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公开(公告)号：EP3849960A1
公开(公告)日：2021-07-21
申请号：EP19773648.1
申请日：2019-09-10
发明人： DE VLIEGER, Dionysius Jacobus Maria , HUIZENGA, Pieter , MACKAY, Munro , KEYZER, Lucas Petrus Simon , MUTHUSAMY, Duraisamy
IPC分类号： C07C29/141 , C07C31/20
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公开(公告)号：EP3230244B1
公开(公告)日：2018-09-12
申请号：EP15805464.3
申请日：2015-12-04
CPC分类号： C07C29/84 , B01D3/40 , B01D3/4294 , C07C29/80 , C07C31/202 , C07C31/207
摘要： The invention provides a process for the separation of MEG and 1,2-BDO from a first mixture comprising MEG and 1,2-BDO, said process comprising the steps of: (i) providing said first mixture comprising MEG and 1,2-BDO as a feed to a distillation column; (ii) providing a feed comprising glycerol to the distillation column above the first mixture; (iii) operating the distillation column at a temperature in the range of from 50 to 250° C. and a pressure in the range of from 0.1 to 400 kPa; (iv) removing a stream comprising MEG and glycerol as a bottoms stream from the distillation column; and (v) (v) removing a stream comprising 1,2-BDO above the point at which the feed comprising glycerol is provided to the distillation column.
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公开(公告)号：EP3365317A1
公开(公告)日：2018-08-29
申请号：EP16790802.9
申请日：2016-10-18
IPC分类号： C07C29/132
CPC分类号： C07C29/132 , C07C29/60 , C07C31/202 , C07C31/205
摘要： Implementations of the disclosed subject matter provide methods for producing ethylene glycol from a carbohydrate feed may include contacting, in a first reactor under hydrogenation conditions, the carbohydrate feed with a bi-functional catalyst system. The bi-functional catalyst system may include a heterogeneous hydrogenation catalyst, and a soluble retro-Aldol catalyst. The carbohydrate feed may include a concentration of carbohydrate, in the total solution entering the first reactor, of 5-40 wt% in a solvent. An intermediate product stream may be obtained from the first reactor including ethylene glycol. The hydrogenation conditions may include a temperature in the range of from 180-250°C.
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5.发明公开PROCESS FOR THE PREPARATION OF MONOETHYLENE GLYCOL 审中-公开VERFAHREN ZUR HERSTELLUNG VON MONOETHYLEN-GLYCOL
公开(公告)号：EP2989085A1
公开(公告)日：2016-03-02
申请号：EP14719009.4
申请日：2014-04-23
IPC分类号： C07D307/46 , C07D307/50 , C07C59/185 , C12P19/02 , C13K3/00
CPC分类号： C07C29/132 , A23L2/60 , A23L27/34 , A23V2002/00 , C07C51/00 , C07D307/50 , C07D307/68 , C07H1/00 , C07H1/08 , C07H3/02 , C08G63/16 , C12P19/02 , C12P19/24 , C13K3/00 , C07C31/202 , C07C59/185
摘要： The invention provides a process for the preparation of monoethylene glycol from sucrose comprising the steps of: i) hydrolyzing sucrose to form a reaction product stream comprising glucose and fructose; ii) separating the reaction product stream comprising glucose and fructose into a fructose or fructose derivative rich stream and a glucose rich stream; and iii) contacting the glucose rich stream with hydrogen in a reactor in the presence of a solvent and a catalyst system with catalytic hydrogenation abilities to produce a product stream comprising monoethylene glycol.
