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1.发明公开POSITIVE ELECTRODE ACTIVE MATERIAL POWDER, METHOD FOR PRODUCING SAME, AND NONAQUEOUS ELECTROLYTE SECONDARY BATTERY 有权粉末的正极活性物质，工艺用于生产和二次电池的非水电解质
公开(公告)号：EP2485305A1
公开(公告)日：2012-08-08
申请号：EP10820498.3
申请日：2010-09-28
发明人： YAMAMOTO, Manabu , NISHIKAWA, Daisuke , ISHIZAKI, Kazutoshi , KIKUYA, Kazuhiko , SANTOKI, Teruaki , SASAKI, Osamu , SADAMURA, Hideaki
CPC分类号： C01G51/50 , B82Y30/00 , C01G45/1228 , C01G51/42 , C01G53/42 , C01G53/50 , C01P2002/52 , C01P2002/72 , C01P2002/74 , C01P2002/76 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/40 , C01P2006/80 , H01M4/505 , H01M4/525 , Y02E60/122 , Y02P70/54
摘要： The present invention relates to positive electrode active substance particles comprising a compound having at least a crystal system belonging to a space group of R-3m and a crystal system belonging to a space group of C2/m, and boron, wherein the compound is a composite oxide comprising at least Li, Mn, and Co and/or Ni; a relative intensity ratio [(a)/(b)] of a maximum diffraction peak intensity (a) observed at 2θ = 20.8±1° in a powder X-ray diffraction pattern of the positive electrode active substance as measured using a Cu-Kα ray to a maximum diffraction peak intensity (b) observed at 28 = 18.6±1° in the powder X-ray diffraction pattern, is 0.02 to 0.5; a content of Mn in the positive electrode active substance particles is controlled such that a molar ratio of Mn/(Ni + Co + Mn) therein is not less than 0.55; and the positive electrode active substance particles comprise the boron in an amount of 0.001 to 3% by weight. The positive electrode active substance particles of the present invention are produced by calcining a mixture comprising precursor particles comprising Mn, and Ni and/or Co, a lithium compound and a boron compound at a temperature of 500 to 1500°C. The positive electrode active substance particles of the present invention can provide a secondary battery which can be improved in charge/discharge capacity and cycle characteristics.
摘要翻译： 本发明涉及包含具有的化合物的正极活性物质粒子的至少属于空间群R-3m的和属于空间群C2 / m的晶系，和硼，worin该化合物是晶体系统 复合氧化物包含至少锂，Mn和Co和/或Ni; 的相对强度比[（A）/（B）]的最大衍射峰强度（a）的观察在2 = 20.8±1°中的正极活性物质的粉末X射线衍射图案作为使用Cu测量 -K±射线到最大衍射峰强度（b）中，在28 =在粉末X射线衍射图案18.6±1°观察，是0时02分至0.5; Mn的正极活性物质粒子的含量被控制搜索那样的Mn /（镍+钴+ Mn）的摩尔比。其中不小于0:55; 和正极活性物质颗粒包含硼的重量为0.001至3％的量。 本发明的正极活性物质粒子通过煅烧一种混合物，包含前体颗粒包括锰，和Ni和/或Co，锂化合物和在500的温度下的硼化合物，以1500℃产生 本发明的正极活性物质颗粒可以提供一种二次电池可以在充电/放电容量和循环特性得到改善。
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2.发明公开Li-Ni COMPOSITE OXIDE PARTICLE POWDER AND METHOD FOR MANUFACTURING SAME, AND NONAQUEOUS ELECTROLYTE SECONDARY CELL 审中-公开LI-NI VERBUNDOXIDTEILCHENPULVER和方法及其制造并用无水ELEKTROLYT二次电池
公开(公告)号：EP2911224A1
公开(公告)日：2015-08-26
申请号：EP13847482.0
申请日：2013-10-15
发明人： ISHIZAKI, Kazutoshi , KIKUYA, Kazuhiko , SUGIHARA, Takahiko , SANTOKI, Teruaki , HARADA, Takamitsu , NISHIMURA, Masaki , MISHIMA, Yuji , SADAMURA, Hideaki
CPC分类号： H01M4/525 , C01G53/006 , C01G53/42 , C01G53/50 , C01P2002/50 , C01P2004/03 , C01P2004/32 , C01P2004/61 , C01P2006/12 , H01M4/485 , H01M4/505 , H01M10/052 , H01M10/0525 , Y02P70/54
