相同的X射线衍射仪开采，大于0.85的; 生产工艺，其包括在存在合成透视特性和基本上不存在有机溶剂的山萮酸银基本上光不敏感的有机银盐的颗粒。

公开(公告)号：EP0962815A1

公开(公告)日：1999-12-08

申请号：EP99201712.9

申请日：1999-05-25

申请人： AGFA-GEVAERT N.V.

发明人： Geuens, Ingrid ,  Gilliams, Yvan ,  Bollen, Dirk ,  Hoogmartens, Yvan ,  Bellens, André

IPC分类号： G03C1/498 ,  C07C51/41

CPC分类号： G03C1/49809 ,  G03C1/4989

摘要： A recording material comprising a support and a thermosensitive element comprising silver palmitate, an organic reducing agent therefor in thermal working relationship therewith and a binder, characterized in that the silver palmitate is not associated with mercury and/or lead ions and when the recording material is irradiated with a copper Kα 1 X-ray source the ratio of the sum of the peak heights of the X-ray diffraction lines attributable to silver palmitate at Bragg angles, 2Θ, of 4.01°, 6.049°, 8.031°, 10.06°, 12.08° and 14.09° to the sum of the peak heights of the X-ray diffraction lines at Bragg angles, 2Θ, of 25.60°, 35.16° and 43.40° of NIST standard 1976, rhombohedral Al 2 O 3 , determined with the same X-ray diffractometer in the same state of adjustment on a sample of the recording material and a sample of the NIST standard 1976 cut to fit a sample holder of the X-ray diffractometer, divided by the square root of the quantity of silver in the recording material, expressed in g per m 2 , is greater than 3.09 m/g 0.5 ; and a process for producing particles of substantially light-insensitive organic silver salt comprising silver palmitate with these X-ray characteristics in the substantial absence of organic solvent.

摘要翻译： 包括载体和热敏元件中的热的工作关系包括在有机还原剂银，棕榈酸为此那里与和粘合剂的记录材料，其特征做了银，棕榈酸不与汞和/或铅离子，并当记录材料是相关联 照射用铜Kα阿尔法1的X射线源的X射线衍射线的峰高度之和的比例属性能够银，棕榈酸在布喇格角，4:01 DEG，6049°，8031°，10.6 DEG 2 THETA ，12.08°和14.09°处的布拉格角，2 THETA的X射线衍射线的峰高度之和，的25.60°，35.16°和NIST 43.40°标准1976，菱面体晶氧化铝，确定性开采具有相同X- 射线衍射仪在调整的相同的状态在记录材料的样品，并NIST标准1976切割的样品，以适应X射线衍射仪的样品保持器，通过的数量的平方根除以 银在记录材料上，在每m <2> g表示，大于3:09平方米/克<0.5>; 和用于基本上制造过程粒子的光不敏感的有机银盐包括银，棕榈酸与在基本上不存在有机溶剂的合成X射线的特性。

公开(公告)号：EP0962814B1

公开(公告)日：2003-01-29

申请号：EP99201626.1

申请日：1999-05-25

申请人： AGFA-GEVAERT

发明人： Geuens, Ingrid ,  Gilliams, Yvan ,  Bollen, Dirk ,  Hoogmartens, Yvan ,  Bellens, André

IPC分类号： G03C1/498 ,  C07C51/41

CPC分类号： G03C1/49809 ,  C07C51/412 ,  G03C1/49872 ,  G03C2001/7635 ,  G03C2007/3025 ,  G03C2200/43 ,  C07C53/126

摘要： A recording material comprising a support and a thermosensitive element containing silver stearate, an organic reducing agent therefor in thermal working relationship therewith and a binder, characterized in that the silver stearate is not associated with mercury and/or lead ions and when the recording material is irradiated with a copper K alpha 1 X-ray source the ratio of the sum of the peak heights of the X-ray diffraction lines attributable to silver stearate at Bragg angles, 2 THETA , of 2 THETA , of 3.62 DEG , 5.45 DEG , 7.30 DEG , 9.04 DEG , 10.97 DEG and 12.71 DEG to the sum of the peak heights of the X-ray diffraction lines at Bragg angles, 2 THETA , of 25.60 DEG , 35.16 DEG and 43.40 DEG of NIST standard 1976, rhombohedral Al2O3, determined with the same X-ray diffractometer in the same state of adjustment on a sample of the recording material and a sample of the NIST standard 1976 cut to fit a sample holder of the X-ray diffractometer, divided by the square root of the quantity of silver in the recording material, expressed in g per m , is greater than 2.2m/g ; and a process for producing particles of substantially light-insensitive organic silver salt comprising silver stearate with these X-ray characteristics in the substantial absence of organic solvent.

