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公开(公告)号：JP2009263338A
公开(公告)日：2009-11-12
申请号：JP2009056721
申请日：2009-03-10
申请人： Daiso Co Ltd , ダイソー株式会社
发明人： FUJIMOTO RYOSUKE , KAGAWA NAOTO , TAKENAKA KEIJI , KITAMURA TORU , OTAKA SEIJI , ISHIHARA TOSHIYUKI , MIKI YASUSHI , KOYANAGI KEIJI
IPC分类号： C07D301/26 , C07D303/08
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method of epichlorohydrin, by dechlorohydrogenation of a dichlorohydrin mainly composed of 1,3-dichloro-2-propanol, which is excellent in the light of yield, waste water load, and energy used in its manufacturing.
SOLUTION: In a process in which epichlorohydrin is generated by dechlorohydrogenation of a dichlorohydrin mainly composed of 1,3-dichloro-2-propanol, it was found that the reaction liquid after dechlorohydrogenation of dichlorohydrin can be separated by the difference of specific gravities of an oil layer and a water layer, and that the property of liquid separation can be controlled by limiting the molar ratio of 1,3-dichloro-2-propanol and 2,3-dichloro-1-propanol of the dichlorohydrin to be dechlorohydrogenated within 87:13-100:0. Optionally, the resultant oil layer and the water layer are treated intermediately.
COPYRIGHT: (C)2010,JPO&INPIT摘要翻译： 待解决的问题：为了提供表氯醇的制造方法，通过氯化氢化主要由1,3-二氯-2-丙醇组成的二氯丙醇，其在产率，废水负荷和使用的能量方面是优异的 在其制造。 解决方案：在主要由1,3-二氯-2-丙醇组成的二氯丙醇的脱氯氢化产生表氯醇的过程中，发现二氯丙醇脱氯氢化后的反应液可以通过特定的 油层和水层的重量，液体分离性能可以通过将二氯丙醇的1,3-二氯-2-丙醇和2,3-二氯-1-丙醇的摩尔比限制为 在87：13-100：0内脱氯氢化。 任选地，中间处理所得的油层和水层。 版权所有（C）2010，JPO＆INPIT
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2.发明专利Method for producing dichlorohydrin exhibiting high selectivity of 1,3-dichloro-2-propanol 有权生产展示1,3-二氯-2-丙醇的高选择性的二氯乙醇的方法
公开(公告)号：JP2009155260A
公开(公告)日：2009-07-16
申请号：JP2007334926
申请日：2007-12-26
申请人： Daiso Co Ltd , ダイソー株式会社
摘要： PROBLEM TO BE SOLVED: To provide a method for producing dichlorohydrin exhibiting high selectivity of 1,3-dichloro-2-propanol by decreasing the content in dichlorohydrin of 2,3-dichloro-1-propanol exhibiting a low reaction rate in the dehydrochlorination reaction in the production of dichlorohydrin by chlorinating glycerol.
SOLUTION: In the reaction process of chlorinating glycerol, while 1,3-dichloro-2-propanol is produced via 3-chloro-1,2-propanediol, 2-chloro-1,3-propanediol does not further react to produce 2,3-dichloro-1-propanol resulting in temporary apparent accumulation of 2-chloro-1,3-propanediol. The problem is solved by removing apparently accumulating 2-chloro-1,3-propanediol as an intermediate of 2,3-dichloro-1-propanol.