摘要： The present invention relates to Li-Ni composite oxide particles that exhibit a high initial discharge capacity and are excellent in thermal stability when used as a positive electrode active substance for non-aqueous electrolyte secondary batteries, and a process for producing the Li-Ni composite oxide particles. The Li-Ni composite oxide particles of the present invention have a composition of Li x Ni 1-y-a-b Co y M1 a M2 b O 2 wherein x, y, a and b represent 1.00 ≤ x ≤ 1.10; 0
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3.发明公开Li-Ni COMPLEX OXIDE PARTICLE POWDER FOR NONAQUEOUS ELECTROLYTE SECONDARY BATTERY, METHOD FOR PRODUCING THE SAME, AND NONAQUEOUS ELECTROLYTE SECONDARY BATTERY 有权LI-NI复合氧化物颗粒粉末与水游离电解液，用于生产和二次电池二次电池用无水ELEKTROLYT
公开(公告)号：EP2128915A1
公开(公告)日：2009-12-02
申请号：EP08720340.2
申请日：2008-03-05
CPC分类号： C01G53/50 , C01G45/1228 , C01G51/50 , C01G53/42 , C01P2002/52 , C01P2002/85 , C01P2002/88 , C01P2004/62 , C01P2004/82 , C01P2006/37 , C01P2006/40 , H01M4/366 , H01M4/505 , H01M4/525 , H01M10/052
摘要： The present invention relates to Li-Ni composite oxide particles for a non-aqueous electrolyte secondary battery which have a large charge/discharge capacity and are excellent in thermal stability under a charged condition. The above object can be achieved by the Li-Ni composite oxide particles for a non-aqueous electrolyte secondary battery, comprising a Li-Ni composite oxide whose secondary particles form core particles thereof and have a composition represented by the formula: Li x1 Ni 1-y1-z1-w1 Co y1 Mn z1 M w1 O 2 (in which 0.9 ≤ x1 ≤ 1.3; 0.1 ≤ y1 ≤ 0.3; 0.0 ≤ z1 ≤ 0.3; 0 ≤ w1 s 0.1; and M is at least one metal selected from the group consisting of Al and Fe), wherein a Li-Ni composite oxide having a composition represented by the formula: Li x2 Ni 1-y2-z2-w2 Co y2 Mn z2 M w2 O 2 (in which 0.9 ≤ x2 ≤ 1 + z2; 0 ≤ y2 ≤ 0.33; 0 ≤ z2 ≤ 0.5; 0 ≤ w2 ≤ 0.1; and M is at least one metal selected from the group consisting of Al, Fe, Mg, Zr and Ti, is coated or present on a surface of the respective secondary particles.
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4.发明公开POSITIVE ELECTRODE MIXTURE AND NONAQUEOUS ELECTROLYTE SECONDARY CELL 审中-公开SEKUNDÄRZELLEMITNICHTWÄSSRIGEMELEKTROLYT的POSITIVELEKTRODENMISCHUNG
公开(公告)号：EP3113253A1
公开(公告)日：2017-01-04
申请号：EP15754705.0
申请日：2015-02-24
发明人： KAJIYAMA, Akihisa , SANTOKI, Teruaki , MORITA, Daisuke , MASAKI, Ryuta , SUGIHARA, Takahiko , WAKIYAMA, Tsuyoshi , MATSUMOTO, Kazutoshi , YODA, Akira , INADA, Taro , YOKOTA, Hiroshi , KAWASAKI, Takashi
CPC分类号： H01M4/364 , H01M4/131 , H01M4/136 , H01M4/505 , H01M4/525 , H01M4/5825 , H01M4/625 , H01M10/052 , H01M10/0525 , H01M2004/028
摘要： An object of the present invention is to provide a positive electrode mixture capable of conducting stable charging and discharging with a less amount of gasses generated which has an operating voltage or an initial crystal phase transition voltage of not less than 4.5 V on the basis of lithium. The present invention relates to a positive electrode mixture comprising carbon black having a bulk density of not more than 0.1 g/cm 3 , a crystallite size of 10 to 40 Å, an iodine adsorption of 1 to 150 mg/g, a volatile content of not more than 0.1% and a metal impurity content of not more than 20 ppm, and a positive electrode active substance having an operating voltage or an initial crystal phase transition voltage of not less than 4.5 V on the basis of lithium.