公开(公告)号：EP0848286B1

公开(公告)日：2005-04-06

申请号：EP97203834.3

申请日：1997-12-06

申请人： AGFA-GEVAERT

发明人： Emmers, Sabine ,  Horsten, Bartholomeus ,  Geuens, Ingrid ,  Gilliams, Yvan ,  Bellens, André ,  Bollen, Dirk ,  Hoogmartens, Ivan

IPC分类号： G03C1/498 ,  C07C51/41 ,  B41M5/32

CPC分类号： G03C1/49809 ,  C07C51/412 ,  G03C1/498 ,  G03C1/4989 ,  G03C2001/0157 ,  G03C2001/7635 ,  G03C2200/43 ,  C07C53/126

摘要： A recording material comprising a support and a thermosensitive element comprising silver behenate, an organic reducing agent therefor in thermal working relationship therewith and a binder, characterized in that the silver behenate is not associated with mercury and/or lead ions and when the recording material is irradiated with a copper K alpha 1 X-ray source the ratio, normalized to a quantity of silver in the recording material of 1g per m thereof, of the sum of the peak heights of the X-ray diffraction lines attributable to silver behenate at Bragg angles, 2 THETA , of 6.01 DEG , 7.56 DEG , 9.12 DEG , 10.66 DEG , 12.12 DEG and 13.62 DEG to the sum of the peak heights of the X-ray diffraction lines at Bragg angles, 2 THETA , of 25.60 DEG , 35.16 DEG and 43.40 DEG of NIST standard 1976, rhombohedral Al2O3, determined with the same X-ray diffractometer in the same state of adjustment, is greater than 0.85; production processes for particles of substantially light-insensitive organic silver salt comprising silver behenate with these X-ray characteristics in the presence and substantial absence of organic solvent.

公开(公告)号：EP0962815B1

公开(公告)日：2003-01-15

申请号：EP99201712.9

申请日：1999-05-25

申请人： AGFA-GEVAERT

发明人： Geuens, Ingrid ,  Gilliams, Yvan ,  Bollen, Dirk ,  Hoogmartens, Yvan ,  Bellens, André

IPC分类号： G03C1/498 ,  C07C51/41

CPC分类号： G03C1/49809 ,  G03C1/4989

公开(公告)号：EP0962814A1

公开(公告)日：1999-12-08

申请号：EP99201626.1

申请日：1999-05-25

申请人： AGFA-GEVAERT N.V.

发明人： Geuens, Ingrid ,  Gilliams, Yvan ,  Bollen, Dirk ,  Hoogmartens, Yvan ,  Bellens, André

IPC分类号： G03C1/498 ,  C07C51/41

CPC分类号： G03C1/49809 ,  C07C51/412 ,  G03C1/49872 ,  G03C2001/7635 ,  G03C2007/3025 ,  G03C2200/43 ,  C07C53/126

摘要： A recording material comprising a support and a thermosensitive element containing silver stearate, an organic reducing agent therefor in thermal working relationship therewith and a binder, characterized in that the silver stearate is not associated with mercury and/or lead ions and when the recording material is irradiated with a copper Kα 1 X-ray source the ratio of the sum of the peak heights of the X-ray diffraction lines attributable to silver stearate at Bragg angles, 2Θ, of 2Θ, of 3.62°, 5.45°, 7.30°, 9.04°, 10.97° and 12.71° to the sum of the peak heights of the X-ray diffraction lines at Bragg angles, 2Θ, of 25.60°, 35.16° and 43.40° of NIST standard 1976, rhombohedral Al 2 O 3 , determined with the same X-ray diffractometer in the same state of adjustment on a sample of the recording material and a sample of the NIST standard 1976 cut to fit a sample holder of the X-ray diffractometer, divided by the square root of the quantity of silver in the recording material, expressed in g per m 2 , is greater than 2.2m/g 0.5 ; and a process for producing particles of substantially light-insensitive organic silver salt comprising silver stearate with these X-ray characteristics in the substantial absence of organic solvent.

摘要翻译： 包含载体和在热的工作关系包含在有机还原剂硬脂酸银为此有有热敏元件和粘合剂的记录材料，其特征做了硬脂酸银不与汞和/或铅离子，并当记录材料是相关联 用铜Kα阿尔法1的X射线源的X射线衍射线的峰高度之和的比率在布拉格属性能够硬脂酸银角，2 THETA，2 THETA的，3.62 DEG的，5点45 DEG，7.30照射 DEG，9点04°，10.97°，12.71°〜X射线在布拉格衍射线角，2 THETA的峰值高度之和，的25.60°，35.16°和NIST 43.40°标准1976，菱面体晶氧化铝，确定性开采与 在调整的相同的状态相同的X射线衍射装置在记录材料的样品，并NIST标准1976切割的样品，以适应X射线衍射仪的样品保持器，通过定量的平方根除以 在记录材料上，在每m <2> g表示银，两者均，比2.2米/克<0.5>更大; 和用于基本上制造过程的光不敏感的有机银盐颗粒包含具有在基本上不存在有机溶剂的合成X射线特征银，硬脂酸银。