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    Fluorinated graphite fibers and method of manufacturing them
    4.
    发明公开
    Fluorinated graphite fibers and method of manufacturing them 失效
    氟化石墨纤维及其制造方法

    公开(公告)号：EP0421306A3

    公开(公告)日：1991-11-27

    申请号：EP90118749.2

    申请日：1990-09-28

    申请人： YAZAKI CORPORATION ,  MITSUBISHI CORPORATION

    发明人： Endo, Morinobu ,  Ohashi, Yoshio ,  Katsumata, Makoto ,  Yamanashi, Hidenori

    IPC分类号： D01F11/12

    CPC分类号： D01F11/121

    摘要： Fluorinated graphite fibers comprising an intercalated compound of graphite fibers having a three-dimensional crystal structure in which carbon hexagonal network faces are substantially in parallel with the axis of fibers and oriented in a coaxial manner and fluorine, wherein the length of repeating periods in the direction of C-axis of the crystals coexist within a range from 5 to 24 Å. The fluorinated carbon fibers are manufactured by graphitizing gas phase-grown carbon fibers obtained by thermally decomposing a hydrocarbon compound in a non-oxidative atmosphere under the presence of a catalyst supported on a substrate or bringing ultra-fine metal particles catalyst suspended in a high temperature zone into contact with a hydrocarbon compound, thereby obtaining graphite fibers having a three-dimensional crystal structure in which the carbon hexagonal network faces are substantially in parallel with the axis of fibers and oriented in a coaxial manner and then bringing them into contact with fluorine.

    Process for the formation of intercalated carbonaceous fibrous material of increased electrical conductivity and fibrous material thus obtained
    5.
    发明公开
    Process for the formation of intercalated carbonaceous fibrous material of increased electrical conductivity and fibrous material thus obtained 失效
    一种用于具有增加的导电性和将如此获得的纤维材料制备存储Kohlenstoffasermaterials过程。

    公开(公告)号：EP0015729A2

    公开(公告)日：1980-09-17

    申请号：EP80300611.3

    申请日：1980-02-29

    申请人： CELANESE CORPORATION

    发明人： Kalnin, Ilmar L.

    IPC分类号： D01F11/10 ,  D01F9/22 ,  H01B1/04

    CPC分类号： D01F11/12 ,  D01F11/121 ,  H01B1/04

    摘要： The formation of improved intercalated graphitic carbon fibers of further diminished electrical resistivity (i.e., increased electrical conductivity) is made possible. Not only is the specific electrical resistivity of the resulting fibers reduced (e.g., to extremely low levels no greater than that of copper in preferred embodiments), but the desirable tensile properties of the fibers are maintained at a satisfactory level even after intercalation. A carbonaceous fibrous material containing the usual turbostratic graphitic carbon which is derived from an acrylonitrile homopolymer or a closely related copolymer (as defined) is selected and is structurally modified in a manner which has been found to render it particularly suited for intercalation as evidenced by a further reduction in the electrical resistivity of the resulting intercalated fibrous material while retaining other desirable properties. More specifically, the carbonaceous fibrous material (as defined) prior to intercalation with an electron acceptor intercalating agent is modified via an atypical extremely high temperature treatment so as to yield a modified structure which can be evidenced upon wide angle x-ray diffraction analysis, i.e. resolved graphitic Miller index (100) and (101) reflections and the presence of a (112) reflection are observed, which surprisingly has been found capable of subsequently yielding an improved intercalated product having a substantially reduced electrical resistivity. The intercalated product finds utility as an improved lightweight electrical conductor.

    摘要翻译： 进一步降低电阻率（即，增加的导电性）的改进的插层石墨碳纤维的形成成为可能。 不仅是得到的纤维的比电阻率降低（例如，以非常低的水平不高于铜在优选实施例中的更大），但纤维的理想的拉伸性质保持在即使嵌入之后令人满意的水平。 含通常的乱层石墨碳的所有这是从在丙烯腈均聚物或密切相关的共聚物（如定义的）衍生的碳质纤维材料被选择并且在已经发现其通过所证明，以使其特别适合于嵌入的方式在结构上被修饰的 在所得到的插层纤维材料的电阻率进一步减小，同时保持其它所需性能。 更具体地，碳质纤维材料（如定义的）之前，在电子受体插入剂有嵌插经由修改，以非典型的极高温处理，以得到改性结构，其能够在宽角X-射线衍射分析来证实，即 解决石墨晶面指数（100）和（101）反射和（112）反射的存在下观察，其令人惊讶地，已经发现能产生以随后改善具有显着减小的电阻率插产物。 插层产品发现可用作改善轻便电导体。

    Fluorinated graphite fibers and method of manufacturing them
    10.
    发明公开
    Fluorinated graphite fibers and method of manufacturing them 失效
    Fluorierte Graphitfasern und Verfahren zu deren Herstellung。

    公开(公告)号：EP0421306A2

    公开(公告)日：1991-04-10

    申请号：EP90118749.2

    申请日：1990-09-28

    申请人： YAZAKI CORPORATION ,  MITSUBISHI CORPORATION

    发明人： Endo, Morinobu ,  Ohashi, Yoshio ,  Katsumata, Makoto ,  Yamanashi, Hidenori

    IPC分类号： D01F11/12

    CPC分类号： D01F11/121

    摘要： Fluorinated graphite fibers comprising an intercalated compound of graphite fibers having a three-dimensional crystal structure in which carbon hexagonal network faces are substantially in parallel with the axis of fibers and oriented in a coaxial manner and fluorine, wherein the length of repeating periods in the direction of C-axis of the crystals coexist within a range from 5 to 24 Å. The fluorinated carbon fibers are manufactured by graphitizing gas phase-grown carbon fibers obtained by thermally decomposing a hydrocarbon compound in a non-oxidative atmosphere under the presence of a catalyst supported on a substrate or bringing ultra-fine metal particles catalyst suspended in a high temperature zone into contact with a hydrocarbon compound, thereby obtaining graphite fibers having a three-dimensional crystal structure in which the carbon hexagonal network faces are substantially in parallel with the axis of fibers and oriented in a coaxial manner and then bringing them into contact with fluorine.

    摘要翻译： 氟化石墨纤维，其包含具有三维晶体结构的石墨纤维的插入化合物，其中碳六方网络面基本上与纤维轴平行并且以同轴方式定向并且氟，其中在方向上的重复周期的长度 的晶体的C轴共存在5至24安培的范围内。 氟化碳纤维通过将石墨化气化生成的碳纤维制造，所述碳纤维通过在负载在基材上的催化剂的存在下在非氧化性气氛中热分解烃化合物而获得，或者使悬浮在高温下的超细金属颗粒催化剂 区域与烃化合物接触，从而获得具有三维晶体结构的石墨纤维，其中碳六方网络面基本上与纤维轴平行并且以同轴方式取向，然后使其与氟接触。