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1.发明公开VERFAHREN ZUR HERSTELLUNG VON SiOH-FUNKTIONELLEN POLYSILOXANEN 有权VERFAHREN ZUR HERSTELLUNG VON SILICIUM-OH-FUNKTIONELLEN POLYSILOXANEN
公开(公告)号：EP3016994A1
公开(公告)日：2016-05-11
申请号：EP14730938.9
申请日：2014-06-18
申请人： Wacker Chemie AG
摘要： The invention relates to a continuous method for producing organopolysiloxanes having an OH content of 3.0 to 10.0 wt%. In said method, chlorosilanes, alkoxysilanes, water, and non-polar solvent soluble in water at no more than 1 g in 1 l water at 20°C and 1 bar are continuously added to the reaction mixture in a metered manner and reaction mixture is continuously discharged. In said method, in parallel with each other, the chlorosilanes are added in a metered manner at a weight fraction of 95% to 60% and the alkoxysilanes are added in a metered manner at a weight fraction of 5% to 40% with respect to the sum of chlorosilanes and alkoxysilanes. No polar solvents are added in a metered manner.
摘要翻译： OH含量为3.0-10.0％（重量）的有机聚硅氧烷通过连续供给基本上不溶于水的氯硅烷，烷氧基硅烷，水和非极性溶剂，连续排出溶解在溶剂相中的含有机聚硅氧烷的反应混合物， 任选地从溶剂相中分离有机聚硅氧烷，其中基于氯硅烷和烷氧基硅烷的总重量，氯硅烷和烷氧基硅烷以相应的重量分数加入95-60％和5-40％。 该方法不使用极性溶剂，并产生具有改善闪点的产品，同时最大限度地降低废水处理的复杂性和费用。
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3.发明公开
公开(公告)号：EP2408832A1
公开(公告)日：2012-01-25
申请号：EP10705880.2
申请日：2010-03-01
申请人： Wacker Chemie AG
发明人： STANJEK, Volker , WEWERS, Wolfgang
CPC分类号： C08G18/718 , C08G18/10 , C08G18/4825 , C08G18/65 , C08G18/837 , C08G2101/0025 , C08K5/01 , C08K5/06 , C08L75/04 , C08L75/12 , C08G18/289 , C08L2666/28
摘要： The invention relates to the continuous production of prepolymers (A) having end groups of the general formula (1): (R
1 )
a (R
2 )
3-a Si-X-A, wherein the end groups (1) can be identical or different, A is a two-band link group selected from - (R
3 )N-CO-NH-, -HN-CO-N(R
3 )-, -O-CO-HN-, -HN-CO-O-, S-CO-HN-, -HN-CO-S-, X is a two-band, linear or branched alkyl group, optionally substituted with halogen atoms, having 1-10 carbon atoms, R
1 is an alkyl, cycloalkyl, alkenyl or aryl residue, optionally substituted with halogen, having 1-10 carbon atoms, R
2 is an alkoxy residue -OR
3 , an acetoxy residue -O-CO-R
3 , an oxime radical -O-N=C(R
3 )
2 or an amine residue -NHR
3 or -NR
3
2 R
3 is hydrogen, a linear, cyclical or branched radical, substituted with heteroatoms, having 1 to 18 carbon atoms, R
4 is a linear, branched or cross-linked polymer radical, a is 0, 1 or 2, and n is a whole number that is at least 1, wherein the prepolymers (A) are produced by a continuous method comprising at least one reaction of an isocyanate group (-N=C=O) having at least one isocyanate reactive group, that is carried out continuously in at least one reactor (R), that enables heat dissipation capacities of greater than 5kW/ (m
3. K) in the laminar flow region.-
4.发明授权
公开(公告)号：EP2686328B1
公开(公告)日：2014-10-01
申请号：EP12708135.4
申请日：2012-03-09
申请人： Wacker Chemie AG
IPC分类号： C07F7/18
CPC分类号： C07F7/188
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5.发明公开
公开(公告)号：EP2686328A1
公开(公告)日：2014-01-22
申请号：EP12708135.4
申请日：2012-03-09
申请人： Wacker Chemie AG
IPC分类号： C07F7/18
CPC分类号： C07F7/188
摘要： Organosilicon compounds bearing SiOC groups and having low residual silicon-bonded chlorine are prepared continuously by reacting a chlorosilane with alcohol and optionally water by contacting a gaseous phase containing alcohol with a liquid phase containing silane, organosilicon intermediates, organosilicon compounds containing SiOC groups and optional inert solvent in a reaction column in which the gas phase passes through the liquid phase in bubble form, or is provided with a vaporizer operating by a crossflow principle.
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6.发明授权
公开(公告)号：EP2408832B1
公开(公告)日：2012-12-26
申请号：EP10705880.2
申请日：2010-03-01
申请人： Wacker Chemie AG
发明人： STANJEK, Volker , WEWERS, Wolfgang
CPC分类号： C08G18/718 , C08G18/10 , C08G18/4825 , C08G18/65 , C08G18/837 , C08G2101/0025 , C08K5/01 , C08K5/06 , C08L75/04 , C08L75/12 , C08G18/289 , C08L2666/28
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