SYNTHESIS OF TETRABUTYLAMMONIUM BIS(FLUOROSULFONYL)IMIDE AND RELATED SALTS
    10.
    发明公开
    SYNTHESIS OF TETRABUTYLAMMONIUM BIS(FLUOROSULFONYL)IMIDE AND RELATED SALTS 审中-公开
    合成TETRABUTYLAMMONIAK双(氟磺酰基)IMID及相关的盐的

    公开(公告)号:EP2920147A4

    公开(公告)日:2016-06-22

    申请号:EP13855564

    申请日:2013-11-15

    申请人: TRINAPCO INC

    发明人: JOHNSON MARTIN R

    摘要: The present invention is directed to methods comprising adding ammonia, either as an ammonium salt or as a gas at pressures below 0.01 MPa, to a sulfuryl fluoride solution to form the anion of bis(fluorosulfonyl)amine under conditions well suited for large-scale production. The bis(fluorosulfonyl)amine so produced can be isolated by methods described in the prior art, or isolated as an organic ion pair, such as an alkylammonium solid salt, or as an ionic liquid.