摘要翻译： 本发明的目的是提供一种正极混合物，其能够以较少量的气体进行稳定的充放电，其具有基于锂的工作电压或不小于4.5V的初始晶体相变电压 。 本发明涉及一种正极混合物，其包含炭黑，其堆积密度不超过0.1g / cm 3，微晶尺寸为10至40，碘吸附为1至150mg / g，挥发物含量为 不大于0.1％，金属杂质含量不大于20ppm，以及基于锂的工作电压或初始晶体相变电压不小于4.5V的正极活性物质。
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5.发明授权Li-Ni COMPOSITE OXIDE PARTICLE POWDER FOR RECHARGEABLE BATTERY WITH NONAQUEOUS ELECTROLYTE, PROCESS FOR PRODUCING THE Li-Ni COMPOSITE OXIDE PARTICLE POWDER, AND RECHARGEABLE BATTERY WITH NONAQUEOUS ELECTROLYTE 有权LI-NI VERBUNDOXIDTEILCHENPULVER有关充电电池与水不含电解质，METHOD FOR LI-NI VERBUNDOXIDTEILCHENPULVERS和可充电电池用无水ELEKTROLYT的生产
公开(公告)号：EP2104163B1
公开(公告)日：2014-06-04
申请号：EP07849798.9
申请日：2007-12-06
CPC分类号： H01M4/525 , C01G51/42 , C01G53/42 , C01P2002/52 , C01P2002/72 , C01P2002/88 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M10/052 , H01M10/446 , H01M2004/021
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6.发明授权LI-NI COMPLEX OXIDE PARTICLE POWDER FOR NONAQUEOUS ELECTROLYTE SECONDARY BATTERY, METHOD FOR PRODUCING THE SAME, AND NONAQUEOUS ELECTROLYTE SECONDARY BATTERY 有权LI-NI复合氧化物颗粒粉末与水游离电解液，用于生产和二次电池二次电池用无水ELEKTROLYT
公开(公告)号：EP2128915B1
公开(公告)日：2016-05-18
申请号：EP08720340.2
申请日：2008-03-05
IPC分类号： H01M4/52 , H01M4/36 , H01M4/50 , C01G45/12 , C01G51/00 , C01G53/00 , H01M4/505 , H01M4/525 , H01M10/052
CPC分类号： C01G53/50 , C01G45/1228 , C01G51/50 , C01G53/42 , C01P2002/52 , C01P2002/85 , C01P2002/88 , C01P2004/62 , C01P2004/82 , C01P2006/37 , C01P2006/40 , H01M4/366 , H01M4/505 , H01M4/525 , H01M10/052
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7.发明公开LI-NI-BASED COMPOSITE OXIDE PARTICLE POWDER FOR RECHARGEABLE BATTERY WITH NONAQUEOUS ELCTROLYTE, PROCESS FOR PRODUCING THE POWDER, AND RECHARGEABLE BATTERY WITH NONAQUEOUS ELECTROLYTE 有权VERBUNDOXIDPARTIKELPULVER ON LI-NI-BASE与水游离电解液，用于生产无水ELEKTROLYT粉末与电池的电池
公开(公告)号：EP2214234A1
公开(公告)日：2010-08-04
申请号：EP08849214.5
申请日：2008-11-11
发明人： KAJIYAMA, Akihisa , KIKUYA, Kazuhiko , SANTOKI, Teruaki , SASAKI, Osamu , NAKAMURA, Satoshi , IMAHASHI, Taiki , SADAMURA, Hideaki
CPC分类号： H01M4/48 , C01F7/141 , C01G45/1228 , C01G51/50 , C01G53/00 , C01G53/42 , C01G53/50 , C01P2002/52 , C01P2002/54 , C01P2004/03 , C01P2004/61 , C01P2004/84 , C01P2006/32 , C01P2006/40 , H01M4/505 , H01M4/525 , H01M10/052
摘要： The present invention relates to Li-Ni-based composite oxide particles comprising Mn, and Co and/or Al, wherein Co and Al are uniformly dispersed within the particles, and Mn is present with a gradient of its concentration in a radial direction of the respective particles such that a concentration of Mn on a surface of the respective particles is higher than that at a central portion thereof. The Li-Ni-based composite oxide particles can be produced by allowing an oxide and a hydroxide comprising Mn to mechanically adhere to Li-Ni-based oxide comprising Co and/or Al; and then heat-treating the obtained material at a temperature of not lower than 400°C and not higher than 1,000°C. The Li-Ni-based composite oxide particles of the present invention are improved in thermal stability and alkalinity.