COPYRIGHT: (C)2009,JPO&INPIT摘要翻译： 待解决的问题：提供一种通过降低2,3-二氯-1-丙醇的二氯丙醇含量显示低反应速率的二氯丙醇的含量，生成二氯丙醇的方法，其显示出高选择性的1,3-二氯-2-丙醇 通过氯化甘油制备二氯丙醇时的脱氯化氢反应。 解决方案：在氯化甘油的反应过程中，虽然通过3-氯-1,2-丙二醇生产1,3-二氯-2-丙醇，但是2-氯-1,3-丙二醇不会进一步反应 产生2,3-二氯-1-丙醇，导致2-氯-1,3-丙二醇的暂时明显的积累。 该问题通过除去显着积累的2-氯-1,3-丙二醇作为2,3-二氯-1-丙醇的中间体来解决。 版权所有（C）2009，JPO＆INPIT
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公开(公告)号：JP2009096727A
公开(公告)日：2009-05-07
申请号：JP2007267253
申请日：2007-10-12
申请人： Daiso Co Ltd , ダイソー株式会社
发明人： KITAMURA TORU , MIKI YASUSHI , ISHIHARA TOSHIYUKI
IPC分类号： C07D303/08 , C07B61/00 , C07D301/26
摘要： PROBLEM TO BE SOLVED: To provide a method for producing epichlorohydrin by collecting dichlorohydrin by distillation or the like without using a special device by eliminating hydrogen chloride contained in a reaction mixture obtained by the production of the dichlorohydrin by using glycerol as a raw material without neutralization with a base, and carrying out the dehydrochlorination of the collected dichlorohydrin. SOLUTION: It has been found that the problem can be solved by eliminating the hydrogen chloride contained in the reaction mixture formed by the production of the dichlorohydrin by the reaction with the epichlorohydrin of the objective substance of the reaction by the repeated various studies for solving the problem. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译： 待解决的问题：提供一种通过蒸馏等收集二氯丙醇来制备表氯醇的方法，而不使用特殊装置，除去通过使用甘油作为原料制备二氯丙醇得到的反应混合物中所含的氯化氢 没有用碱中和的物质，并进行所收集的二氯丙醇的脱氯化氢。 解决方案：已经发现，通过重复的各种研究，通过与反应的目标物质的表氯醇反应，除去由二氯丙醇生产形成的反应混合物中所含的氯化氢，可以解决该问题 解决问题。 版权所有（C）2009，JPO＆INPIT
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公开(公告)号：JP2009292812A
公开(公告)日：2009-12-17
申请号：JP2009111695
申请日：2009-05-01
申请人： Daiso Co Ltd , ダイソー株式会社
发明人： KITAMURA TORU , TAKENAKA KEIJI , OTAKA SEIJI , ISHIHARA TOSHIYUKI , KAGAWA NAOTO , MIKI YASUSHI
IPC分类号： C07C67/58 , B01J31/04 , B01J31/40 , B01J38/00 , C07B61/00 , C07C29/62 , C07C29/86 , C07C31/34 , C07C31/42 , C07C69/63
CPC分类号： Y02P20/584
摘要： PROBLEM TO BE SOLVED: To provide a method for recovering a catalyst in a simple process with low energy in producing chlorohydrins by a chlorinating reaction of a multihydroxy group-substituted aliphatic hydrocarbon and/or an ester of the multihydroxy group-substituted hydrocarbon using a carboxylic acid-based compound as the catalyst. SOLUTION: It is found that the catalyst present as an ester of the chlorohydrins can be recovered by extracting oligomers of the multihydroxy group-substituted aliphatic hydrocarbon, produced as a by-product in a chlorinating step, in an extraction step, and carrying out separation thereof. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译： 待解决的问题：提供一种通过多羟基取代的脂族烃和/或多羟基取代烃的酯的氯化反应以简单的方法回收催化剂的方法，其中低能量生产氯氢化物 使用羧酸类化合物作为催化剂。 解决方案：发现作为氯氢化物的酯存在的催化剂可以通过提取在提取步骤中作为副产物在氯化步骤中产生的多羟基取代的脂族烃的低聚物来回收，以及 进行分离。 版权所有（C）2010，JPO＆INPIT
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公开(公告)号：JP2009249309A
公开(公告)日：2009-10-29
申请号：JP2008097123
申请日：2008-04-03
申请人： Daiso Co Ltd , ダイソー株式会社
发明人： ISHIHARA TOSHIYUKI , KITAMURA TORU , MIKI YASUSHI , TAKENAKA KEIJI , OTAKA SEIJI , KAGAWA NAOTO
IPC分类号： C07C29/64 , C07B61/00 , C07C31/36 , C07D303/08
摘要： PROBLEM TO BE SOLVED: To reduce the amount of an alkali required in a subsequent dehydrochlorination process and the amount of water and a salt formed in the dehydrochlorination process by efficiently recovering hydrogen chloride from the resulting reaction mixture in the process of producing dichlorohydrin by way of chlorinating glycerin.
SOLUTION: It has been discovered that the above problem can be solved by separating and recovering hydrogen chloride gas by way of heating at least a part of the reaction mixture comprising dichlorohydrin, hydrogen chloride and water obtained by chlorinating glycerin.
