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    Method for producing carried ruthenium oxide, and method for producing chlorine
    7.
    发明专利
    Method for producing carried ruthenium oxide, and method for producing chlorine 有权
    生产载体氧化锆的方法及其生产方法

    公开(公告)号：JP2013169516A

    公开(公告)日：2013-09-02

    申请号：JP2012035874

    申请日：2012-02-22

    申请人： Sumitomo Chemical Co Ltd ,  住友化学株式会社

    发明人： NISHIMOTO JUNICHI

    IPC分类号： B01J23/46 ,  B01J37/14 ,  C01B7/04

    摘要： PROBLEM TO BE SOLVED: To provide a method for producing carried ruthenium oxide excelling in thermal stability and catalyst life, and a method for producing chlorine stably for many hours using the carried ruthenium oxide obtained by the method.SOLUTION: A method for producing carried ruthenium oxide obtained by supporting ruthenium oxide on a titanium carrier includes carrying out contact treatment of the titanium carrier in a solution containing a ruthenium compound and a solvent, and then drying the titanium carrier until the content of the solvent reaches 0.10-15 wt.% based on the weight of the titanium carrier; and holding an obtained dry product in a state of containing 1.0-15 wt% solvent based on the weight of the titanium carrier, and then baking the dried product in an oxidizing gas atmosphere. The carried ruthenium oxide produced by this method is used as a catalyst, and hydrogen chloride is oxidized with oxygen in the presence of this catalyst to produce chlorine.

    摘要翻译： 要解决的问题：提供一种制备具有良好的热稳定性和催化剂寿命的载体氧化钌的方法，以及使用通过该方法获得的携带的氧化钌稳定地生产氯的方法。溶液：一种制备载体钌的方法 通过在钛载体上负载氧化钌而获得的氧化物包括在含有钌化合物和溶剂的溶液中进行钛载体的接触处理，然后干燥钛载体，直到溶剂的含量达到基于0.10-15重量％ 关于钛载体的重量; 并以所述钛载体的重量含有1.0-15重量％溶剂的状态保存所得的干燥产物，然后在氧化气体气氛中烘烤所述干燥产物。 使用该方法生产的携带的氧化钌用作催化剂，并在该催化剂存在下用氧气将氯化氢氧化以产生氯。

    Method for producing supported ruthenium oxide, and method for production of chlorine
    8.
    发明专利
    Method for producing supported ruthenium oxide, and method for production of chlorine 审中-公开
    生产支持的氧化钌的方法及其生产方法

    公开(公告)号：JP2013146720A

    公开(公告)日：2013-08-01

    申请号：JP2012095374

    申请日：2012-04-19

    申请人： Sumitomo Chemical Co Ltd ,  住友化学株式会社

    发明人： NISHIMOTO JUNICHI

    IPC分类号： B01J23/46 ,  B01J37/14 ,  C01B7/04

    摘要： PROBLEM TO BE SOLVED: To provide a method for producing a supported ruthenium oxide comprising making a titania carrier efficiently support ruthenium oxide and silica, the supported ruthenium oxide having excellent thermal stability and catalyst lifetime; and to provide a method for stably producing chlorine over a long time using the supported ruthenium oxide obtained by the above method.SOLUTION: A method for producing a supported ruthenium oxide formed by supporting ruthenium oxide and silica on a titania carrier includes: contact-treating the titania carrier with a solution including an alkoxysilane compound and water; performing a first calcination under an oxidizing gas atmosphere; and performing a second calcination under the oxidizing gas atmosphere after contact treatment with a ruthenium compound. Using the supported ruthenium oxide produced by the above method as a catalyst, chlorine is produced by oxidizing hydrogen chloride with oxygen in the presence of the catalyst.

    摘要翻译： 要解决的问题：提供一种制备负载氧化钌的方法，包括使二氧化钛载体有效地支撑氧化钌和二氧化硅，所述负载氧化钌具有优异的热稳定性和催化剂寿命; 并提供使用通过上述方法获得的负载氧化钌来长时间稳定地生产氯的方法。解决方案：通过在氧化钛载体上负载氧化钌和二氧化硅形成的负载氧化钌的制备方法包括：接触处理 具有包含烷氧基硅烷化合物和水的溶液的二氧化钛载体; 在氧化气体气氛下进行第一次煅烧; 并在与钌化合物接触处理之后在氧化气体气氛下进行第二次煅烧。 使用通过上述方法制备的负载型氧化钌作为催化剂，在催化剂存在下，用氧氧化氯化氢制备氯。

    Production method of chlorine
    9.
    发明专利
    Production method of chlorine 有权

    公开(公告)号：JP5189954B2

    公开(公告)日：2013-04-24

    申请号：JP2008280262

    申请日：2008-10-30

    申请人： 住友化学株式会社

    发明人： 航平 関 ,  宣仁 大本

    IPC分类号： C01B7/04

    CPC分类号： C01B7/0718 ,  B01J20/08 ,  B01J20/28061 ,  B01J21/063 ,  B01J21/08 ,  B01J23/26 ,  B01J23/462 ,  B01J23/72 ,  C01B7/04 ,  Y02P20/228

    摘要： Disclosed is a process for producing chlorine, which makes it possible to successfully continue an oxidation reaction, even if sulfur component-containing hydrogen chloride is used. This process comprises a step of feeding sulfur component-containing hydrogen chloride and oxygen into a reaction tube 1 comprising a catalyst packed bed 10, to thereby oxidize the hydrogen chloride to produce chlorine, wherein the catalyst packed bed 10 includes an alumina-mixed catalyst packed bed 20 formed of a mixture of a catalyst 3 with alumina (or a diluent 4), and wherein the BET specific surface area of the alumina is from 10 to 500 m 2 /g. Preferably, the alumina is ³-alumina and/or ¸-alumina.