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1.发明公开1,3-Dialkyl-2-imidazolidinones and a manufacturing process therefor 有权1,3-二烷基-2-咪唑啉酮衍生物和Verfahren zu ihrer Herstellung
公开(公告)号：EP0992497A1
公开(公告)日：2000-04-12
申请号：EP99307978.9
申请日：1999-10-08
IPC分类号： C07D233/32
CPC分类号： C07D233/32 , B01J19/02 , B01J2219/00247 , B01J2219/00252 , B01J2219/0209 , B01J2219/024 , B01J2219/0254 , B01J2219/0281
摘要： 1,3-dialkyl-2-imidazolidinones are made by a process involving a direct one-step reaction from industrially available alkylene carbonate, N-alkylethanolamine or 1,2-diol; the process can minimize formation of solid material and can be readily conducted in a large-scale industrial production with high yield and few byproducts. The process is characterized in that alkylene carbonate, N-alkylethanolamine or 1,2-diol is reacted with monoalkylamine and carbon dioxide, alkylcarbamate alkylamine salt, and/or 1,3-dialkyurea, by heating them at 50°C or higher in a reactor whose area in contact with at least part of the reactants and/or products is made of a metal comprising titanium or zirconium and/or an oxide thereof, or an inorganic glass.
摘要翻译： 1,3-二烷基-2-咪唑啉酮通过涉及由工业上可获得的碳酸亚烷基酯，N-烷基乙醇胺或1,2-二醇的直接一步反应的方法制备; 该方法可以最小化固体材料的形成，并且可以容易地在高产率和少量副产物的大规模工业生产中进行。 该方法的特征在于，使碳酸亚烷基酯，N-烷基乙醇胺或1,2-二醇与单烷基胺和二
氧化碳，烷基氨基甲酸酯烷基胺盐和/或1,3-二
氨基脲反应，在50℃或更高温度下加热 反应物，其与至少部分反应物和/或产物接触的区域由包含钛或锆和/或其氧化物的金属或无机玻璃制成。-
公开(公告)号：EP1148051A3
公开(公告)日：2003-10-15
申请号：EP01115276.6
申请日：1999-10-08
IPC分类号： C07D233/32
CPC分类号： C07D233/32 , B01J19/02 , B01J2219/00247 , B01J2219/00252 , B01J2219/0209 , B01J2219/024 , B01J2219/0254 , B01J2219/0281
摘要： 1,3-dialkyl-2-imidazolidinones are made by a process involving a direct one-step reaction from industrially available alkylene carbonate, N-alkylethanolamine or 1,2-diol; the process can minimize formation of solid material and can be readily conducted in a large-scale industrial production with high yield and few byproducts. The process is characterized in that alkylene carbonate, N-alkylethanolamine or 1,2-diol is reacted with monoalkylamine and carbon dioxide, alkylcarbamate alkylamine salt, and/or 1,3-dialkyurea, by heating them at 50°C or higher in a reactor whose area in contact with at least part of the reactants and/or products is made of a metal comprising titanium or zirconium and/or an oxide thereof, or an inorganic glass.
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3.发明公开
公开(公告)号：EP1148051A2
公开(公告)日：2001-10-24
申请号：EP01115276.6
申请日：1999-10-08
IPC分类号： C07D233/32
CPC分类号： C07D233/32 , B01J19/02 , B01J2219/00247 , B01J2219/00252 , B01J2219/0209 , B01J2219/024 , B01J2219/0254 , B01J2219/0281
摘要： 1,3-dialkyl-2-imidazolidinones are made by a process involving a direct one-step reaction from industrially available alkylene carbonate, N-alkylethanolamine or 1,2-diol; the process can minimize formation of solid material and can be readily conducted in a large-scale industrial production with high yield and few byproducts. The process is characterized in that alkylene carbonate, N-alkylethanolamine or 1,2-diol is reacted with monoalkylamine and carbon dioxide, alkylcarbamate alkylamine salt, and/or 1,3-dialkyurea, by heating them at 50°C or higher in a reactor whose area in contact with at least part of the reactants and/or products is made of a metal comprising titanium or zirconium and/or an oxide thereof, or an inorganic glass.