摘要翻译： 本发明提供从蔗糖制备单乙二醇的方法，包括以下步骤：i）水解蔗糖以形成包含葡萄糖和果糖的反应产物流; ii）将包含葡萄糖和果糖的反应产物流分离成富含果糖或果糖衍生物流和富含葡萄糖的流; 和iii）在溶剂和具有催化氢化能力的催化剂体系的存在下在反应器中使富含葡萄糖的物流与氢气接触，以产生包含单乙二醇的产物流。
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公开(公告)号：EP3551600A1
公开(公告)日：2019-10-16
申请号：EP17808902.5
申请日：2017-12-04
IPC分类号： C07C29/132 , C07C29/60 , C07C29/00 , C07C31/20 , C07C31/26
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公开(公告)号：EP3280692B1
公开(公告)日：2019-03-06
申请号：EP16714417.9
申请日：2016-04-05
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公开(公告)号：EP3004038B1
公开(公告)日：2018-08-29
申请号：EP14726655.5
申请日：2014-05-28
CPC分类号： C07C29/86 , C07C29/80 , C07C31/202 , C07C31/205 , C07C31/207
摘要： The invention provides a process for the recovery of a first alcohol from a stream comprising two or more alcohols, said process comprising the steps of providing a stream comprising two or more alcohols, providing a solvent stream, combining said stream comprising two or more alcohols with said solvent stream in the presence of water and recovering at least a portion of the first alcohol by liquid-liquid extraction.
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公开(公告)号：EP3039002B1
公开(公告)日：2018-07-25
申请号：EP14758127.6
申请日：2014-08-29
IPC分类号： C07C29/132 , C07C29/60 , C07C31/20
CPC分类号： C07C29/60 , C07C29/132 , C07C31/202 , C07C31/205
摘要： The invention provides a process for the catalytic conversion of a saccharide-containing feedstock in a reactor, wherein saccharide-containing feedstock is provided to the reactor as a feed stream through a feed pipe and is contacted with a catalyst system in the reactor, wherein the saccharide-containing feedstock in the feed pipe is maintained at a temperature below the degradation temperature of the saccharide contained therein and a section of the wall of the reactor at the point where the feed pipe enters the reactor is cooled to a temperature below the temperature of the bulk of the reactor and the reactor contents.
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公开(公告)号：EP3215479A1
公开(公告)日：2017-09-13
申请号：EP15788091.5
申请日：2015-11-04
发明人： HUIZENGA, Pieter , FISCHER, Kai, Jürgen , DE VILLIERS, Waldo, Eugene , VELDHUIZEN, Dorien , BUS, Karin
CPC分类号： C07C29/86 , B01D11/0426 , B01D11/0492 , B01D2011/002 , C07C31/202 , C07C31/207
摘要： The invention provides a process for the separation of MEG and 1,2-BDO from a first mixture comprising MEG and 1,2-BDO in a first solvent by the steps of: (i) combining said first mixture with a second solvent stream comprising a second solvent in a first extraction column; (ii) recovering (a) a second mixture of MEG and 1,2-BDO in the second solvent, wherein the molar ratio of MEG:1,2-BDO is lower in the second mixture than in the first mixture; and (b) a solution comprising MEG in the first solvent; (iii) combining said second mixture with a first washing stream, said first washing stream also comprising the first solvent in a second extraction column; (iv) recovering (c) a first extract stream comprising the second solvent and 1,2-BDO and (d) a third mixture comprising MEG and, optionally, 1,2-BDO in the first solvent.
摘要翻译： 本发明提供了从包含MEG和1,2-BDO的第一混合物中分离第一溶剂中的MEG和1,2-BDO的方法，其步骤为：（i）将所述第一混合物与第二溶剂物流合并，所述第二溶剂物流包含 第一萃取塔中的第二溶剂; （ii）回收（a）在第二溶剂中的MEG和1,2-BDO的第二混合物，其中第二混合物中MEG：1,2-BDO的摩尔比低于第一混合物中MEG：1,2-BDO的摩尔比; 和（b）在第一溶剂中包含MEG的溶液; （iii）将所述第二混合物与第一洗涤物流混合，所述第一洗涤物流还包含第二萃取塔中的第一溶剂; （iv）在第一溶剂中回收（c）包含第二溶剂和1,2-BDO的第一提取物流和（d）包含MEG和任选的1,2-BDO的第三混合物。
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