摘要:
This invention provides a method for rapidly detecting volatile substances of very high concern (SVHCs) in a textile. Based on the ion mobility spectrometry technique, this method may achieve rapid detection of 11 kinds of volatile SVHCs within 1-6 minutes, respectively, by means of direct introduction of textile samples or in combination with an efficient and convenient solvent extraction pretreatment step. The detection limit is less than 100ppm, which absolutely satisfies the mass fraction limit of 1000ppm prescribed in REACH Regulation of the European Union. This method may greatly shorten detection periods of these volatile organics and enable the possibility to realize online detection for these substances.
摘要:
The present invention discloses a sampling device for an ion migration spectrometer (IMS), comprising: an inner sleeve part, inside of which an inner cavity is defined, one end of the inner sleeve part is connected with an inlet of an migration pipe via an inner-layer channel, and the other end of the inner sleeve part is configured with an inner end cap having an inner opening; and an outer sleeve part, which is configured as an eccentric sleeve that is coaxial with the inner sleeve part and able to rotate with respect to the inner sleeve part, so as to form a sleeve cavity between the inner sleeve part and the outer sleeve part, wherein one end of the outer sleeve part is configured with at least one connecting opening that is selectively connected with the inner-layer channel, and the other end of the outer sleeve part is configured with an outer end cap, on which a first outer opening selectively connected with the inner opening and a second outer opening selectively connected with the sleeve cavity are configured, wherein the outer end cap is configured to be able to rotate between a first location and a second location with respect to the inner end cap, so as to selectively introduce a sample to be detected into the inner-layer channel via one of the inner cavity and the sleeve cavity. Moreover, the present invention further relates to a method for solid and gas sampling by using the above sampling device.
摘要:
Embodiments of the present invention provide an air dryer for an ion mobility spectrometer, comprising a heating element used to heat a thermal conduction device, thereby heating the desiccant. Embodiments of the present invention further provide a regeneration method, by which the operation mode of the ion mobility spectrometer may be switched, so that during a non-working time of the ion mobility spectrometer, the desiccant is heated and thereby regenerated. With the present invention, the desiccant is avoided from being regularly replaced, thereby improving the performance and increasing the service life of the dryer. Regeneration of thedesiccant is performed by making full use of the non-working time of the ion mobility spectrometerwithout affecting normal operation of instrument.
摘要:
The present invention relates to a method of improving detection sensitivity of an ion mobility spectrometer, comprising: inserting a sample into a sample receiving device of the ion mobility spectrometer; triggering an operation of spectra acquisition through an optocoupler; when the number of the acquired spectra reaches the level required to contain enough information for accurate detection of explosives with relatively high vapor pressure, adding a dopant instantly to the ionization region by controlling the ON/OFF-state of an electromagnetic valve; when the number of the acquired spectra reaches the level required to contain enough information for accurate detection of explosives with relatively low vapor pressure, stopping the acquisition operation, and turning off the electromagnetic valve so as to stop adding the dopant to the ionization region; analyzing all of the acquired spectra to obtain the detection result. The addition time of the dopant is controlled such that the dopant can take effect on the detection of some explosives with relatively low vapor pressure while the explosives which can be detected with higher sensitivity when no dopant is added can be analyzed in the case that the dopant concentration is very low, thereby achieving the optimal detection performance of the apparatus by taking account of its response to various explosives.