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1.发明公开
公开(公告)号：EP2702027A1
公开(公告)日：2014-03-05
申请号：EP12720736.3
申请日：2012-04-26
发明人： LEE, David , OROSCO, Adam , RIBEIRO, Claudio , WARNER, R. Jay , DECK, Robert Alan , DUFF, Emily , JOHNSTON, Victor J.
IPC分类号： C07C29/149 , C07C29/88
CPC分类号： C07C29/88 , C07C29/149 , C07C67/08 , C07C31/08 , C07C69/14
摘要： A process for recovering ethanol obtained from the hydrogenation of acetic acid. The crude ethanol product is separated in a column to produce a distillate stream comprising acetaldehyde and ethyl acetate and a residue stream comprising ethanol, acetic acid, ethyl acetate and water. Unreacted acetic acid can be reduced or removed through configurations of esterification secondary reactors. The ethanol product is recovered from the residue stream.
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公开(公告)号：EP2590919A1
公开(公告)日：2013-05-15
申请号：EP11738098.0
申请日：2011-07-07
发明人： JOHNSTON, Victor, J. , LEE, David , OROSCO, Adam , SARAGER, Lincoln , HALE, Trinity , WOLLRAB, Radmila
IPC分类号： C07C29/149 , C07C29/80 , C07C31/08
CPC分类号： C07C29/149 , C07C29/76 , C07C29/80 , C07C31/08
摘要： Recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid using various combinations of membranes and/or distillation columns.
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公开(公告)号：EP2702019A1
公开(公告)日：2014-03-05
申请号：EP11793543.7
申请日：2011-11-09
发明人： LEE, David , OROSCO, Adam , POWELL, Nathan , SALADO, Manuel , SARAGER, Lincoln , WARNER, R. Jay , HALE, Trinity , WOLLRAB, Radmila , JOHNSTON, Victor J.
IPC分类号： C07C29/149 , C07C29/80 , C07C31/08 , C07C51/12 , C07C53/08
CPC分类号： C07C29/149 , C07C29/80 , C07C51/12 , C07C31/08 , C07C53/12
摘要： This invention relates to a process for removing water from an alcohol mixture, such as an ethanol mixture, to produce ethanol by hydrogenating acetic acid. The water is removed from a distillate of a first column using an adsorption unit, membrane, extractive column distillation, or a combination thereof.
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公开(公告)号：EP2590926A1
公开(公告)日：2013-05-15
申请号：EP11734223.8
申请日：2011-07-01
发明人： WARNER, R. Jay , HALE, Trinity , WOLLRAB, Radmila , JOHNSTON, Victor J. , LEE, David , OROSCO, Adam , SARAGER, Lincoln
IPC分类号： C07C31/08 , C07C29/149 , C07C29/80
CPC分类号： C07C29/149 , B01D3/002 , B01D3/143 , C07C29/80 , C07C31/08
摘要： Recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid and recovery of unreacted acetic acid from a weak acid stream. The unreacted acetic acid may be recovered as a dry acetic acid composition and may be directly or indirectly fed to the hydrogenation reactor.
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5.发明公开PROCESS FOR OBTAINING ETHANOL BY SEPARATION OF VAPOR CRUDE ETHANOL PRODUCT 审中-公开对于乙醇生产方法的蒸汽LIKE ROHETHANOLPRODUKTS分离
公开(公告)号：EP2590921A2
公开(公告)日：2013-05-15
申请号：EP11738875.1
申请日：2011-07-01
发明人： LEE, David , OROSCO, Adam , SARAGER, Lincoln , HALE, Trinity , VOLLRAB, Radmila , JOHNSTON, Victor, J.
IPC分类号： C07C29/149 , C07C29/80 , C07C31/08 , C07C29/76
CPC分类号： C07C29/80 , C07C29/149 , C07C29/76 , C07C31/08
摘要： Recovery of alcohol, in particular ethanol, by separating a vapor crude alcohol product obtained from the hydrogenation of acetic acid using a low energy process. The vapor crude ethanol product is separated in a column to produce a distillate stream comprising ethanol and at least one non-condensable gas. The vapor crude ethanol product may pass through a membrane before the first distillation column to separate the at least one non-condensable gas from the ethanol. The ethanol product is subsequently recovered from the distillate stream.
