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    Process for the preparation of nitroguanidine derivatives starting from 2-nitroimino-hexahydro-1,3,5-triazines in the presence of ammonia, primary or secondary amine
    2.
    发明公开
    Process for the preparation of nitroguanidine derivatives starting from 2-nitroimino-hexahydro-1,3,5-triazines in the presence of ammonia, primary or secondary amine 失效
    一种制备由2-硝基亚氨基六氢-1,3,5-三嗪在氨，伯胺或仲胺的存在下起始的硝基胍衍生物的方法

    公开(公告)号：EP0869120A1

    公开(公告)日：1998-10-07

    申请号：EP98105850.6

    申请日：1998-03-31

    申请人： MITSUI CHEMICALS, INC.

    发明人： Ebihara, Koichi ,  Ura, Daisuke ,  Miyamoto, Michihiko ,  Kaiho, Tatsuo

    IPC分类号： C07D213/61 ,  C07D277/32 ,  C07D307/14

    CPC分类号： C07D277/32 ,  C07D407/06 ,  C07D417/06

    摘要： Described is a convenient process, as a substitute for hydrolysis, for preparing a nitroguanidine derivative represented by the following formula (2):
    wherein A represents a substituted or unsubstituted aromatic or non-aromatic hydrocarbon ring, a substituted or unsubstituted aromatic or non-aromatic heterocycle, a hydrogen atom or a substituted or unsubstituted alkyl, alkenyl or alkynyl group; and R 2 represents a hydrogen atom, a substituted or unsubstituted C 1-6 alkyl, alkenyl or alkynyl group, which comprises reacting a compound represented by the following formula (1):
    wherein R 1 represents a substituted or unsubstituted, linear or cyclic C 1-10 alkyl group and A and R 2 have the same meanings as defined above, with ammonia, a primary amine or a secondary amine, or a salt thereof.

    摘要翻译： 描述的是一个方便的方法中，作为用于水解的替代物，用于制备由下式表示的硝基胍衍生物（2）： worin甲darstellt一个substituiertem奥德unsubstituiertem芳族或非芳族烃环，substituiertem奥德unsubstituiertem芳族或 非芳族杂环，氢原子或substituiertem奥德unsubstituiertem烷基，烯基或炔基; 和R2 darstellt一个氢原子，substituiertem奥德unsubstituiertem C 1-6烷基，烯基或炔基，该方法包括使由下式表示的化合物（1）： worin R1 darstellt一个substituiertem奥德unsubstituiertem，直链或环状的C1 -10烷基以及A和R2具有与上述定义，与氨，伯胺或仲胺，或它们的盐的相同含义。