COPYRIGHT: (C)2010,JPO&INPIT摘要翻译： 待解决的问题：为了减少随后的脱氯化氢过程中所需的碱的量以及在脱氯化氢过程中形成的盐的量，在生产二氯丙醇的过程中从所得反应混合物中有效地回收氯化氢 通过氯化甘油。 解决方案：已经发现，通过加热至少一部分包含二氯丙醇，氯化氢和通过氯化甘油获得的水的反应混合物，可以分离和回收氯化氢气体来解决上述问题。 版权所有（C）2010，JPO＆INPIT
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公开(公告)号：JP2001239234A
公开(公告)日：2001-09-04
申请号：JP2000053066
申请日：2000-02-29
申请人： DAISO CO LTD
IPC分类号： B09B3/00
摘要： PROBLEM TO BE SOLVED: To provide an organic waste treating material which enables using the bacteria which are naturally attached to organic waste as they are, promoting the propagation of the fermentation decomposition bacteria and stably continuing high decomposing rate for a long term in the fermentation decomposition method of extinct decomposition type. SOLUTION: Chaff containing 10% water (1.2 kg), powdery 4MgCO3.Mg(OH)2.5H2O(500 gr) and service water (2 kg) are charged into a garbage treating machine as the base material for treatment and the temperature of the vessel contents is elevated up to 50 deg.C under stirring. Subsequently, the garbage (1 kg) composed of cabbage (230 gr), Japanese radish (160 gr), onion (100 gr), boiled rice (150 gr), raw sardine (30 gr), pork (90 gr), mandarine orange (30 gr), apple (90 gr) and macaroni (120 gr) is charged into the garbage treating machine. After the charging, the treatment temperature is set 50 deg.C, is continuously stirred for 3 hr after the charging and, thereafter, the intermittent string operation comprising stopping for 50 min and stirring for 10 min is repeated.
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公开(公告)号：JPH07206974A
公开(公告)日：1995-08-08
申请号：JP105294
申请日：1994-01-11
申请人： DAISO CO LTD
IPC分类号： G02B1/04 , C08F290/00 , C08F290/06 , C08G18/67 , C08G18/71 , C08G18/73 , C08G18/76
摘要： PURPOSE:To provide a polymerizable composition having a high refractive index and a high Abbe number, excellent in workability, moldability, heat resistance and impact resistance, and useful for plastic lenses, etc., by adding a specific amount of a monoisocyanate, etc., to a specified mixture. CONSTITUTION:This polymerizable composition is obtained by adding a monoisocyanate and/or a tertiary polyisocyanate, such as isopropenyl-alpha, alpha- dimethylbenzylisocyanate, in an amount of 0.1-2 equivalent based on alcoholic hydroxyl groups in a mixture to the mixture obtained by dissolving (A) 20-60 pts.wt. of a multi-functional (meth)acrylate in (B) 80-40 pts.wt. of a styrenic compound or a radically polymerizable monofunctional unsaturated monomer mixture solution containing the styrenic compound. The multi-functional (meth) acrylate has alcoholic hydroxyl groups in the molecule, aromatic groups replaced with phenyl groups or halogen atoms excluding a fluorine atom, and two or more (meth)acryloyl groups, and is represented by the formula (R is H, methyl; X is halogen other than fluorine, phenyl; Y is isopropylidene, -CH2-, SO2, etc.; m1,m2 are 1,2; n1 is 1-6).
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公开(公告)号：JP2002179801A
公开(公告)日：2002-06-26
申请号：JP2000384030
申请日：2000-12-18
申请人： DAISO CO LTD , TEIJIN LTD
IPC分类号： E04F15/10 , B29C43/18 , B29C45/00 , B32B25/04 , B32B27/36 , C08G81/00 , C08K3/00 , C08L67/02
摘要： PROBLEM TO BE SOLVED: To provide a resin material for a laminated flooring tile, and to provide the laminated flooring tile so controlled that no chlorine is emitted when the tile is incinerated, having such plasticity as equal to that of conventional tiles even though no plasticizer is added thereto, having good workability, and excellent in abrasion resistance and heat resistance. SOLUTION: This resin material for the laminated flooring tile contains a polyester-based elastomer. The polyester-based elastomer preferably comprises a polybutylene terephthalate-based elastomer, and more preferably comprises a block copolymer comprising polybutylene terephthalate and an amorphous or lowly crystalline aromatic polyester. A block copolymer which is formed by using a high-melting, highly crystalline aromatic polyester as hard segments and the amorphous or lowly crystalline aromatic polyester as soft segments is exemplified as the polyester-based elastomer. Further, the resin material for the laminated flooring tile may contain polyethylene terephthalate resin.
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