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6.发明授权
公开(公告)号：EP2702024B1
公开(公告)日：2017-09-20
申请号：EP12719222.7
申请日：2012-04-26
发明人： LEE, David , OROSCO, Adam , RIBEIRO, Claudio , WARNER, R., Jay , DECK, Robert, Alan , DUFF, Emily , JOHNSTON, Victor, J.
IPC分类号： C07C29/149 , C07C29/80 , C07C31/08 , C07C51/12 , C07C53/08
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公开(公告)号：EP2739598A1
公开(公告)日：2014-06-11
申请号：EP11746378.6
申请日：2011-08-03
发明人： LEE, David , OROSCO, Adam , SARAGER, Lincoln , WARNER, R. Jay , JEVTIC, Radmila , JOHNSTON, Victor J.
IPC分类号： C07C29/149 , C07C29/80 , C07C31/08
CPC分类号： C07C29/149 , C07C29/80 , C07C31/08
摘要： To reduce acetal concentrations when separating ethanol from a crude product in one or more distillation column, at least one of the columns is operated at a higher pressure to increase the equilibrium constant that favors hydrolysis of the acetal. The crude product may comprise ethanol, acetaldehyde, water and one or more acetals, such as diethyl acetal. The acetal concentration may be reduced thus reducing the need to separate acetal from the crude product.
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8.发明公开
公开(公告)号：EP2702024A1
公开(公告)日：2014-03-05
申请号：EP12719222.7
申请日：2012-04-26
发明人： LEE, David , OROSCO, Adam , RIBEIRO, Claudio , WARNER, R., Jay , DECK, Robert, Alan , DUFF, Emily , JOHNSTON, Victor, J.
IPC分类号： C07C29/149 , C07C29/76 , C07C29/80 , C07C29/84 , C07C31/08
摘要： A process for recovering ethanol obtained from the hydrogenation of acetic acid. The crude ethanol product is separated in a column to produce a distillate stream comprising acetaldehyde and ethyl acetate and a residue stream comprising ethanol, acetic acid, ethyl acetate and water. A portion of the first residue is separated in a second distillation column to yield a second residue comprising acetic acid and an vapor overhead comprising ethanol, ethyl acetate and water. Water is removed from at least a portion of the vapor overhead to yield an ethanol mixture stream having a lower water content than the at least a portion of the vapor overhead
摘要翻译： 从使用低能量处理从乙酸的氢化获得的粗乙醇产物回收乙醇。 粗乙醇产物是在塔中分离，以产生馏出物流包含乙醛和残余物流包含乙醇，乙酸，乙酸乙酯和水。 将乙醇产物从残余物物流回收。
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公开(公告)号：EP2590920A2
公开(公告)日：2013-05-15
申请号：EP11738531.0
申请日：2011-07-07
发明人： WARNER, R. Jay , HALE, Trinity , WOLLRAB, Radmila , JOHNSTON, Victor J. , LEE, David , OROSCO, Adam , SARAGER, Lincoln
IPC分类号： C07C29/149 , C07C29/90 , C07C67/08 , C07C29/88
CPC分类号： C07C29/141 , C07C29/149 , C07C29/88 , C07C29/90 , C07C67/08 , C07C31/08 , C07C69/14
摘要： Recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid and by reacting a portion of the crude ethanol product or one or more derivative streams containing ethyl acetate obtained therefrom in the presence of hydrogen, via hydrogenolysis. The one or more derivative streams comprise ethyl acetate that are reacted via hydrogenolysis to form additional ethanol that may be directly or indirectly fed to the separation zone or the hydrogenation reactor.
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10.发明授权
公开(公告)号：EP2702027B1
公开(公告)日：2014-12-24
申请号：EP12720736.3
申请日：2012-04-26
发明人： LEE, David , OROSCO, Adam , RIBEIRO, Claudio , WARNER, R. Jay , DECK, Robert Alan , DUFF, Emily , JOHNSTON, Victor J.
IPC分类号： C07C29/149 , C07C29/88
CPC分类号： C07C29/88 , C07C29/149 , C07C67/08 , C07C31/08 , C07C69/14
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