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4.发明公开1,3-dialkyl-2-imidazolidinones and a manufacturing process therefor 审中-公开1,3-二烷基-2-咪唑啉酮衍生物和Verfahren zu ihrer Herstellung
公开(公告)号：EP1148052A3
公开(公告)日：2003-10-15
申请号：EP01115277.4
申请日：1999-10-08
IPC分类号： C07D233/32
CPC分类号： C07D233/32 , B01J19/02 , B01J2219/00247 , B01J2219/00252 , B01J2219/0209 , B01J2219/024 , B01J2219/0254 , B01J2219/0281
摘要： 1,3-dialkyl-2-imidazolidinones are made by a process involving a direct one-step reaction from industrially available alkylene carbonate, N-alkylethanolamine or 1,2-diol; the process can minimize formation of solid material and can be readily conducted in a large-scale industrial production with high yield and few byproducts. The process is characterized in that alkylene carbonate, N-alkylethanolamine or 1,2-diol is reacted with monoalkylamine and carbon dioxide, alkylcarbamate alkylamine salt, and/or 1,3-dialkyurea, by heating them at 50°C or higher in a reactor whose area in contact with at least part of the reactants and/or products is made of a metal comprising titanium or zirconium and/or an oxide thereof, or an inorganic glass.
摘要翻译： 1,3-二烷基-2-咪唑啉酮通过涉及由工业上可获得的碳酸亚烷基酯，N-烷基乙醇胺或1,2-二醇的直接一步反应的方法制备; 该方法可以最小化固体材料的形成，并且可以容易地在高产率和少量副产物的大规模工业生产中进行。 该方法的特征在于，使碳酸亚烷基酯，N-烷基乙醇胺或1,2-二醇与单烷基胺和二
氧化碳，烷基氨基甲酸酯烷基胺盐和/或1,3-二
氨基脲反应，在50℃或更高温度下加热 反应物，其与至少部分反应物和/或产物接触的区域由包含钛或锆和/或其氧化物的金属或无机玻璃制成。-
5.发明公开
公开(公告)号：EP1148052A2
公开(公告)日：2001-10-24
申请号：EP01115277.4
申请日：1999-10-08
IPC分类号： C07D233/32
CPC分类号： C07D233/32 , B01J19/02 , B01J2219/00247 , B01J2219/00252 , B01J2219/0209 , B01J2219/024 , B01J2219/0254 , B01J2219/0281
摘要： 1,3-dialkyl-2-imidazolidinones are made by a process involving a direct one-step reaction from industrially available alkylene carbonate, N-alkylethanolamine or 1,2-diol; the process can minimize formation of solid material and can be readily conducted in a large-scale industrial production with high yield and few byproducts. The process is characterized in that alkylene carbonate, N-alkylethanolamine or 1,2-diol is reacted with monoalkylamine and carbon dioxide, alkylcarbamate alkylamine salt, and/or 1,3-dialkyurea, by heating them at 50°C or higher in a reactor whose area in contact with at least part of the reactants and/or products is made of a metal comprising titanium or zirconium and/or an oxide thereof, or an inorganic glass.
摘要翻译： 1,3-二烷基-2-咪唑啉酮是通过包括来自工业上可获得的碳酸亚烷基酯，N-烷基乙醇胺或1,2-二醇的直接一步反应的方法制备的; 该方法可以使固体物质的形成最小化，并且可以容易地在高产率和少量副产物的大规模工业生产中进行。 该方法的特征在于碳酸亚烷基酯，N-烷基乙醇胺或1,2-二醇与单烷基胺和二氧化碳，烷基氨基甲酸酯烷基胺盐和/或1,3-二烷基脲在50℃或更高温度下在 与至少部分反应物和/或产物接触的面积由包含钛或锆和/或其氧化物的金属或无机玻璃制成。
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6.发明授权
公开(公告)号：EP0992497B1
公开(公告)日：2003-12-17
申请号：EP99307978.9
申请日：1999-10-08
IPC分类号： C07D233/32
CPC分类号： C07D233/32 , B01J19/02 , B01J2219/00247 , B01J2219/00252 , B01J2219/0209 , B01J2219/024 , B01J2219/0254 , B01J2219/0281
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