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    Tertiary amine catalysts for polyurethanes
    1.
    发明公开
    Tertiary amine catalysts for polyurethanes 失效
    TertiäreAmine-Katalysatorenfür聚氨酯。

    公开(公告)号：EP0456194A2

    公开(公告)日：1991-11-13

    申请号：EP91107416.9

    申请日：1991-05-07

    申请人： AIR PRODUCTS AND CHEMICALS, INC.

    发明人： Casey, Jeremiah Patrick ,  Carr, Richard van Court ,  Wasilczyk, George James ,  Petrella, Robert Gabriel

    IPC分类号： C08G18/18 ,  C08G18/20 ,  C07C217/08 ,  C07D295/088 ,  B01J31/02

    CPC分类号： C07D295/088 ,  C07C217/08 ,  C08G18/1825 ,  C08G18/1833 ,  C08G18/2009

    摘要： The invention pertains to tertiary amines used as catalysts for the preparation of polyurethane foams prepared via the catalytic reaction of a polyisocyanate with a polyol in the presence of blowing agents, etc. The tertiary amine catalysts are prepared by reacting an olefinic nitrile with aliphatic polyol having at least secondary hydroxyl functionality in a ratio less than stoichiometric for providing cyanoalkylated polyol having residual hydroxyl functionality. The resulting cyanoalkylated polyol then is reacted with a secondary amine under conditions for effective reductive alkylation.
    The tertiary amine catalysts, because of residual secondary hydroxyl functionality, provide for uniform dispersion within a polyurethane formulation; they provide for additional or extended pot life in polyurethane formulations at temperatures below reaction condition, and they are bound by reaction on cure.

    摘要翻译： 本发明涉及用于制备通过多异氰酸酯与多元醇在发泡剂等的催化反应制备的聚氨酯泡沫的催化剂的叔胺。叔胺催化剂是通过使烯烃腈与具有 至少具有小于化学计量比的仲羟基官能团以提供具有残余羟基官能团的氰基烷基化多元醇。 然后将所得的氰基烷基化多元醇与仲胺在有效还原烷基化的条件下反应。 由于残留的仲羟基官能团，叔胺催化剂在聚氨酯配方中提供均匀的分散体; 它们在低于反应条件的温度下在聚氨酯配方中提供额外的或延长的适用期，并且它们通过固化反应结合。

    Coproduction of propanediamine and alkylated aminopropylamines
    3.
    发明公开
    Coproduction of propanediamine and alkylated aminopropylamines 失效
    丙酰胺和烷基氨基丙烯酸的共聚

    公开(公告)号：EP0391349A3

    公开(公告)日：1991-05-22

    申请号：EP90106369.3

    申请日：1990-04-03

    申请人： AIR PRODUCTS AND CHEMICALS, INC.

    发明人： Carr, Richard van Court

    IPC分类号： C07C209/48

    CPC分类号： C07C255/24 ,  C07C209/48

    摘要： This invention relates to a process for the coproduction of propanediamines and alkylated aminopropanediamines. The process contemplates an initial cyanoethylation of ammonia under conditions for producing aminopropionitrile and modest levels of iminobispropionitrile. After separation of the iminobispropionitrile from the aminopropionitrile, the process involves the catalytic reductive alkylation of the iminobispropionitrile by reaction with an aldehyde in the presence of hydrogen to form the alkylated iminobispropionitrile followed by the catalytic hydrogenation of the nitrile group in aminopropionnitrile and iminobispropionitrile to the amine.

    Coproduction of propanediamine and alkylated aminopropylamines
    4.
    发明公开
    Coproduction of propanediamine and alkylated aminopropylamines 失效
    Koproduktion von Propandiamin und alkylierten Aminopropylaminen。

    公开(公告)号：EP0391349A2

    公开(公告)日：1990-10-10

    申请号：EP90106369.3

    申请日：1990-04-03

    申请人： AIR PRODUCTS AND CHEMICALS, INC.

    发明人： Carr, Richard van Court

    IPC分类号： C07C209/48

    CPC分类号： C07C255/24 ,  C07C209/48

    摘要： This invention relates to a process for the coproduction of propanediamines and alkylated aminopropanediamines. The process contemplates an initial cyanoethylation of ammonia under conditions for producing aminopropionitrile and modest levels of iminobispropionitrile. After separation of the iminobispropionitrile from the aminopropionitrile, the process involves the catalytic reductive alkylation of the iminobispropionitrile by reaction with an aldehyde in the presence of hydrogen to form the alkylated iminobispropionitrile followed by the catalytic hydrogenation of the nitrile group in aminopropionnitrile and iminobispropionitrile to the amine.

    摘要翻译： 本发明涉及丙二胺和烷基化氨基丙二胺的共生产方法。 该方法考虑了用于生产氨基丙腈和适度水平的亚氨基二甲腈的条件下氨的初始氰基乙基化。 在亚氨基二甲腈从氨基丙腈分离后，该方法涉及通过在氢气存在下与醛反应形成亚烷基二亚丙腈的亚氨基二甲腈的催化还原烷基化，然后将氨基丙腈和亚氨基双丙腈中的腈基催化氢化为胺 。