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公开(公告)号：EP1406832B1
公开(公告)日：2006-08-09
申请号：EP02745423.0
申请日：2002-07-02
发明人： WOSTBROCK, Karl-Heinz , THIEL, Joachim , KRÜGER, Heinz , STRÖFER, Eckhard , WEBER, Markus , GERBER, Bernd , RUMPF, Bernd , SACHWEH, Bernd , KERTH, Steffen
CPC分类号： C01B21/1445 , B01D3/16 , B01J19/30 , B01J19/32 , B01J2219/30215 , B01J2219/30466 , B01J2219/3221 , B01J2219/32483 , Y10S203/20 , Y10S261/72
摘要： The invention relates to a method for the production of a salt-free aqueous hydroxylamine solution by distilling an aqueous solution of an hydroxylammonium salt and a base in a plate column having at least two mechanical plates. The invention is characterized in that packings or structured packings are placed above at least one of the plates of the plate column along the cross section of said column.
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公开(公告)号：EP1406832A1
公开(公告)日：2004-04-14
申请号：EP02745423.0
申请日：2002-07-02
发明人： WOSTBROCK, Karl-Heinz , THIEL, Joachim , KRÜGER, Heinz , STRÖFER, Eckhard , WEBER, Markus , GERBER, Bernd , RUMPF, Bernd , SACHWEH, Bernd , KERTH, Steffen
CPC分类号： C01B21/1445 , B01D3/16 , B01J19/30 , B01J19/32 , B01J2219/30215 , B01J2219/30466 , B01J2219/3221 , B01J2219/32483 , Y10S203/20 , Y10S261/72
摘要： The invention relates to a method for the production of a salt-free aqueous hydroxylamine solution by distilling an aqueous solution of an hydroxylammonium salt and a base in a plate column having at least two mechanical plates. The invention is characterized in that packings or structured packings are placed above at least one of the plates of the plate column along the cross section of said column.
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公开(公告)号：EP1409401B1
公开(公告)日：2004-12-15
申请号：EP02753076.5
申请日：2002-07-02
IPC分类号： C01B21/14
CPC分类号： C01B21/1445 , Y10S203/20
摘要： The invention relates to a method for producing an aqueous hydroxylamine solution that is devoid of salt by reacting an aqueous solution of a hydroxylammonium salt with a base to obtain a mixture and by separating an aqueous hydroxylamine solution devoid of salt by distillation from said mixture. The method is characterised in that an aqueous solution of a mixture of NaOH and KOH with a molar ratio of Na+: K+ in the region of between 70: 30 and 95: 5 and a total concentration of Na+ and K+ in the region of between 0.1 and 10 m/m % (in relation to the total quantity of the mixture) is used as the base.
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4.发明授权VERFAHREN ZUR HERSTELLUNG EINER SALZFREIEN, WÄSSRIGEN HYDROXYLAMINLÖSUNG 有权VERFAHREN ZUR HERSTELLUNG EINER SALZFREIEN，WÄSSRIGENHYDROXYLAMINLÖSUNG
公开(公告)号：EP1406833B1
公开(公告)日：2004-11-17
申请号：EP02767163.5
申请日：2002-07-02
发明人： WOSTBROCK, Karl-Heinz , THIEL, Joachim , KRÜGER, Heinz , STRÖFER, Eckhard , WEBER, Markus , GERBER, Bernd , RUMPF, Bernd , SACHWEH, Bernd , KERTH, Steffen
CPC分类号： B01J19/30 , B01D3/16 , B01J19/32 , B01J2219/30215 , B01J2219/30466 , B01J2219/3221 , B01J2219/32483 , C01B21/1445 , Y10S203/11 , Y10S261/72
摘要： The invention relates to a method for producing a highly pure, aqueous hydroxylamine solution by distilling an aqueous solution, devoid of salt, of a hydroxyl ammonium salt in a plate column comprising at least two mechanical plates. Said method is characterised in that packing bodies are arranged between at least two plates of the plate column over the cross-section of said column.
摘要翻译： 本发明涉及通过在包含至少两个机械板的板式塔中蒸馏羟基铵盐的无盐水溶液来生产高纯羟胺水溶液的方法。 所述方法的特征在于，在所述塔的横截面上在所述板塔的至少两个板之间布置包装体。
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5.发明公开VERFAHREN ZUR HERSTELLUNG EINER SALZFREIEN, WAESSRIGEN HYDROXYLAMINLOESUNG 有权VERFAHREN ZUR HERSTELLUNG EINER SALZFREIEN，WAESSRIGEN HYDROXYLAMINLOESUNG
公开(公告)号：EP1409401A1
公开(公告)日：2004-04-21
申请号：EP02753076.5
申请日：2002-07-02
IPC分类号： C01B21/14
CPC分类号： C01B21/1445 , Y10S203/20
摘要： The invention relates to a method for producing an aqueous hydroxylamine solution that is devoid of salt by reacting an aqueous solution of a hydroxylammonium salt with a base to obtain a mixture and by separating an aqueous hydroxylamine solution devoid of salt by distillation from said mixture. The method is characterised in that an aqueous solution of a mixture of NaOH and KOH with a molar ratio of Na+: K+ in the region of between 70: 30 and 95: 5 and a total concentration of Na+ and K+ in the region of between 0.1 and 10 m/m % (in relation to the total quantity of the mixture) is used as the base.
摘要翻译： 本发明涉及通过羟基铵盐的水溶液与碱反应以获得混合物并通过从所述混合物中分离无盐蒸馏水溶液来制备不含盐的羟胺水溶液的方法。 该方法的特征在于NaOH和KOH的混合物的水溶液，其中Na +：K +的摩尔比在70:30和95:5之间的区域内，并且Na +和K +的总浓度在0.1 和10m / m％（相对于混合物的总量）用作基础。
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公开(公告)号：EP1406833A1
公开(公告)日：2004-04-14
申请号：EP02767163.5
申请日：2002-07-02
发明人： WOSTBROCK, Karl-Heinz , THIEL, Joachim , KRÜGER, Heinz , STRÖFER, Eckhard , WEBER, Markus , GERBER, Bernd , RUMPF, Bernd , SACHWEH, Bernd , KERTH, Steffen
CPC分类号： B01J19/30 , B01D3/16 , B01J19/32 , B01J2219/30215 , B01J2219/30466 , B01J2219/3221 , B01J2219/32483 , C01B21/1445 , Y10S203/11 , Y10S261/72
摘要： The invention relates to a method for producing a highly pure, aqueous hydroxylamine solution by distilling an aqueous solution, devoid of salt, of a hydroxyl ammonium salt in a plate column comprising at least two mechanical plates. Said method is characterised in that packing bodies are arranged between at least two plates of the plate column over the cross-section of said column.
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