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8.发明授权LI-NI-BASED COMPOSITE OXIDE PARTICLE POWDER FOR RECHARGEABLE BATTERY WITH NONAQUEOUS ELCTROLYTE, PROCESS FOR PRODUCING THE POWDER, AND RECHARGEABLE BATTERY WITH NONAQUEOUS ELECTROLYTE 有权VERBUNDOXIDPARTIKELPULVER ON LI-NI-BASE与水游离电解液，用于生产无水ELEKTROLYT粉末与电池的电池
公开(公告)号：EP2214234B1
公开(公告)日：2014-01-08
申请号：EP08849214.5
申请日：2008-11-11
发明人： KAJIYAMA, Akihisa , KIKUYA, Kazuhiko , SANTOKI, Teruaki , SASAKI, Osamu , NAKAMURA, Satoshi , IMAHASHI, Taiki , SADAMURA, Hideaki
CPC分类号： H01M4/48 , C01F7/141 , C01G45/1228 , C01G51/50 , C01G53/00 , C01G53/42 , C01G53/50 , C01P2002/52 , C01P2002/54 , C01P2004/03 , C01P2004/61 , C01P2004/84 , C01P2006/32 , C01P2006/40 , H01M4/505 , H01M4/525 , H01M10/052
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9.发明公开Li-Ni COMPOSITE OXIDE PARTICLE POWDER FOR RECHARGEABLE BATTERY WITH NONAQUEOUS ELECTROLYTE, PROCESS FOR PRODUCING THE Li-Ni COMPOSITE OXIDE PARTICLE POWDER, AND RECHARGEABLE BATTERY WITH NONAQUEOUS ELECTROLYTE 有权LI-NI VERBUNDOXIDTEILCHENPULVER有关充电电池与水不含电解质，METHOD FOR LI-NI VERBUNDOXIDTEILCHENPULVERS和可充电电池用无水ELEKTROLYT的生产
公开(公告)号：EP2104163A1
公开(公告)日：2009-09-23
申请号：EP07849798.9
申请日：2007-12-06
IPC分类号： H01M4/52
CPC分类号： H01M4/525 , C01G51/42 , C01G53/42 , C01P2002/52 , C01P2002/72 , C01P2002/88 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M10/052 , H01M10/446 , H01M2004/021
摘要： The present invention relates to Li-Ni composite oxide particles for a non-aqueous electrolyte secondary cell which have a large charge/discharge capacity, an excellent packing density and excellent storage performance. The Li-Ni composite oxide particles for a non-aqueous electrolyte secondary cell which have a composition represented by the formula:
Li x Ni 1-y-z Co y Al z O 2
in which 0.9 2 thereto, and a sulfate ion content of not more than 1.0%, can be produced by mixing Ni-Co hydroxide particles having a sulfate ion content of not more than 1.0% whose surface is coated with an Al compound having a primary particle diameter of not more than 1 µm, with a lithium compound; and calcining the resulting mixture.
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