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    APPARATUS AND PROCESS FOR PRODUCING DIMETHYL CARBONATE
    3.
    发明公开
    APPARATUS AND PROCESS FOR PRODUCING DIMETHYL CARBONATE 审中-公开

    公开(公告)号：EP4011857A1

    公开(公告)日：2022-06-15

    申请号：EP21212795.5

    申请日：2021-12-07

    Applicant: Blueplasma Power, S.L.

    Inventor： ARAYA BRENES, MARIO

    IPC: C07C29/151 ,  C07C31/04 ,  C07C68/04 ,  C07C69/96

    Abstract: The present application relates to an apparatus and process for producing dimethyl carbonate, in particular a system (apparatus or process) for DMC synthesis without the need of using a dehydrating agent. More particularly, the feed mixture for the process can be selected from the following options: a) carbon monoxide, methanol and flue gas from the process, b) synthesis gas without CO 2 and flue gas from the process, c) synthesis gas with CO 2 and added synthesis gas from purified flue gas from the process. The process uses a catalyst cluster comprising a specific combination of different groups of heterogeneous catalysts wherein each group has a different function. Also the invention relates to an apparatus comprising a specific combination of heterogeneous catalysts for applying different routes to produce dimethyl carbonate from each feed mixture option, on continuous basis.

    METHOD FOR PRODUCING A CARBONIC ESTER
    8.
    发明授权
    METHOD FOR PRODUCING A CARBONIC ESTER 有权
    方法产生的二氧化碳酯的研究

    公开(公告)号：EP1460056B1

    公开(公告)日：2011-10-05

    申请号：EP02793446.2

    申请日：2002-12-27

    Applicant: Asahi Kasei Chemicals Corporation

    Inventor： MIYAKE, Nobuhisa ,  NAGAHARA, Hajime

    IPC: C07C68/04 ,  C07C69/96 ,  C07C68/08

    CPC classification number: C07C68/08 ,  C07C68/04 ,  C07C69/96

    Abstract: A process for producing a carbonic ester which comprises the steps of: (1) reacting an organometallic compound having a metal-oxygen-carbon bond with carbon dioxide to obtain a reaction mixture containing a carbonic ester formed by the reaction; (2) separating the carbonic ester from the reaction mixture to obtain a liquid residue; and (3) reacting the liquid residue with an alcohol to form an organometallic compound having a metal-oxygen-carbon bond and water, removing the water from the organometallic compound, and recovering the organometallic compound obtained in the step (3) in order to recycle it to the step (1).

    PROCESS FOR PRODUCTION OF ALKYL TIN ALKOXIDE COMPOUND, AND PROCESS FOR PRODUCTION OF CARBONATE ESTER USING THE COMPOUND
    9.
    发明公开
    PROCESS FOR PRODUCTION OF ALKYL TIN ALKOXIDE COMPOUND, AND PROCESS FOR PRODUCTION OF CARBONATE ESTER USING THE COMPOUND 有权
    制造方法ALKYLZINNOXIDVERBINDUNG和方法，用于生产碳酸酯的使用连接

    公开(公告)号：EP2226328A1

    公开(公告)日：2010-09-08

    申请号：EP09804784.8

    申请日：2009-03-31

    Applicant: Asahi Kasei Chemicals Corporation

    Inventor： SHINOHATA, Masaaki ,  MIYAKE, Nobuhisa

    IPC: C07F7/22 ,  C07C68/04 ,  C07C69/96 ,  C07B61/00

    CPC classification number: C07F7/2232 ,  C07C68/04 ,  C07C69/96

    Abstract: The present invention provides a process for producing : a compound represented by XOR 2 ; a dialkyl tin dialkoxide compound having one tin atom, two Sn-R 1 bonds and two Sn-OR 2 bonds; and/or a tetraalkyl dialkoxy distannoxane compound having one Sn-O-Sn bond, in which each tin atom of the tetraalkyl dialkoxy distannoxane compound has two Sn-R 1 bonds and one Sn-OR 2 bond, the process comprising reacting in the absence of a catalyst at least one alkyl tin compound selected from the group consisting of i) and ii) below:
    i) a dialkyl tin compound having one tin atom, two Sn-R 1 (wherein R 1 represents an alkyl group) bonds, and two Sn-OX bonds (wherein OX is a group in which HOX that is a conjugate acid of OX is a Bronsted acid having a pKa of from 0 to 6.8); and
    ii) a tetraalkyl distannoxane compound having one Sn-O-Sn bond, in which each tin atom of the tetraalkyl distannoxane compound has two Sn-R 1 bonds and one Sn-OX bond (wherein OX is a group in which HOX that is a conjugate acid of OX is a Bronsted acid having a pKa of from 0 to 6.8); and

    a carbonic acid ester represented by R 2 OCOOR 2 (wherein R 2 represents a linear or branched, saturated or unsaturated hydrocarbon group, a hydrocarbon group having a saturated or unsaturated cyclic hydrocarbon substituent, or a Y-CH 2 - group (wherein Y represents an alkyl polyalkylene group, an aromatic group or a cyclic saturated or unsaturated alkylene ether group)), and/or
    an alcohol represented by R 2 OH (wherein R 2 is the same as defined above).

    Abstract translation: 本发明提供了生产的方法：通过XOR 2所示的化合物; 具有一个锡原子，2个Sn-R 1个键和2个Sn-OR 2键的二烷基锡二醇盐化合物; 和/或具有一个的Sn-O-斯恩·邦德四烷基二烷氧基distannoxanes化合物，其中，所述四烷基二烷氧基distannoxanes化合物的各锡原子具有2个Sn-R 1个键和一个的Sn-OR 2键，该方法包括在不存在起反应 催化剂选自I的）和选择的至少一种烷基锡化合物II）所示：i）具有一个锡原子的二烷基锡化合物，2个Sn-R 1（worin，R 1个darstellt到的烷基）键和 2个Sn-OX键（worin OX是其中HOX的基团确实是OX的共轭酸是具有pKa在0〜6.8的布朗斯台德酸）; 和ii）具有一个的Sn-O-斯恩·邦德四烷基distannoxanes化合物，其中所述四烷基distannoxanes化合物的各锡原子具有2个Sn-R 1个键和一个的Sn-OX键（worin OX是其中HOX的基团即 OX的共轭酸是具有pKa在0〜6.8）布朗斯台德酸; 并且由R表示的碳酸酯2 OCOOR 2（worin R 2表示直链或支链的，饱和或不饱和烃基，具有的烃基的饱和或不饱和环状烃取代基，或者Y-CH 2 - 基（worinÿ 烷基聚亚烷基的darstellt，芳族基或环状饱和或不饱和亚烷基醚基）），和/或醇的R 2 OH（worin R2至表示的与上述相同的定义）。

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